data_Os2PdPb
_symmetry_space_group_name_H-M   'P 1'
_cell_length_a   2.9
_cell_length_b   4.86
_cell_length_c   4.89
_cell_angle_alpha   90.0
_cell_angle_beta   90.11
_cell_angle_gamma   90.0
_symmetry_Int_Tables_number   1
_chemical_formula_structural   Os2PdPb
_chemical_formula_sum   'Os2 Pd1 Pb1'
_cell_volume   69.01
_cell_formula_units_Z   1
loop_
 _symmetry_equiv_pos_site_id
 _symmetry_equiv_pos_as_xyz
  1  'x, y, z'
loop_
 _atom_site_type_symbol
 _atom_site_label
 _atom_site_symmetry_multiplicity
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_occupancy
  Os  Os0  1  0.14  0.43  0.1  1.0
  Os  Os1  1  0.75  0.43  0.8  1.0
  Pd  Pd3  1  0.0  0.0  0.0  1.0
  Pb  Pb2  1  0.45  0.0  0.45  1.0

data_Os2PdPb
_symmetry_space_group_name_H-M   P1
_cell_length_a   2.9
_cell_length_b   4.86
_cell_length_c   4.89
_cell_angle_alpha   90.0
_cell_angle_beta   90.11
_cell_angle_gamma   90.0
_symmetry_Int_Tables_number   1
_chemical_formula_structural   Os2PdPb
_chemical_formula_sum   'Os2 Pd1 Pb1'
_cell_volume   69.01
_cell_formula_units_Z   1
loop_
 _symmetry_equiv_pos_site_id
 _symmetry_equiv_pos_as_xyz
  1  'x, y, z'
loop_
 _atom_site_type_symbol
 _atom_site_label
 _atom_site_symmetry_multiplicity
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_occupancy
  Pd  Pd0  1  0.0  0.0  0.0  1.0
  Os  Os1  1  0.14  0.43  0.1  1.0
  Os  Os2  1  0.75  0.43  0.8  1.0
  Pb  Pb3  1  0.45  0.0  0.45  1.0

Os Os Pd Pb
Os2PdPb crystallizes in the triclinic P1 space group. There are two inequivalent Os sites. In the first Os site, Os(1) is bonded in a 1-coordinate geometry to one Os(2), two equivalent Pd(1), and three equivalent Pb(1) atoms. The Os(1)-Os(2) bond length is 1.86 Å. There is one shorter (2.19 Å) and one longer (2.84 Å) Os(1)-Pd(1) bond length. There are a spread of Os(1)-Pb(1) bond distances ranging from 2.84-3.38 Å. In the second Os site, Os(2) is bonded in a 1-coordinate geometry to one Os(1), two equivalent Pd(1), and three equivalent Pb(1) atoms. There is one shorter (2.43 Å) and one longer (3.03 Å) Os(2)-Pd(1) bond length. There are a spread of Os(2)-Pb(1) bond distances ranging from 2.84-3.38 Å. Pd(1) is bonded in a 10-coordinate geometry to two equivalent Os(1), two equivalent Os(2), two equivalent Pd(1), and four equivalent Pb(1) atoms. Both Pd(1)-Pd(1) bond lengths are 2.90 Å. There are a spread of Pd(1)-Pb(1) bond distances ranging from 2.53-3.15 Å. Pb(1) is bonded in a 12-coordinate geometry to three equivalent Os(1), three equivalent Os(2), four equivalent Pd(1), and two equivalent Pb(1) atoms. Both Pb(1)-Pb(1) bond lengths are 2.90 Å.