DyC3H4O8(CH)4(CH2CO)2C4H4O is Indium-derived structured and crystallizes in the triclinic P-1 space group. The structure is zero-dimensional and consists of eight 02329_fluka molecules; two 1-propene, 1-methoxy-, (1z)- molecules; four dimethyl ether molecules; and one DyC3H4O8 cluster. In the DyC3H4O8 cluster, Dy(1) is bonded in a 9-coordinate geometry to one O(1), one O(10), one O(11), one O(2), one O(5), one O(7), one O(8), and two equivalent O(6) atoms. The Dy(1)-O(1) bond length is 2.37 Å. The Dy(1)-O(10) bond length is 2.62 Å. The Dy(1)-O(11) bond length is 2.37 Å. The Dy(1)-O(2) bond length is 2.36 Å. The Dy(1)-O(5) bond length is 2.46 Å. The Dy(1)-O(7) bond length is 2.44 Å. The Dy(1)-O(8) bond length is 2.39 Å. There is one shorter (2.31 Å) and one longer (2.52 Å) Dy(1)-O(6) bond length. There are three inequivalent C sites. In the first C site, C(1) is bonded in a distorted bent 120 degrees geometry to one O(1) and one O(2) atom. The C(1)-O(1) bond length is 1.27 Å. The C(1)-O(2) bond length is 1.27 Å. In the second C site, C(10) is bonded in a distorted bent 120 degrees geometry to one O(5) and one O(6) atom. The C(10)-O(5) bond length is 1.26 Å. The C(10)-O(6) bond length is 1.29 Å. In the third C site, C(11) is bonded in a distorted bent 120 degrees geometry to one O(7) and one O(8) atom. The C(11)-O(7) bond length is 1.29 Å. The C(11)-O(8) bond length is 1.26 Å. There are four inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one O(1) and one O(10) atom. The H(1)-O(1) bond length is 1.73 Å. The H(1)-O(10) bond length is 1.00 Å. In the second H site, H(2) is bonded in a single-bond geometry to one O(10) atom. The H(2)-O(10) bond length is 0.97 Å. In the third H site, H(3) is bonded in a single-bond geometry to one O(11) atom. The H(3)-O(11) bond length is 0.99 Å. In the fourth H site, H(4) is bonded in a single-bond geometry to one O(11) atom. The H(4)-O(11) bond length is 1.01 Å. There are eight inequivalent O sites. In the first O site, O(1) is bonded in a distorted single-bond geometry to one Dy(1), one C(1), and one H(1) atom. In the second O site, O(2) is bonded in a 2-coordinate geometry to one Dy(1) and one C(1) atom. In the third O site, O(5) is bonded in a distorted single-bond geometry to one Dy(1) and one C(10) atom. In the fourth O site, O(6) is bonded in a 3-coordinate geometry to two equivalent Dy(1) and one C(10) atom. In the fifth O site, O(7) is bonded in a distorted single-bond geometry to one Dy(1) and one C(11) atom. In the sixth O site, O(8) is bonded in a distorted L-shaped geometry to one Dy(1) and one C(11) atom. In the seventh O site, O(10) is bonded in a water-like geometry to one Dy(1), one H(1), and one H(2) atom. In the eighth O site, O(11) is bonded in a distorted water-like geometry to one Dy(1), one H(3), and one H(4) atom. Linkers: 3 [O]C(=O)COc1ccc(OCC([O])=O)cc1. Metal clusters: 1 O.O.O.O.O=[C]O[Dy]12(O[C]O1)O[C]O[Dy]1(O[C]=O)(O[C]O1)O[C]O2. RCSR code: sql. The MOF has largest included sphere 2.27 A, density 2.07 g/cm3, surface area 3195.34 m2/g, accessible volume 0.11 cm3/g