(CH2)2CHPb2C13PNH11O11 crystallizes in the triclinic P-1 space group. The structure consists of two 02329_fluka molecules and four 02329_fluka molecules inside a Pb2C13PNH11O11 framework. In the Pb2C13PNH11O11 framework, there are two inequivalent Pb sites. In the first Pb site, Pb(1) is bonded in a 7-coordinate geometry to one O(1), one O(10), one O(5), one O(6), one O(7), one O(8), and one O(9) atom. The Pb(1)-O(1) bond length is 2.42 Å. The Pb(1)-O(10) bond length is 2.84 Å. The Pb(1)-O(5) bond length is 2.74 Å. The Pb(1)-O(6) bond length is 2.69 Å. The Pb(1)-O(7) bond length is 2.49 Å. The Pb(1)-O(8) bond length is 2.76 Å. The Pb(1)-O(9) bond length is 2.51 Å. In the second Pb site, Pb(2) is bonded in a 5-coordinate geometry to one O(2), one O(3), one O(4), one O(5), and one O(7) atom. The Pb(2)-O(2) bond length is 2.45 Å. The Pb(2)-O(3) bond length is 2.41 Å. The Pb(2)-O(4) bond length is 2.40 Å. The Pb(2)-O(5) bond length is 2.67 Å. The Pb(2)-O(7) bond length is 2.71 Å. There are thirteen inequivalent C sites. In the first C site, C(1) is bonded in a distorted tetrahedral geometry to one P(1), one N(1), one H(3), and one H(4) atom. The C(1)-P(1) bond length is 1.85 Å. The C(1)-N(1) bond length is 1.50 Å. The C(1)-H(3) bond length is 1.10 Å. The C(1)-H(4) bond length is 1.10 Å. In the second C site, C(2) is bonded in a 3-coordinate geometry to one N(1), one H(5), and one H(6) atom. The C(2)-N(1) bond length is 1.51 Å. The C(2)-H(5) bond length is 1.10 Å. The C(2)-H(6) bond length is 1.10 Å. In the third C site, C(6) is bonded in a 3-coordinate geometry to one N(1), one H(12), and one H(13) atom. The C(6)-N(1) bond length is 1.51 Å. The C(6)-H(12) bond length is 1.10 Å. The C(6)-H(13) bond length is 1.10 Å. In the fourth C site, C(7) is bonded in a distorted bent 120 degrees geometry to one O(4) and one O(5) atom. The C(7)-O(4) bond length is 1.28 Å. The C(7)-O(5) bond length is 1.27 Å. In the fifth C site, C(8) is bonded in a trigonal planar geometry to one C(13), one C(14), and one C(9) atom. The C(8)-C(13) bond length is 1.40 Å. The C(8)-C(14) bond length is 1.49 Å. The C(8)-C(9) bond length is 1.40 Å. In the sixth C site, C(9) is bonded in a distorted single-bond geometry to one C(10), one C(8), and one H(14) atom. The C(9)-C(10) bond length is 1.40 Å. The C(9)-H(14) bond length is 1.09 Å. In the seventh C site, C(10) is bonded in a trigonal planar geometry to one C(11), one C(15), and one C(9) atom. The C(10)-C(11) bond length is 1.40 Å. The C(10)-C(15) bond length is 1.50 Å. In the eighth C site, C(11) is bonded in a distorted single-bond geometry to one C(10), one C(12), and one H(15) atom. The C(11)-C(12) bond length is 1.40 Å. The C(11)-H(15) bond length is 1.09 Å. In the ninth C site, C(12) is bonded in a trigonal planar geometry to one C(11), one C(13), and one C(16) atom. The C(12)-C(13) bond length is 1.40 Å. The C(12)-C(16) bond length is 1.49 Å. In the tenth C site, C(13) is bonded in a distorted single-bond geometry to one C(12), one C(8), and one H(16) atom. The C(13)-H(16) bond length is 1.09 Å. In the eleventh C site, C(14) is bonded in a distorted bent 120 degrees geometry to one C(8), one O(6), and one O(7) atom. The C(14)-O(6) bond length is 1.28 Å. The C(14)-O(7) bond length is 1.27 Å. In the twelfth C site, C(15) is bonded in a distorted bent 120 degrees geometry to one C(10), one O(8), and one O(9) atom. The C(15)-O(8) bond length is 1.28 Å. The C(15)-O(9) bond length is 1.27 Å. In the thirteenth C site, C(16) is bonded in a distorted bent 120 degrees geometry to one C(12), one O(10), and one O(11) atom. The C(16)-O(10) bond length is 1.24 Å. The C(16)-O(11) bond length is 1.33 Å. P(1) is bonded to one C(1), one O(1), one O(2), and one O(3) atom to form PCO3 tetrahedra that share  a cornercorner with one N(1)HC3 tetrahedra. The P(1)-O(1) bond length is 1.54 Å. The P(1)-O(2) bond length is 1.53 Å. The P(1)-O(3) bond length is 1.54 Å. N(1) is bonded to one C(1), one C(2), one C(6), and one H(2) atom to form NHC3 tetrahedra that share  a cornercorner with one P(1)CO3 tetrahedra. The N(1)-H(2) bond length is 1.07 Å. There are eleven inequivalent H sites. In the first H site, H(1) is bonded in a linear geometry to one O(11) and one O(8) atom. The H(1)-O(11) bond length is 1.02 Å. The H(1)-O(8) bond length is 1.58 Å. In the second H site, H(2) is bonded in a distorted single-bond geometry to one N(1) and one O(6) atom. The H(2)-O(6) bond length is 1.64 Å. In the third H site, H(3) is bonded in a single-bond geometry to one C(1) atom. In the fourth H site, H(4) is bonded in a single-bond geometry to one C(1) atom. In the fifth H site, H(5) is bonded in a single-bond geometry to one C(2) atom. In the sixth H site, H(6) is bonded in a single-bond geometry to one C(2) atom. In the seventh H site, H(12) is bonded in a single-bond geometry to one C(6) atom. In the eighth H site, H(13) is bonded in a single-bond geometry to one C(6) atom. In the ninth H site, H(14) is bonded in a single-bond geometry to one C(9) atom. In the tenth H site, H(15) is bonded in a single-bond geometry to one C(11) atom. In the eleventh H site, H(16) is bonded in a single-bond geometry to one C(13) atom. There are eleven inequivalent O sites. In the first O site, O(1) is bonded in a distorted single-bond geometry to one Pb(1) and one P(1) atom. In the second O site, O(2) is bonded in a distorted single-bond geometry to one Pb(2) and one P(1) atom. In the third O site, O(3) is bonded in a distorted bent 120 degrees geometry to one Pb(2) and one P(1) atom. In the fourth O site, O(4) is bonded in a distorted single-bond geometry to one Pb(2) and one C(7) atom. In the fifth O site, O(5) is bonded in a single-bond geometry to one Pb(1), one Pb(2), and one C(7) atom. In the sixth O site, O(6) is bonded in a 2-coordinate geometry to one Pb(1), one C(14), and one H(2) atom. In the seventh O site, O(7) is bonded in a distorted single-bond geometry to one Pb(1), one Pb(2), and one C(14) atom. In the eighth O site, O(8) is bonded in a distorted linear geometry to one Pb(1), one C(15), and one H(1) atom. In the ninth O site, O(9) is bonded in a distorted single-bond geometry to one Pb(1) and one C(15) atom. In the tenth O site, O(10) is bonded in a single-bond geometry to one Pb(1) and one C(16) atom. In the eleventh O site, O(11) is bonded in a water-like geometry to one C(16) and one H(1) atom. Linkers: 2 [O]C(=O)C1CC[NH](CC1)CP(=O)([O])[O] ,2 [O]C(=O)c1cc(C([O])=O)cc(C(=O)O)c1. Metal clusters: 4 [Pb]. The MOF has largest included sphere 2.63 A, density 2.78 g/cm3, surface area 2322.27 m2/g, accessible volume 0.07 cm3/g