DyC11NH8O8CH crystallizes in the triclinic P-1 space group. The structure consists of two 02329_fluka molecules inside a DyC11NH8O8 framework. In the DyC11NH8O8 framework, Dy(1) is bonded in a 9-coordinate geometry to one O(1), one O(2), one O(4), one O(5), one O(6), one O(7), one O(8), and two equivalent O(3) atoms. The Dy(1)-O(1) bond length is 2.42 Å. The Dy(1)-O(2) bond length is 2.47 Å. The Dy(1)-O(4) bond length is 2.48 Å. The Dy(1)-O(5) bond length is 2.43 Å. The Dy(1)-O(6) bond length is 2.41 Å. The Dy(1)-O(7) bond length is 2.29 Å. The Dy(1)-O(8) bond length is 2.35 Å. There is one shorter (2.37 Å) and one longer (2.69 Å) Dy(1)-O(3) bond length. There are eleven inequivalent C sites. In the first C site, C(1) is bonded in a distorted bent 120 degrees geometry to one C(2), one N(1), and one H(5) atom. The C(1)-C(2) bond length is 1.42 Å. The C(1)-N(1) bond length is 1.32 Å. The C(1)-H(5) bond length is 1.09 Å. In the second C site, C(2) is bonded in a trigonal planar geometry to one C(1), one C(3), and one C(4) atom. The C(2)-C(3) bond length is 1.49 Å. The C(2)-C(4) bond length is 1.39 Å. In the third C site, C(3) is bonded in a distorted bent 120 degrees geometry to one C(2), one O(1), and one O(2) atom. The C(3)-O(1) bond length is 1.29 Å. The C(3)-O(2) bond length is 1.27 Å. In the fourth C site, C(4) is bonded in a trigonal planar geometry to one C(2), one C(5), and one C(6) atom. The C(4)-C(5) bond length is 1.50 Å. The C(4)-C(6) bond length is 1.42 Å. In the fifth C site, C(5) is bonded in a distorted bent 120 degrees geometry to one C(4), one O(3), and one O(4) atom. The C(5)-O(3) bond length is 1.27 Å. The C(5)-O(4) bond length is 1.27 Å. In the sixth C site, C(6) is bonded in a trigonal planar geometry to one C(11), one C(4), and one C(7) atom. The C(6)-C(11) bond length is 1.43 Å. The C(6)-C(7) bond length is 1.42 Å. In the seventh C site, C(7) is bonded in a distorted single-bond geometry to one C(6) and one H(6) atom. The C(7)-H(6) bond length is 1.09 Å. In the eighth C site, C(9) is bonded in a distorted single-bond geometry to one C(10) and one H(8) atom. The C(9)-C(10) bond length is 1.38 Å. The C(9)-H(8) bond length is 1.09 Å. In the ninth C site, C(10) is bonded in a distorted single-bond geometry to one C(11), one C(9), and one H(9) atom. The C(10)-C(11) bond length is 1.41 Å. The C(10)-H(9) bond length is 1.09 Å. In the tenth C site, C(11) is bonded in a distorted trigonal planar geometry to one C(10), one C(6), and one N(1) atom. The C(11)-N(1) bond length is 1.37 Å. In the eleventh C site, C(12) is bonded in a distorted bent 120 degrees geometry to one O(5) and one O(6) atom. The C(12)-O(5) bond length is 1.28 Å. The C(12)-O(6) bond length is 1.25 Å. N(1) is bonded in a trigonal planar geometry to one C(1), one C(11), and one H(2) atom. The N(1)-H(2) bond length is 1.67 Å. There are eight inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one O(7) atom. The H(1)-O(7) bond length is 0.99 Å. In the second H site, H(2) is bonded in a distorted linear geometry to one N(1) and one O(7) atom. The H(2)-O(7) bond length is 1.02 Å. In the third H site, H(3) is bonded in a distorted single-bond geometry to one O(1) and one O(8) atom. The H(3)-O(1) bond length is 1.67 Å. The H(3)-O(8) bond length is 1.00 Å. In the fourth H site, H(4) is bonded in a single-bond geometry to one O(8) atom. The H(4)-O(8) bond length is 0.98 Å. In the fifth H site, H(5) is bonded in a single-bond geometry to one C(1) atom. In the sixth H site, H(6) is bonded in a single-bond geometry to one C(7) atom. In the seventh H site, H(8) is bonded in a single-bond geometry to one C(9) atom. In the eighth H site, H(9) is bonded in a single-bond geometry to one C(10) atom. There are eight inequivalent O sites. In the first O site, O(1) is bonded in a 3-coordinate geometry to one Dy(1), one C(3), and one H(3) atom. In the second O site, O(2) is bonded in a distorted single-bond geometry to one Dy(1) and one C(3) atom. In the third O site, O(3) is bonded in a distorted single-bond geometry to two equivalent Dy(1) and one C(5) atom. In the fourth O site, O(4) is bonded in a distorted single-bond geometry to one Dy(1) and one C(5) atom. In the fifth O site, O(5) is bonded in a distorted single-bond geometry to one Dy(1) and one C(12) atom. In the sixth O site, O(6) is bonded in a distorted bent 120 degrees geometry to one Dy(1) and one C(12) atom. In the seventh O site, O(7) is bonded in a distorted water-like geometry to one Dy(1), one H(1), and one H(2) atom. In the eighth O site, O(8) is bonded in a water-like geometry to one Dy(1), one H(3), and one H(4) atom. Linkers: 2 [O]C(=O)c1cnc2ccccc2c1C([O])=O ,1 [O]C(=O)C([O])=O. Metal clusters: 2 [Dy]. RCSR code: bey. The MOF has largest included sphere 2.32 A, density 2.49 g/cm3, surface area 2470.21 m2/g, accessible volume 0.06 cm3/g