Ni4C86N16H74O19(CH)16(CH2)20(CH2CO)3 is Indium-derived structured and crystallizes in the triclinic P1 space group. The structure is zero-dimensional and consists of sixteen 02329_fluka molecules, twenty 02329_fluka molecules, three dimethyl ether molecules, and one Ni4C86N16H74O19 cluster. In the Ni4C86N16H74O19 cluster, there are four inequivalent Ni sites. In the first Ni site, Ni(1) is bonded in a rectangular see-saw-like geometry to one N(1), one N(9), one O(2), and one O(7) atom. The Ni(1)-N(1) bond length is 1.88 Å. The Ni(1)-N(9) bond length is 1.91 Å. The Ni(1)-O(2) bond length is 1.88 Å. The Ni(1)-O(7) bond length is 1.90 Å. In the second Ni site, Ni(2) is bonded in an octahedral geometry to one N(10), one N(2), one O(1), one O(10), one O(6), and one O(8) atom. The Ni(2)-N(10) bond length is 2.09 Å. The Ni(2)-N(2) bond length is 2.02 Å. The Ni(2)-O(1) bond length is 2.07 Å. The Ni(2)-O(10) bond length is 2.13 Å. The Ni(2)-O(6) bond length is 2.15 Å. The Ni(2)-O(8) bond length is 2.10 Å. In the third Ni site, Ni(3) is bonded in a distorted octahedral geometry to one N(16), one N(7), one O(11), one O(13), one O(15), and one O(17) atom. The Ni(3)-N(16) bond length is 2.04 Å. The Ni(3)-N(7) bond length is 2.01 Å. The Ni(3)-O(11) bond length is 2.09 Å. The Ni(3)-O(13) bond length is 2.19 Å. The Ni(3)-O(15) bond length is 2.15 Å. The Ni(3)-O(17) bond length is 2.11 Å. In the fourth Ni site, Ni(4) is bonded in a distorted octahedral geometry to one N(15), one N(8), one O(12), one O(14), one O(16), and one O(18) atom. The Ni(4)-N(15) bond length is 2.03 Å. The Ni(4)-N(8) bond length is 2.02 Å. The Ni(4)-O(12) bond length is 2.10 Å. The Ni(4)-O(14) bond length is 2.21 Å. The Ni(4)-O(16) bond length is 2.10 Å. The Ni(4)-O(18) bond length is 2.14 Å. There are eighty-six inequivalent C sites. In the first C site, C(1) is bonded in a distorted single-bond geometry to one C(3) and one H(5) atom. The C(1)-C(3) bond length is 1.40 Å. The C(1)-H(5) bond length is 1.09 Å. In the second C site, C(2) is bonded in a distorted single-bond geometry to one C(4) and one H(6) atom. The C(2)-C(4) bond length is 1.40 Å. The C(2)-H(6) bond length is 1.09 Å. In the third C site, C(3) is bonded in a distorted single-bond geometry to one C(1), one C(5), and one N(1) atom. The C(3)-C(5) bond length is 1.42 Å. The C(3)-N(1) bond length is 1.39 Å. In the fourth C site, C(4) is bonded in a distorted single-bond geometry to one C(2), one C(6), and one N(2) atom. The C(4)-C(6) bond length is 1.42 Å. The C(4)-N(2) bond length is 1.39 Å. In the fifth C site, C(5) is bonded in a distorted trigonal planar geometry to one C(3), one C(7), and one N(3) atom. The C(5)-C(7) bond length is 1.40 Å. The C(5)-N(3) bond length is 1.39 Å. In the sixth C site, C(6) is bonded in a distorted single-bond geometry to one C(4), one C(8), and one N(4) atom. The C(6)-C(8) bond length is 1.40 Å. The C(6)-N(4) bond length is 1.39 Å. In the seventh C site, C(7) is bonded in a distorted single-bond geometry to one C(5) and one H(7) atom. The C(7)-H(7) bond length is 1.09 Å. In the eighth C site, C(8) is bonded in a distorted single-bond geometry to one C(6) and one H(8) atom. The C(8)-H(8) bond length is 1.09 Å. In the ninth C site, C(13) is bonded in a distorted trigonal planar geometry to one C(15), one N(1), and one N(3) atom. The C(13)-C(15) bond length is 1.48 Å. The C(13)-N(1) bond length is 1.35 Å. The C(13)-N(3) bond length is 1.37 Å. In the tenth C site, C(14) is bonded in a distorted trigonal planar geometry to one C(16), one N(2), and one N(4) atom. The C(14)-C(16) bond length is 1.48 Å. The C(14)-N(2) bond length is 1.34 Å. The C(14)-N(4) bond length is 1.37 Å. In the eleventh C site, C(15) is bonded in a distorted trigonal non-coplanar geometry to one C(13), one H(13), one H(15), and one H(17) atom. The C(15)-H(13) bond length is 1.10 Å. The C(15)-H(15) bond length is 1.10 Å. The C(15)-H(17) bond length is 1.10 Å. In the twelfth C site, C(16) is bonded in a distorted trigonal non-coplanar geometry to one C(14), one H(14), one H(16), and one H(18) atom. The C(16)-H(14) bond length is 1.09 Å. The C(16)-H(16) bond length is 1.10 Å. The C(16)-H(18) bond length is 1.10 Å. In the thirteenth C site, C(17) is bonded in a distorted trigonal non-coplanar geometry to one N(3); one H(19); and one H(21,22) atom. The C(17)-N(3) bond length is 1.46 Å. The C(17)-H(19) bond length is 1.10 Å. The C(17)-H(21,22) bond length is 1.10 Å. In the fourteenth C site, C(18) is bonded in a distorted trigonal non-coplanar geometry to one N(4); one H(20); and one H(21,22) atom. The C(18)-N(4) bond length is 1.46 Å. The C(18)-H(20) bond length is 1.10 Å. The C(18)-H(21,22) bond length is 1.10 Å. In the fifteenth C site, C(25) is bonded in a distorted trigonal non-coplanar geometry to one N(5), one H(35), and one H(37) atom. The C(25)-N(5) bond length is 1.46 Å. The C(25)-H(35) bond length is 1.10 Å. The C(25)-H(37) bond length is 1.10 Å. In the sixteenth C site, C(26) is bonded in a distorted trigonal non-coplanar geometry to one N(6), one H(36), and one H(38) atom. The C(26)-N(6) bond length is 1.46 Å. The C(26)-H(36) bond length is 1.10 Å. The C(26)-H(38) bond length is 1.10 Å. In the seventeenth C site, C(27) is bonded in a distorted single-bond geometry to one C(29), one C(37), and one N(5) atom. The C(27)-C(29) bond length is 1.39 Å. The C(27)-C(37) bond length is 1.42 Å. The C(27)-N(5) bond length is 1.39 Å. In the eighteenth C site, C(28) is bonded in a distorted single-bond geometry to one C(30), one C(38), and one N(6) atom. The C(28)-C(30) bond length is 1.39 Å. The C(28)-C(38) bond length is 1.42 Å. The C(28)-N(6) bond length is 1.39 Å. In the nineteenth C site, C(29) is bonded in a distorted single-bond geometry to one C(27) and one H(39) atom. The C(29)-H(39) bond length is 1.09 Å. In the twentieth C site, C(30) is bonded in a distorted single-bond geometry to one C(28) and one H(40) atom. The C(30)-H(40) bond length is 1.09 Å. In the twenty-first C site, C(35) is bonded in a distorted single-bond geometry to one C(37) and one H(45) atom. The C(35)-C(37) bond length is 1.40 Å. The C(35)-H(45) bond length is 1.09 Å. In the twenty-second C site, C(36) is bonded in a distorted single-bond geometry to one C(38) and one H(46) atom. The C(36)-C(38) bond length is 1.40 Å. The C(36)-H(46) bond length is 1.09 Å. In the twenty-third C site, C(37) is bonded in a distorted single-bond geometry to one C(27), one C(35), and one N(7) atom. The C(37)-N(7) bond length is 1.39 Å. In the twenty-fourth C site, C(38) is bonded in a distorted single-bond geometry to one C(28), one C(36), and one N(8) atom. The C(38)-N(8) bond length is 1.39 Å. In the twenty-fifth C site, C(39) is bonded in a distorted trigonal planar geometry to one C(41), one N(5), and one N(7) atom. The C(39)-C(41) bond length is 1.48 Å. The C(39)-N(5) bond length is 1.37 Å. The C(39)-N(7) bond length is 1.33 Å. In the twenty-sixth C site, C(40) is bonded in a distorted trigonal planar geometry to one C(42), one N(6), and one N(8) atom. The C(40)-C(42) bond length is 1.48 Å. The C(40)-N(6) bond length is 1.37 Å. The C(40)-N(8) bond length is 1.34 Å. In the twenty-seventh C site, C(41) is bonded in a distorted trigonal non-coplanar geometry to one C(39), one H(47), one H(49), and one H(51) atom. The C(41)-H(47) bond length is 1.10 Å. The C(41)-H(49) bond length is 1.10 Å. The C(41)-H(51) bond length is 1.10 Å. In the twenty-eighth C site, C(42) is bonded in a distorted trigonal non-coplanar geometry to one C(40), one H(48), one H(50), and one H(52) atom. The C(42)-H(48) bond length is 1.10 Å. The C(42)-H(50) bond length is 1.10 Å. The C(42)-H(52) bond length is 1.10 Å. In the twenty-ninth C site, C(43) is bonded in a distorted single-bond geometry to one C(53) and one H(53) atom. The C(43)-C(53) bond length is 1.40 Å. The C(43)-H(53) bond length is 1.08 Å. In the thirtieth C site, C(44) is bonded in a distorted single-bond geometry to one C(54) and one H(54) atom. The C(44)-C(54) bond length is 1.40 Å. The C(44)-H(54) bond length is 1.08 Å. In the thirty-first C site, C(49) is bonded in a distorted single-bond geometry to one C(51) and one H(59) atom. The C(49)-C(51) bond length is 1.40 Å. The C(49)-H(59) bond length is 1.09 Å. In the thirty-second C site, C(50) is bonded in a distorted single-bond geometry to one C(52) and one H(60) atom. The C(50)-C(52) bond length is 1.40 Å. The C(50)-H(60) bond length is 1.09 Å. In the thirty-third C site, C(51) is bonded in a distorted single-bond geometry to one C(49), one C(53), and one N(11) atom. The C(51)-C(53) bond length is 1.42 Å. The C(51)-N(11) bond length is 1.39 Å. In the thirty-fourth C site, C(52) is bonded in a distorted single-bond geometry to one C(50), one C(54), and one N(12) atom. The C(52)-C(54) bond length is 1.42 Å. The C(52)-N(12) bond length is 1.39 Å. In the thirty-fifth C site, C(53) is bonded in a distorted single-bond geometry to one C(43), one C(51), and one N(9) atom. The C(53)-N(9) bond length is 1.40 Å. In the thirty-sixth C site, C(54) is bonded in a distorted single-bond geometry to one C(44), one C(52), and one N(10) atom. The C(54)-N(10) bond length is 1.39 Å. In the thirty-seventh C site, C(55) is bonded in a distorted trigonal planar geometry to one C(57), one N(11), and one N(9) atom. The C(55)-C(57) bond length is 1.48 Å. The C(55)-N(11) bond length is 1.37 Å. The C(55)-N(9) bond length is 1.34 Å. In the thirty-eighth C site, C(56) is bonded in a distorted trigonal planar geometry to one C(58), one N(10), and one N(12) atom. The C(56)-C(58) bond length is 1.49 Å. The C(56)-N(10) bond length is 1.34 Å. The C(56)-N(12) bond length is 1.37 Å. In the thirty-ninth C site, C(57) is bonded in a distorted trigonal non-coplanar geometry to one C(55), one H(61), one H(63), and one H(65) atom. The C(57)-H(61) bond length is 1.10 Å. The C(57)-H(63) bond length is 1.09 Å. The C(57)-H(65) bond length is 1.10 Å. In the fortieth C site, C(58) is bonded in a distorted trigonal non-coplanar geometry to one C(56), one H(62), one H(64), and one H(66) atom. The C(58)-H(62) bond length is 1.10 Å. The C(58)-H(64) bond length is 1.10 Å. The C(58)-H(66) bond length is 1.10 Å. In the forty-first C site, C(59) is bonded in a 3-coordinate geometry to one N(11), one H(67), and one H(69) atom. The C(59)-N(11) bond length is 1.46 Å. The C(59)-H(67) bond length is 1.10 Å. The C(59)-H(69) bond length is 1.10 Å. In the forty-second C site, C(60) is bonded in a distorted trigonal non-coplanar geometry to one N(12), one H(68), and one H(70) atom. The C(60)-N(12) bond length is 1.46 Å. The C(60)-H(68) bond length is 1.10 Å. The C(60)-H(70) bond length is 1.10 Å. In the forty-third C site, C(67) is bonded in a distorted trigonal non-coplanar geometry to one N(13), one H(83), and one H(85) atom. The C(67)-N(13) bond length is 1.46 Å. The C(67)-H(83) bond length is 1.10 Å. The C(67)-H(85) bond length is 1.10 Å. In the forty-fourth C site, C(68) is bonded in a distorted trigonal non-coplanar geometry to one N(14), one H(84), and one H(86) atom. The C(68)-N(14) bond length is 1.46 Å. The C(68)-H(84) bond length is 1.10 Å. The C(68)-H(86) bond length is 1.10 Å. In the forty-fifth C site, C(69) is bonded in a distorted trigonal non-coplanar geometry to one C(71), one H(87), one H(89), and one H(91) atom. The C(69)-C(71) bond length is 1.48 Å. The C(69)-H(87) bond length is 1.09 Å. The C(69)-H(89) bond length is 1.10 Å. The C(69)-H(91) bond length is 1.10 Å. In the forty-sixth C site, C(70) is bonded in a distorted trigonal non-coplanar geometry to one C(72), one H(88), one H(90), and one H(92) atom. The C(70)-C(72) bond length is 1.48 Å. The C(70)-H(88) bond length is 1.09 Å. The C(70)-H(90) bond length is 1.10 Å. The C(70)-H(92) bond length is 1.10 Å. In the forty-seventh C site, C(71) is bonded in a distorted trigonal planar geometry to one C(69), one N(13), and one N(15) atom. The C(71)-N(13) bond length is 1.38 Å. The C(71)-N(15) bond length is 1.34 Å. In the forty-eighth C site, C(72) is bonded in a distorted trigonal planar geometry to one C(70), one N(14), and one N(16) atom. The C(72)-N(14) bond length is 1.38 Å. The C(72)-N(16) bond length is 1.33 Å. In the forty-ninth C site, C(73) is bonded in a distorted single-bond geometry to one C(75), one C(83), and one N(13) atom. The C(73)-C(75) bond length is 1.40 Å. The C(73)-C(83) bond length is 1.42 Å. The C(73)-N(13) bond length is 1.39 Å. In the fiftieth C site, C(74) is bonded in a distorted single-bond geometry to one C(76), one C(84), and one N(14) atom. The C(74)-C(76) bond length is 1.40 Å. The C(74)-C(84) bond length is 1.42 Å. The C(74)-N(14) bond length is 1.39 Å. In the fifty-first C site, C(75) is bonded in a distorted single-bond geometry to one C(73) and one H(93) atom. The C(75)-H(93) bond length is 1.09 Å. In the fifty-second C site, C(76) is bonded in a distorted single-bond geometry to one C(74) and one H(94) atom. The C(76)-H(94) bond length is 1.09 Å. In the fifty-third C site, C(81) is bonded in a distorted single-bond geometry to one C(83) and one H(99) atom. The C(81)-C(83) bond length is 1.40 Å. The C(81)-H(99) bond length is 1.09 Å. In the fifty-fourth C site, C(82) is bonded in a distorted single-bond geometry to one C(84) and one H(100) atom. The C(82)-C(84) bond length is 1.40 Å. The C(82)-H(100) bond length is 1.09 Å. In the fifty-fifth C site, C(83) is bonded in a distorted single-bond geometry to one C(73), one C(81), and one N(15) atom. The C(83)-N(15) bond length is 1.39 Å. In the fifty-sixth C site, C(84) is bonded in a distorted trigonal planar geometry to one C(74), one C(82), and one N(16) atom. The C(84)-N(16) bond length is 1.39 Å. In the fifty-seventh C site, C(85) is bonded in a distorted bent 120 degrees geometry to one C(87), one O(1), and one O(3) atom. The C(85)-C(87) bond length is 1.51 Å. The C(85)-O(1) bond length is 1.27 Å. The C(85)-O(3) bond length is 1.28 Å. In the fifty-eighth C site, C(86) is bonded in a distorted bent 120 degrees geometry to one C(88), one O(2), and one O(4) atom. The C(86)-C(88) bond length is 1.51 Å. The C(86)-O(2) bond length is 1.29 Å. The C(86)-O(4) bond length is 1.26 Å. In the fifty-ninth C site, C(87) is bonded in a trigonal planar geometry to one C(85), one C(89), and one C(97) atom. The C(87)-C(89) bond length is 1.40 Å. The C(87)-C(97) bond length is 1.40 Å. In the sixtieth C site, C(88) is bonded in a trigonal planar geometry to one C(86), one C(90), and one C(98) atom. The C(88)-C(90) bond length is 1.40 Å. The C(88)-C(98) bond length is 1.41 Å. In the sixty-first C site, C(89) is bonded in a distorted single-bond geometry to one C(87) and one H(101) atom. The C(89)-H(101) bond length is 1.09 Å. In the sixty-second C site, C(90) is bonded in a distorted single-bond geometry to one C(88) and one H(102) atom. The C(90)-H(102) bond length is 1.09 Å. In the sixty-third C site, C(93) is bonded in a distorted single-bond geometry to one C(95) and one H(103) atom. The C(93)-C(95) bond length is 1.40 Å. The C(93)-H(103) bond length is 1.09 Å. In the sixty-fourth C site, C(94) is bonded in a distorted single-bond geometry to one C(96) and one H(104) atom. The C(94)-C(96) bond length is 1.40 Å. The C(94)-H(104) bond length is 1.09 Å. In the sixty-fifth C site, C(95) is bonded in a trigonal planar geometry to one C(93), one C(97), and one C(99) atom. The C(95)-C(97) bond length is 1.40 Å. The C(95)-C(99) bond length is 1.50 Å. In the sixty-sixth C site, C(96) is bonded in a trigonal planar geometry to one C(100), one C(94), and one C(98) atom. The C(96)-C(100) bond length is 1.50 Å. The C(96)-C(98) bond length is 1.40 Å. In the sixty-seventh C site, C(97) is bonded in a distorted trigonal planar geometry to one C(87), one C(95), and one H(105) atom. The C(97)-H(105) bond length is 1.09 Å. In the sixty-eighth C site, C(98) is bonded in a distorted trigonal planar geometry to one C(88), one C(96), and one H(106) atom. The C(98)-H(106) bond length is 1.09 Å. In the sixty-ninth C site, C(99) is bonded in a bent 120 degrees geometry to one C(95), one O(11), and one O(13) atom. The C(99)-O(11) bond length is 1.29 Å. The C(99)-O(13) bond length is 1.27 Å. In the seventieth C site, C(100) is bonded in a bent 120 degrees geometry to one C(96), one O(12), and one O(14) atom. The C(100)-O(12) bond length is 1.29 Å. The C(100)-O(14) bond length is 1.27 Å. In the seventy-first C site, C(105) is bonded in a distorted bent 120 degrees geometry to one C(107), one O(5), and one O(7) atom. The C(105)-C(107) bond length is 1.50 Å. The C(105)-O(5) bond length is 1.25 Å. The C(105)-O(7) bond length is 1.31 Å. In the seventy-second C site, C(106) is bonded in a bent 120 degrees geometry to one C(108), one O(6), and one O(8) atom. The C(106)-C(108) bond length is 1.49 Å. The C(106)-O(6) bond length is 1.28 Å. The C(106)-O(8) bond length is 1.28 Å. In the seventy-third C site, C(107) is bonded in a trigonal planar geometry to one C(105), one C(109), and one C(117) atom. The C(107)-C(109) bond length is 1.39 Å. The C(107)-C(117) bond length is 1.40 Å. In the seventy-fourth C site, C(108) is bonded in a trigonal planar geometry to one C(106), one C(110), and one C(118) atom. The C(108)-C(110) bond length is 1.39 Å. The C(108)-C(118) bond length is 1.40 Å. In the seventy-fifth C site, C(109) is bonded in a distorted trigonal planar geometry to one C(107), one C(111), and one H(115) atom. The C(109)-C(111) bond length is 1.39 Å. The C(109)-H(115) bond length is 1.09 Å. In the seventy-sixth C site, C(110) is bonded in a distorted single-bond geometry to one C(108) and one H(116) atom. The C(110)-H(116) bond length is 1.09 Å. In the seventy-seventh C site, C(111) is bonded in a distorted single-bond geometry to one C(109) and one O(21) atom. The C(111)-O(21) bond length is 1.35 Å. In the seventy-eighth C site, C(113) is bonded in a distorted single-bond geometry to one C(115) and one H(117) atom. The C(113)-C(115) bond length is 1.41 Å. The C(113)-H(117) bond length is 1.09 Å. In the seventy-ninth C site, C(114) is bonded in a distorted single-bond geometry to one C(116) and one H(118) atom. The C(114)-C(116) bond length is 1.40 Å. The C(114)-H(118) bond length is 1.09 Å. In the eightieth C site, C(115) is bonded in a trigonal planar geometry to one C(113), one C(117), and one C(119) atom. The C(115)-C(117) bond length is 1.40 Å. The C(115)-C(119) bond length is 1.49 Å. In the eighty-first C site, C(116) is bonded in a trigonal planar geometry to one C(114), one C(118), and one C(120) atom. The C(116)-C(118) bond length is 1.40 Å. The C(116)-C(120) bond length is 1.49 Å. In the eighty-second C site, C(117) is bonded in a distorted trigonal planar geometry to one C(107), one C(115), and one H(119) atom. The C(117)-H(119) bond length is 1.09 Å. In the eighty-third C site, C(118) is bonded in a distorted trigonal planar geometry to one C(108), one C(116), and one H(120) atom. The C(118)-H(120) bond length is 1.09 Å. In the eighty-fourth C site, C(119) is bonded in a distorted bent 120 degrees geometry to one C(115), one O(15), and one O(17) atom. The C(119)-O(15) bond length is 1.27 Å. The C(119)-O(17) bond length is 1.28 Å. In the eighty-fifth C site, C(120) is bonded in a distorted bent 120 degrees geometry to one C(116), one O(16), and one O(18) atom. The C(120)-O(16) bond length is 1.28 Å. The C(120)-O(18) bond length is 1.28 Å. In the eighty-sixth C site, C(121) is bonded in a distorted trigonal non-coplanar geometry to one H(121), one H(123), and one O(21) atom. The C(121)-H(121) bond length is 1.10 Å. The C(121)-H(123) bond length is 1.10 Å. The C(121)-O(21) bond length is 1.44 Å. There are sixteen inequivalent N sites. In the first N site, N(1) is bonded in a trigonal planar geometry to one Ni(1), one C(13), and one C(3) atom. In the second N site, N(2) is bonded in a trigonal planar geometry to one Ni(2), one C(14), and one C(4) atom. In the third N site, N(3) is bonded in a trigonal planar geometry to one C(13), one C(17), and one C(5) atom. In the fourth N site, N(4) is bonded in a trigonal planar geometry to one C(14), one C(18), and one C(6) atom. In the fifth N site, N(5) is bonded in a trigonal planar geometry to one C(25), one C(27), and one C(39) atom. In the sixth N site, N(6) is bonded in a trigonal planar geometry to one C(26), one C(28), and one C(40) atom. In the seventh N site, N(7) is bonded in a trigonal planar geometry to one Ni(3), one C(37), and one C(39) atom. In the eighth N site, N(8) is bonded in a trigonal planar geometry to one Ni(4), one C(38), and one C(40) atom. In the ninth N site, N(9) is bonded in a trigonal planar geometry to one Ni(1), one C(53), and one C(55) atom. In the tenth N site, N(10) is bonded in a trigonal planar geometry to one Ni(2), one C(54), and one C(56) atom. In the eleventh N site, N(11) is bonded in a trigonal planar geometry to one C(51), one C(55), and one C(59) atom. In the twelfth N site, N(12) is bonded in a trigonal planar geometry to one C(52), one C(56), and one C(60) atom. In the thirteenth N site, N(13) is bonded in a trigonal planar geometry to one C(67), one C(71), and one C(73) atom. In the fourteenth N site, N(14) is bonded in a trigonal planar geometry to one C(68), one C(72), and one C(74) atom. In the fifteenth N site, N(15) is bonded in a trigonal planar geometry to one Ni(4), one C(71), and one C(83) atom. In the sixteenth N site, N(16) is bonded in a trigonal planar geometry to one Ni(3), one C(72), and one C(84) atom. There are seventy-three inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one O(4) and one O(9) atom. The H(1)-O(4) bond length is 1.67 Å. The H(1)-O(9) bond length is 1.00 Å. In the second H site, H(2) is bonded in a linear geometry to one O(10) and one O(3) atom. The H(2)-O(10) bond length is 1.06 Å. The H(2)-O(3) bond length is 1.48 Å. In the third H site, H(3) is bonded in a single-bond geometry to one O(9) atom. The H(3)-O(9) bond length is 0.97 Å. In the fourth H site, H(4) is bonded in a single-bond geometry to one O(10) atom. The H(4)-O(10) bond length is 0.97 Å. In the fifth H site, H(5) is bonded in a single-bond geometry to one C(1) atom. In the sixth H site, H(6) is bonded in a single-bond geometry to one C(2) atom. In the seventh H site, H(7) is bonded in a single-bond geometry to one C(7) atom. In the eighth H site, H(8) is bonded in a single-bond geometry to one C(8) atom. In the ninth H site, H(13) is bonded in a single-bond geometry to one C(15) atom. In the tenth H site, H(14) is bonded in a single-bond geometry to one C(16) atom. In the eleventh H site, H(15) is bonded in a single-bond geometry to one C(15) atom. In the twelfth H site, H(16) is bonded in a single-bond geometry to one C(16) atom. In the thirteenth H site, H(17) is bonded in a single-bond geometry to one C(15) atom. In the fourteenth H site, H(18) is bonded in a single-bond geometry to one C(16) atom. In the fifteenth H site, H(19) is bonded in a single-bond geometry to one C(17) atom. In the sixteenth H site, H(20) is bonded in a single-bond geometry to one C(18) atom. In the seventeenth H site, H(21,22) is bonded in a single-bond geometry to one C(17) atom. In the eighteenth H site, H(35) is bonded in a single-bond geometry to one C(25) atom. In the nineteenth H site, H(36) is bonded in a single-bond geometry to one C(26) atom. In the twentieth H site, H(37) is bonded in a single-bond geometry to one C(25) atom. In the twenty-first H site, H(38) is bonded in a single-bond geometry to one C(26) atom. In the twenty-second H site, H(39) is bonded in a single-bond geometry to one C(29) atom. In the twenty-third H site, H(40) is bonded in a single-bond geometry to one C(30) atom. In the twenty-fourth H site, H(45) is bonded in a single-bond geometry to one C(35) atom. In the twenty-fifth H site, H(46) is bonded in a single-bond geometry to one C(36) atom. In the twenty-sixth H site, H(47) is bonded in a single-bond geometry to one C(41) atom. In the twenty-seventh H site, H(48) is bonded in a single-bond geometry to one C(42) atom. In the twenty-eighth H site, H(49) is bonded in a single-bond geometry to one C(41) atom. In the twenty-ninth H site, H(50) is bonded in a single-bond geometry to one C(42) atom. In the thirtieth H site, H(51) is bonded in a single-bond geometry to one C(41) atom. In the thirty-first H site, H(52) is bonded in a single-bond geometry to one C(42) atom. In the thirty-second H site, H(53) is bonded in a single-bond geometry to one C(43) atom. In the thirty-third H site, H(54) is bonded in a single-bond geometry to one C(44) atom. In the thirty-fourth H site, H(59) is bonded in a single-bond geometry to one C(49) atom. In the thirty-fifth H site, H(60) is bonded in a single-bond geometry to one C(50) atom. In the thirty-sixth H site, H(61) is bonded in a single-bond geometry to one C(57) atom. In the thirty-seventh H site, H(62) is bonded in a single-bond geometry to one C(58) atom. In the thirty-eighth H site, H(63) is bonded in a single-bond geometry to one C(57) atom. In the thirty-ninth H site, H(64) is bonded in a single-bond geometry to one C(58) atom. In the fortieth H site, H(65) is bonded in a single-bond geometry to one C(57) atom. In the forty-first H site, H(66) is bonded in a single-bond geometry to one C(58) atom. In the forty-second H site, H(67) is bonded in a single-bond geometry to one C(59) atom. In the forty-third H site, H(68) is bonded in a single-bond geometry to one C(60) atom. In the forty-fourth H site, H(69) is bonded in a single-bond geometry to one C(59) atom. In the forty-fifth H site, H(70) is bonded in a single-bond geometry to one C(60) atom. In the forty-sixth H site, H(83) is bonded in a single-bond geometry to one C(67) atom. In the forty-seventh H site, H(84) is bonded in a single-bond geometry to one C(68) atom. In the forty-eighth H site, H(85) is bonded in a single-bond geometry to one C(67) atom. In the forty-ninth H site, H(86) is bonded in a single-bond geometry to one C(68) atom. In the fiftieth H site, H(87) is bonded in a single-bond geometry to one C(69) atom. In the fifty-first H site, H(88) is bonded in a single-bond geometry to one C(70) atom. In the fifty-second H site, H(89) is bonded in a single-bond geometry to one C(69) atom. In the fifty-third H site, H(90) is bonded in a single-bond geometry to one C(70) atom. In the fifty-fourth H site, H(91) is bonded in a single-bond geometry to one C(69) atom. In the fifty-fifth H site, H(92) is bonded in a single-bond geometry to one C(70) atom. In the fifty-sixth H site, H(93) is bonded in a single-bond geometry to one C(75) atom. In the fifty-seventh H site, H(94) is bonded in a single-bond geometry to one C(76) atom. In the fifty-eighth H site, H(99) is bonded in a single-bond geometry to one C(81) atom. In the fifty-ninth H site, H(100) is bonded in a single-bond geometry to one C(82) atom. In the sixtieth H site, H(101) is bonded in a single-bond geometry to one C(89) atom. In the sixty-first H site, H(102) is bonded in a single-bond geometry to one C(90) atom. In the sixty-second H site, H(103) is bonded in a single-bond geometry to one C(93) atom. In the sixty-third H site, H(104) is bonded in a single-bond geometry to one C(94) atom. In the sixty-fourth H site, H(105) is bonded in a single-bond geometry to one C(97) atom. In the sixty-fifth H site, H(106) is bonded in a single-bond geometry to one C(98) atom. In the sixty-sixth H site, H(115) is bonded in a single-bond geometry to one C(109) atom. In the sixty-seventh H site, H(116) is bonded in a single-bond geometry to one C(110) atom. In the sixty-eighth H site, H(117) is bonded in a single-bond geometry to one C(113) atom. In the sixty-ninth H site, H(118) is bonded in a single-bond geometry to one C(114) atom. In the seventieth H site, H(119) is bonded in a single-bond geometry to one C(117) atom. In the seventy-first H site, H(120) is bonded in a single-bond geometry to one C(118) atom. In the seventy-second H site, H(121) is bonded in a single-bond geometry to one C(121) atom. In the seventy-third H site, H(123) is bonded in a single-bond geometry to one C(121) atom. There are nineteen inequivalent O sites. In the first O site, O(1) is bonded in a bent 120 degrees geometry to one Ni(2) and one C(85) atom. In the second O site, O(2) is bonded in a bent 120 degrees geometry to one Ni(1) and one C(86) atom. In the third O site, O(3) is bonded in a water-like geometry to one C(85) and one H(2) atom. In the fourth O site, O(4) is bonded in a distorted bent 120 degrees geometry to one C(86) and one H(1) atom. In the fifth O site, O(5) is bonded in a single-bond geometry to one C(105) atom. In the sixth O site, O(6) is bonded in an L-shaped geometry to one Ni(2) and one C(106) atom. In the seventh O site, O(7) is bonded in a water-like geometry to one Ni(1) and one C(105) atom. In the eighth O site, O(8) is bonded in an L-shaped geometry to one Ni(2) and one C(106) atom. In the ninth O site, O(9) is bonded in a water-like geometry to one H(1) and one H(3) atom. In the tenth O site, O(10) is bonded in a distorted water-like geometry to one Ni(2), one H(2), and one H(4) atom. In the eleventh O site, O(11) is bonded in an L-shaped geometry to one Ni(3) and one C(99) atom. In the twelfth O site, O(12) is bonded in an L-shaped geometry to one Ni(4) and one C(100) atom. In the thirteenth O site, O(13) is bonded in a distorted L-shaped geometry to one Ni(3) and one C(99) atom. In the fourteenth O site, O(14) is bonded in a distorted L-shaped geometry to one Ni(4) and one C(100) atom. In the fifteenth O site, O(15) is bonded in a distorted L-shaped geometry to one Ni(3) and one C(119) atom. In the sixteenth O site, O(16) is bonded in an L-shaped geometry to one Ni(4) and one C(120) atom. In the seventeenth O site, O(17) is bonded in an L-shaped geometry to one Ni(3) and one C(119) atom. In the eighteenth O site, O(18) is bonded in a distorted L-shaped geometry to one Ni(4) and one C(120) atom. In the nineteenth O site, O(21) is bonded in a bent 120 degrees geometry to one C(111) and one C(121) atom. Linkers: 1 [CH2].[CH2].[CH2].[CH2].[CH2].[CH2].[CH2].[CH2].[CH2].[CH2].[CH2][N].[CH2][O].[CH3].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH].[CH]=[CH].[CH][CH2].[CH][N].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].[C].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Metal clusters: 1 O.O=[C]O[Ni]1O[C]O1. The MOF has largest included sphere 5.03 A, density 1.27 g/cm3, surface area 4978.22 m2/g, accessible volume 0.25 cm3/g