FeAu2H12(C10N3)2(C5H3)3CH crystallizes in the triclinic P1 space group. The structure consists of four 02329_fluka molecules; four 1,9-dimethyl-9bh-phenalene molecules; and two FeAu2H12(C10N3)2 frameworks. In one of the FeAu2H12(C10N3)2 frameworks, there are two inequivalent Fe sites. In the first Fe site, Fe(1) is bonded in an octahedral geometry to one N(1), one N(12), one N(3), one N(6), one N(7), and one N(9) atom. The Fe(1)-N(1) bond length is 2.11 Å. The Fe(1)-N(12) bond length is 2.20 Å. The Fe(1)-N(3) bond length is 2.20 Å. The Fe(1)-N(6) bond length is 2.10 Å. The Fe(1)-N(7) bond length is 2.09 Å. The Fe(1)-N(9) bond length is 2.09 Å. In the second Fe site, Fe(2) is bonded in an octahedral geometry to one N(10), one N(11), one N(2), one N(4), one N(5), and one N(8) atom. The Fe(2)-N(10) bond length is 2.09 Å. The Fe(2)-N(11) bond length is 2.20 Å. The Fe(2)-N(2) bond length is 2.11 Å. The Fe(2)-N(4) bond length is 2.20 Å. The Fe(2)-N(5) bond length is 2.10 Å. The Fe(2)-N(8) bond length is 2.09 Å. There are four inequivalent Au sites. In the first Au site, Au(1) is bonded in a linear geometry to one C(1) and one C(3) atom. The Au(1)-C(1) bond length is 1.97 Å. The Au(1)-C(3) bond length is 1.97 Å. In the second Au site, Au(2) is bonded in a linear geometry to one C(2) and one C(4) atom. The Au(2)-C(2) bond length is 1.97 Å. The Au(2)-C(4) bond length is 1.97 Å. In the third Au site, Au(3) is bonded in a distorted linear geometry to one C(17,18) and one C(9,10) atom. The Au(3)-C(17,18) bond length is 1.97 Å. The Au(3)-C(9,10) bond length is 1.97 Å. In the fourth Au site, Au(4) is bonded in a distorted linear geometry to one C(17,18) and one C(9,10) atom. The Au(4)-C(17,18) bond length is 1.97 Å. The Au(4)-C(9,10) bond length is 1.97 Å. There are thirty-one inequivalent C sites. In the first C site, C(29) is bonded in a trigonal planar geometry to one C(25,26); one C(27,28); and one C(31,32) atom. The C(29)-C(25,26) bond length is 1.41 Å. The C(29)-C(27,28) bond length is 1.41 Å. The C(29)-C(31,32) bond length is 1.48 Å. In the second C site, C(30) is bonded in a trigonal planar geometry to one C(25,26); one C(27,28); and one C(31,32) atom. The C(30)-C(25,26) bond length is 1.41 Å. The C(30)-C(27,28) bond length is 1.41 Å. The C(30)-C(31,32) bond length is 1.48 Å. In the third C site, C(31,32) is bonded in a trigonal planar geometry to one C(29); one C(33,34); and one C(35,36) atom. The C(31,32)-C(33,34) bond length is 1.41 Å. The C(31,32)-C(35,36) bond length is 1.41 Å. In the fourth C site, C(33,34) is bonded in a distorted trigonal planar geometry to one C(31,32); one C(37); and one H(17,18) atom. The C(33,34)-C(37) bond length is 1.39 Å. The C(33,34)-H(17,18) bond length is 1.09 Å. In the fifth C site, C(35,36) is bonded in a distorted single-bond geometry to one C(31,32); one C(39); and one H(19,20) atom. The C(35,36)-C(39) bond length is 1.39 Å. The C(35,36)-H(19,20) bond length is 1.09 Å. In the sixth C site, C(37) is bonded in a distorted bent 120 degrees geometry to one C(33,34); one N(11); and one H(21,22) atom. The C(37)-N(11) bond length is 1.35 Å. The C(37)-H(21,22) bond length is 1.09 Å. In the seventh C site, C(38) is bonded in a distorted bent 120 degrees geometry to one C(33,34); one N(12); and one H(21,22) atom. The C(38)-C(33,34) bond length is 1.39 Å. The C(38)-N(12) bond length is 1.35 Å. The C(38)-H(21,22) bond length is 1.09 Å. In the eighth C site, C(39) is bonded in a distorted trigonal planar geometry to one C(35,36); one N(11); and one H(23,24) atom. The C(39)-N(11) bond length is 1.35 Å. The C(39)-H(23,24) bond length is 1.09 Å. In the ninth C site, C(40) is bonded in a distorted trigonal planar geometry to one C(35,36); one N(12); and one H(23,24) atom. The C(40)-C(35,36) bond length is 1.39 Å. The C(40)-N(12) bond length is 1.35 Å. The C(40)-H(23,24) bond length is 1.09 Å. In the tenth C site, C(1) is bonded in a single-bond geometry to one Au(1) and one N(1) atom. The C(1)-N(1) bond length is 1.17 Å. In the eleventh C site, C(2) is bonded in a single-bond geometry to one Au(2) and one N(2) atom. The C(2)-N(2) bond length is 1.17 Å. In the twelfth C site, C(3) is bonded in a single-bond geometry to one Au(1) and one N(5) atom. The C(3)-N(5) bond length is 1.17 Å. In the thirteenth C site, C(4) is bonded in a single-bond geometry to one Au(2) and one N(6) atom. The C(4)-N(6) bond length is 1.17 Å. In the fourteenth C site, C(5,6) is bonded in a distorted trigonal planar geometry to one C(11), one N(3), and one H(1) atom. The C(5,6)-C(11) bond length is 1.39 Å. The C(5,6)-N(3) bond length is 1.35 Å. The C(5,6)-H(1) bond length is 1.09 Å. In the fifteenth C site, C(7,8) is bonded in a distorted trigonal planar geometry to one C(13); one N(3); and one H(3,4) atom. The C(7,8)-C(13) bond length is 1.39 Å. The C(7,8)-N(3) bond length is 1.35 Å. The C(7,8)-H(3,4) bond length is 1.09 Å. In the sixteenth C site, C(9,10) is bonded in a single-bond geometry to one Au(3) and one N(7) atom. The C(9,10)-N(7) bond length is 1.17 Å. In the seventeenth C site, C(11) is bonded in a distorted single-bond geometry to one C(15); one C(5,6); and one H(5,6) atom. The C(11)-C(15) bond length is 1.41 Å. The C(11)-H(5,6) bond length is 1.09 Å. In the eighteenth C site, C(12) is bonded in a distorted single-bond geometry to one C(16); one C(5,6); and one H(5,6) atom. The C(12)-C(16) bond length is 1.41 Å. The C(12)-C(5,6) bond length is 1.39 Å. The C(12)-H(5,6) bond length is 1.09 Å. In the nineteenth C site, C(13) is bonded in a distorted single-bond geometry to one C(15); one C(7,8); and one H(7,8) atom. The C(13)-C(15) bond length is 1.41 Å. The C(13)-H(7,8) bond length is 1.09 Å. In the twentieth C site, C(14) is bonded in a distorted single-bond geometry to one C(16); one C(7,8); and one H(7,8) atom. The C(14)-C(16) bond length is 1.41 Å. The C(14)-C(7,8) bond length is 1.39 Å. The C(14)-H(7,8) bond length is 1.09 Å. In the twenty-first C site, C(15) is bonded in a trigonal planar geometry to one C(11), one C(13), and one C(19) atom. The C(15)-C(19) bond length is 1.47 Å. In the twenty-second C site, C(16) is bonded in a trigonal planar geometry to one C(12), one C(14), and one C(20) atom. The C(16)-C(20) bond length is 1.47 Å. In the twenty-third C site, C(17,18) is bonded in a distorted single-bond geometry to one Au(4) and one N(9) atom. The C(17,18)-N(9) bond length is 1.17 Å. In the twenty-fourth C site, C(19) is bonded in a trigonal planar geometry to one C(15), one C(21), and one C(23) atom. The C(19)-C(21) bond length is 1.41 Å. The C(19)-C(23) bond length is 1.41 Å. In the twenty-fifth C site, C(20) is bonded in a trigonal planar geometry to one C(16), one C(22), and one C(24) atom. The C(20)-C(22) bond length is 1.41 Å. The C(20)-C(24) bond length is 1.41 Å. In the twenty-sixth C site, C(21) is bonded in a distorted trigonal planar geometry to one C(19); one C(25,26); and one H(9,10) atom. The C(21)-C(25,26) bond length is 1.39 Å. The C(21)-H(9,10) bond length is 1.09 Å. In the twenty-seventh C site, C(22) is bonded in a distorted trigonal planar geometry to one C(20); one C(25,26); and one H(9,10) atom. The C(22)-C(25,26) bond length is 1.39 Å. The C(22)-H(9,10) bond length is 1.09 Å. In the twenty-eighth C site, C(23) is bonded in a distorted trigonal planar geometry to one C(19); one C(27,28); and one H(11,12) atom. The C(23)-C(27,28) bond length is 1.39 Å. The C(23)-H(11,12) bond length is 1.09 Å. In the twenty-ninth C site, C(24) is bonded in a distorted trigonal planar geometry to one C(20); one C(27,28); and one H(11,12) atom. The C(24)-C(27,28) bond length is 1.39 Å. The C(24)-H(11,12) bond length is 1.09 Å. In the thirtieth C site, C(25,26) is bonded in a distorted single-bond geometry to one C(21); one C(29); and one H(13,14) atom. The C(25,26)-H(13,14) bond length is 1.09 Å. In the thirty-first C site, C(27,28) is bonded in a distorted trigonal planar geometry to one C(23), one C(29), and one H(15) atom. The C(27,28)-H(15) bond length is 1.09 Å. There are twelve inequivalent N sites. In the first N site, N(12) is bonded in a trigonal planar geometry to one Fe(1), one C(38), and one C(40) atom. In the second N site, N(8) is bonded in a linear geometry to one Fe(2) and one C(9,10) atom. The N(8)-C(9,10) bond length is 1.17 Å. In the third N site, N(9) is bonded in a linear geometry to one Fe(1) and one C(17,18) atom. In the fourth N site, N(11) is bonded in a trigonal planar geometry to one Fe(2), one C(37), and one C(39) atom. In the fifth N site, N(4) is bonded in a trigonal planar geometry to one Fe(2); one C(5,6); and one C(7,8) atom. The N(4)-C(5,6) bond length is 1.35 Å. The N(4)-C(7,8) bond length is 1.35 Å. In the sixth N site, N(5) is bonded in a linear geometry to one Fe(2) and one C(3) atom. In the seventh N site, N(10) is bonded in a linear geometry to one Fe(2) and one C(17,18) atom. The N(10)-C(17,18) bond length is 1.17 Å. In the eighth N site, N(6) is bonded in a linear geometry to one Fe(1) and one C(4) atom. In the ninth N site, N(7) is bonded in a linear geometry to one Fe(1) and one C(9,10) atom. In the tenth N site, N(1) is bonded in a linear geometry to one Fe(1) and one C(1) atom. In the eleventh N site, N(2) is bonded in a linear geometry to one Fe(2) and one C(2) atom. In the twelfth N site, N(3) is bonded in a trigonal planar geometry to one Fe(1); one C(5,6); and one C(7,8) atom. There are fourteen inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one C(5,6) atom. In the second H site, H(2) is bonded in a single-bond geometry to one C(5,6) atom. The H(2)-C(5,6) bond length is 1.09 Å. In the third H site, H(3,4) is bonded in a single-bond geometry to one C(7,8) atom. In the fourth H site, H(5,6) is bonded in a single-bond geometry to one C(11) atom. In the fifth H site, H(7,8) is bonded in a single-bond geometry to one C(13) atom. In the sixth H site, H(9,10) is bonded in a single-bond geometry to one C(21) atom. In the seventh H site, H(11,12) is bonded in a single-bond geometry to one C(23) atom. In the eighth H site, H(13,14) is bonded in a single-bond geometry to one C(25,26) atom. In the ninth H site, H(15) is bonded in a single-bond geometry to one C(27,28) atom. In the tenth H site, H(16) is bonded in a single-bond geometry to one C(27,28) atom. The H(16)-C(27,28) bond length is 1.09 Å. In the eleventh H site, H(17,18) is bonded in a single-bond geometry to one C(33,34) atom. In the twelfth H site, H(19,20) is bonded in a single-bond geometry to one C(35,36) atom. In the thirteenth H site, H(21,22) is bonded in a single-bond geometry to one C(37) atom. In the fourteenth H site, H(23,24) is bonded in a single-bond geometry to one C(39) atom. In one of the FeAu2H12(C10N3)2 frameworks, there are two inequivalent Fe sites. In the first Fe site, Fe(3) is bonded in an octahedral geometry to one N(13), one N(16), one N(17), one N(19), one N(21), and one N(24) atom. The Fe(3)-N(13) bond length is 2.08 Å. The Fe(3)-N(16) bond length is 2.07 Å. The Fe(3)-N(17) bond length is 2.07 Å. The Fe(3)-N(19) bond length is 2.09 Å. The Fe(3)-N(21) bond length is 2.17 Å. The Fe(3)-N(24) bond length is 2.16 Å. In the second Fe site, Fe(4) is bonded in an octahedral geometry to one N(14), one N(15), one N(18), one N(20), one N(22), and one N(23) atom. The Fe(4)-N(14) bond length is 2.08 Å. The Fe(4)-N(15) bond length is 2.07 Å. The Fe(4)-N(18) bond length is 2.08 Å. The Fe(4)-N(20) bond length is 2.09 Å. The Fe(4)-N(22) bond length is 2.15 Å. The Fe(4)-N(23) bond length is 2.15 Å. There are four inequivalent Au sites. In the first Au site, Au(5) is bonded in a distorted linear geometry to one C(41) and one C(43) atom. The Au(5)-C(41) bond length is 1.96 Å. The Au(5)-C(43) bond length is 1.96 Å. In the second Au site, Au(6) is bonded in a linear geometry to one C(42) and one C(44) atom. The Au(6)-C(42) bond length is 1.96 Å. The Au(6)-C(44) bond length is 1.96 Å. In the third Au site, Au(7) is bonded in a linear geometry to one C(45) and one C(56) atom. The Au(7)-C(45) bond length is 1.96 Å. The Au(7)-C(56) bond length is 1.96 Å. In the fourth Au site, Au(8) is bonded in a linear geometry to one C(46) and one C(55) atom. The Au(8)-C(46) bond length is 1.96 Å. The Au(8)-C(55) bond length is 1.96 Å. There are thirty-nine inequivalent C sites. In the first C site, C(41) is bonded in a distorted single-bond geometry to one Au(5) and one N(13) atom. The C(41)-N(13) bond length is 1.17 Å. In the second C site, C(42) is bonded in a distorted single-bond geometry to one Au(6) and one N(14) atom. The C(42)-N(14) bond length is 1.17 Å. In the third C site, C(43) is bonded in a distorted single-bond geometry to one Au(5) and one N(15) atom. The C(43)-N(15) bond length is 1.17 Å. In the fourth C site, C(44) is bonded in a distorted single-bond geometry to one Au(6) and one N(16) atom. The C(44)-N(16) bond length is 1.17 Å. In the fifth C site, C(45) is bonded in a distorted single-bond geometry to one Au(7) and one N(17) atom. The C(45)-N(17) bond length is 1.17 Å. In the sixth C site, C(46) is bonded in a distorted single-bond geometry to one Au(8) and one N(18) atom. The C(46)-N(18) bond length is 1.17 Å. In the seventh C site, C(47) is bonded in a distorted trigonal planar geometry to one C(51), one N(21), and one H(25) atom. The C(47)-C(51) bond length is 1.38 Å. The C(47)-N(21) bond length is 1.34 Å. The C(47)-H(25) bond length is 1.09 Å. In the eighth C site, C(48) is bonded in a distorted trigonal planar geometry to one C(52), one N(22), and one H(26) atom. The C(48)-C(52) bond length is 1.38 Å. The C(48)-N(22) bond length is 1.35 Å. The C(48)-H(26) bond length is 1.09 Å. In the ninth C site, C(49) is bonded in a distorted trigonal planar geometry to one C(53), one N(21), and one H(27) atom. The C(49)-C(53) bond length is 1.39 Å. The C(49)-N(21) bond length is 1.35 Å. The C(49)-H(27) bond length is 1.09 Å. In the tenth C site, C(50) is bonded in a distorted trigonal planar geometry to one C(54), one N(22), and one H(28) atom. The C(50)-C(54) bond length is 1.39 Å. The C(50)-N(22) bond length is 1.35 Å. The C(50)-H(28) bond length is 1.09 Å. In the eleventh C site, C(51) is bonded in a distorted single-bond geometry to one C(47), one C(57), and one H(29) atom. The C(51)-C(57) bond length is 1.41 Å. The C(51)-H(29) bond length is 1.09 Å. In the twelfth C site, C(52) is bonded in a distorted single-bond geometry to one C(48), one C(58), and one H(30) atom. The C(52)-C(58) bond length is 1.41 Å. The C(52)-H(30) bond length is 1.09 Å. In the thirteenth C site, C(53) is bonded in a distorted single-bond geometry to one C(49), one C(57), and one H(31) atom. The C(53)-C(57) bond length is 1.41 Å. The C(53)-H(31) bond length is 1.09 Å. In the fourteenth C site, C(54) is bonded in a distorted single-bond geometry to one C(50), one C(58), and one H(32) atom. The C(54)-C(58) bond length is 1.41 Å. The C(54)-H(32) bond length is 1.09 Å. In the fifteenth C site, C(55) is bonded in a distorted single-bond geometry to one Au(8) and one N(19) atom. The C(55)-N(19) bond length is 1.17 Å. In the sixteenth C site, C(56) is bonded in a distorted single-bond geometry to one Au(7) and one N(20) atom. The C(56)-N(20) bond length is 1.17 Å. In the seventeenth C site, C(57) is bonded in a trigonal planar geometry to one C(51), one C(53), and one C(59) atom. The C(57)-C(59) bond length is 1.47 Å. In the eighteenth C site, C(58) is bonded in a trigonal planar geometry to one C(52), one C(54), and one C(60) atom. The C(58)-C(60) bond length is 1.47 Å. In the nineteenth C site, C(59) is bonded in a trigonal planar geometry to one C(57), one C(61), and one C(63) atom. The C(59)-C(61) bond length is 1.41 Å. The C(59)-C(63) bond length is 1.41 Å. In the twentieth C site, C(60) is bonded in a trigonal planar geometry to one C(58), one C(62), and one C(64) atom. The C(60)-C(62) bond length is 1.41 Å. The C(60)-C(64) bond length is 1.41 Å. In the twenty-first C site, C(61) is bonded in a distorted trigonal planar geometry to one C(59); one C(65); and one H(33,34) atom. The C(61)-C(65) bond length is 1.39 Å. The C(61)-H(33,34) bond length is 1.09 Å. In the twenty-second C site, C(62) is bonded in a distorted trigonal planar geometry to one C(60); one C(66); and one H(33,34) atom. The C(62)-C(66) bond length is 1.39 Å. The C(62)-H(33,34) bond length is 1.09 Å. In the twenty-third C site, C(63) is bonded in a distorted trigonal planar geometry to one C(59); one C(67); and one H(35,36) atom. The C(63)-C(67) bond length is 1.38 Å. The C(63)-H(35,36) bond length is 1.09 Å. In the twenty-fourth C site, C(64) is bonded in a distorted trigonal planar geometry to one C(60); one C(68); and one H(35,36) atom. The C(64)-C(68) bond length is 1.38 Å. The C(64)-H(35,36) bond length is 1.09 Å. In the twenty-fifth C site, C(65) is bonded in a distorted single-bond geometry to one C(61); one C(69,70); and one H(37,38,39) atom. The C(65)-C(69,70) bond length is 1.41 Å. The C(65)-H(37,38,39) bond length is 1.09 Å. In the twenty-sixth C site, C(66) is bonded in a distorted single-bond geometry to one C(62); one C(69,70); and one H(37,38,39) atom. The C(66)-C(69,70) bond length is 1.41 Å. The C(66)-H(37,38,39) bond length is 1.09 Å. In the twenty-seventh C site, C(67) is bonded in a distorted trigonal planar geometry to one C(63); one C(69,70); and one H(37,38,39) atom. The C(67)-C(69,70) bond length is 1.41 Å. The C(67)-H(37,38,39) bond length is 1.09 Å. In the twenty-eighth C site, C(68) is bonded in a distorted trigonal planar geometry to one C(64); one C(69,70); and one H(40) atom. The C(68)-C(69,70) bond length is 1.41 Å. The C(68)-H(40) bond length is 1.09 Å. In the twenty-ninth C site, C(69,70) is bonded in a trigonal planar geometry to one C(65), one C(67), and one C(71) atom. The C(69,70)-C(71) bond length is 1.47 Å. In the thirtieth C site, C(71) is bonded in a trigonal planar geometry to one C(69,70); one C(73); and one C(75) atom. The C(71)-C(73) bond length is 1.41 Å. The C(71)-C(75) bond length is 1.40 Å. In the thirty-first C site, C(72) is bonded in a trigonal planar geometry to one C(69,70); one C(74); and one C(76) atom. The C(72)-C(69,70) bond length is 1.47 Å. The C(72)-C(74) bond length is 1.41 Å. The C(72)-C(76) bond length is 1.40 Å. In the thirty-second C site, C(73) is bonded in a distorted single-bond geometry to one C(71), one C(77), and one H(41) atom. The C(73)-C(77) bond length is 1.38 Å. The C(73)-H(41) bond length is 1.09 Å. In the thirty-third C site, C(74) is bonded in a distorted single-bond geometry to one C(72), one C(78), and one H(42) atom. The C(74)-C(78) bond length is 1.38 Å. The C(74)-H(42) bond length is 1.09 Å. In the thirty-fourth C site, C(75) is bonded in a distorted single-bond geometry to one C(71), one C(79), and one H(43) atom. The C(75)-C(79) bond length is 1.39 Å. The C(75)-H(43) bond length is 1.09 Å. In the thirty-fifth C site, C(76) is bonded in a distorted single-bond geometry to one C(72), one C(80), and one H(44) atom. The C(76)-C(80) bond length is 1.39 Å. The C(76)-H(44) bond length is 1.09 Å. In the thirty-sixth C site, C(77) is bonded in a distorted trigonal planar geometry to one C(73), one N(23), and one H(45) atom. The C(77)-N(23) bond length is 1.35 Å. The C(77)-H(45) bond length is 1.09 Å. In the thirty-seventh C site, C(78) is bonded in a distorted trigonal planar geometry to one C(74), one N(24), and one H(46) atom. The C(78)-N(24) bond length is 1.35 Å. The C(78)-H(46) bond length is 1.09 Å. In the thirty-eighth C site, C(79) is bonded in a distorted trigonal planar geometry to one C(75), one N(23), and one H(47) atom. The C(79)-N(23) bond length is 1.35 Å. The C(79)-H(47) bond length is 1.09 Å. In the thirty-ninth C site, C(80) is bonded in a distorted trigonal planar geometry to one C(76), one N(24), and one H(48) atom. The C(80)-N(24) bond length is 1.35 Å. The C(80)-H(48) bond length is 1.09 Å. There are twelve inequivalent N sites. In the first N site, N(13) is bonded in a linear geometry to one Fe(3) and one C(41) atom. In the second N site, N(14) is bonded in a linear geometry to one Fe(4) and one C(42) atom. In the third N site, N(15) is bonded in a linear geometry to one Fe(4) and one C(43) atom. In the fourth N site, N(16) is bonded in a linear geometry to one Fe(3) and one C(44) atom. In the fifth N site, N(17) is bonded in a linear geometry to one Fe(3) and one C(45) atom. In the sixth N site, N(18) is bonded in a linear geometry to one Fe(4) and one C(46) atom. In the seventh N site, N(19) is bonded in a linear geometry to one Fe(3) and one C(55) atom. In the eighth N site, N(20) is bonded in a linear geometry to one Fe(4) and one C(56) atom. In the ninth N site, N(21) is bonded in a trigonal planar geometry to one Fe(3), one C(47), and one C(49) atom. In the tenth N site, N(22) is bonded in a trigonal planar geometry to one Fe(4), one C(48), and one C(50) atom. In the eleventh N site, N(23) is bonded in a trigonal planar geometry to one Fe(4), one C(77), and one C(79) atom. In the twelfth N site, N(24) is bonded in a trigonal planar geometry to one Fe(3), one C(78), and one C(80) atom. There are twenty inequivalent H sites. In the first H site, H(25) is bonded in a single-bond geometry to one C(47) atom. In the second H site, H(26) is bonded in a single-bond geometry to one C(48) atom. In the third H site, H(27) is bonded in a single-bond geometry to one C(49) atom. In the fourth H site, H(28) is bonded in a single-bond geometry to one C(50) atom. In the fifth H site, H(29) is bonded in a single-bond geometry to one C(51) atom. In the sixth H site, H(30) is bonded in a single-bond geometry to one C(52) atom. In the seventh H site, H(31) is bonded in a single-bond geometry to one C(53) atom. In the eighth H site, H(32) is bonded in a single-bond geometry to one C(54) atom. In the ninth H site, H(33,34) is bonded in a single-bond geometry to one C(61) atom. In the tenth H site, H(35,36) is bonded in a single-bond geometry to one C(63) atom. In the eleventh H site, H(37,38,39) is bonded in a single-bond geometry to one C(65) atom. In the twelfth H site, H(40) is bonded in a single-bond geometry to one C(68) atom. In the thirteenth H site, H(41) is bonded in a single-bond geometry to one C(73) atom. In the fourteenth H site, H(42) is bonded in a single-bond geometry to one C(74) atom. In the fifteenth H site, H(43) is bonded in a single-bond geometry to one C(75) atom. In the sixteenth H site, H(44) is bonded in a single-bond geometry to one C(76) atom. In the seventeenth H site, H(45) is bonded in a single-bond geometry to one C(77) atom. In the eighteenth H site, H(46) is bonded in a single-bond geometry to one C(78) atom. In the nineteenth H site, H(47) is bonded in a single-bond geometry to one C(79) atom. In the twentieth H site, H(48) is bonded in a single-bond geometry to one C(80) atom. Linkers: 4 c1cc(-c2ccc(-c3ccncc3)cc2)ccn1. Metal clusters: 4 [Fe] ,8 [Au]. The MOF has largest included sphere 3.04 A, density 2.04 g/cm3, surface area 3399.57 m2/g, accessible volume 0.15 cm3/g