Zn3C28H18(NO5)2(CH3)2 crystallizes in the tetragonal P-4c2 space group. The structure consists of eight 02329_fluka molecules inside a Zn3C28H18(NO5)2 framework. In the Zn3C28H18(NO5)2 framework, there are two inequivalent Zn sites. In the first Zn site, Zn(1) is bonded to one N(1), one O(1), one O(3), one O(5), and two equivalent O(4) atoms to form distorted ZnNO5 octahedra that share corners with two equivalent Zn(1)NO5 octahedra and  a cornercorner with one Zn(2)O4 tetrahedra. The corner-sharing octahedral tilt angles are 15°. The Zn(1)-N(1) bond length is 2.11 Å. The Zn(1)-O(1) bond length is 2.14 Å. The Zn(1)-O(3) bond length is 2.00 Å. The Zn(1)-O(5) bond length is 2.09 Å. There is one shorter (2.13 Å) and one longer (2.46 Å) Zn(1)-O(4) bond length. In the second Zn site, Zn(2) is bonded to two equivalent O(2) and two equivalent O(3) atoms to form corner-sharing ZnO4 tetrahedra. The corner-sharing octahedral tilt angles are 58°. Both Zn(2)-O(2) bond lengths are 1.99 Å. Both Zn(2)-O(3) bond lengths are 1.93 Å. There are fourteen inequivalent C sites. In the first C site, C(4) is bonded in a trigonal planar geometry to one C(3), one C(5), and one C(7) atom. The C(4)-C(3) bond length is 1.41 Å. The C(4)-C(5) bond length is 1.41 Å. The C(4)-C(7) bond length is 1.47 Å. In the second C site, C(5) is bonded in a distorted single-bond geometry to one C(4), one C(6), and one H(3) atom. The C(5)-C(6) bond length is 1.39 Å. The C(5)-H(3) bond length is 1.09 Å. In the third C site, C(6) is bonded in a distorted trigonal planar geometry to one C(1), one C(5), and one H(4) atom. The C(6)-C(1) bond length is 1.40 Å. The C(6)-H(4) bond length is 1.09 Å. In the fourth C site, C(7) is bonded in a trigonal planar geometry to one C(11), one C(4), and one C(8) atom. The C(7)-C(11) bond length is 1.40 Å. The C(7)-C(8) bond length is 1.41 Å. In the fifth C site, C(8) is bonded in a distorted trigonal planar geometry to one C(7), one C(9), and one H(5) atom. The C(8)-C(9) bond length is 1.39 Å. The C(8)-H(5) bond length is 1.09 Å. In the sixth C site, C(9) is bonded in a distorted bent 120 degrees geometry to one C(8), one N(1), and one H(6) atom. The C(9)-N(1) bond length is 1.34 Å. The C(9)-H(6) bond length is 1.09 Å. In the seventh C site, C(10) is bonded in a distorted bent 120 degrees geometry to one N(1) and one H(7) atom. The C(10)-N(1) bond length is 1.34 Å. The C(10)-H(7) bond length is 1.09 Å. In the eighth C site, C(11) is bonded in a distorted single-bond geometry to one C(7) and one H(8) atom. The C(11)-H(8) bond length is 1.09 Å. In the ninth C site, C(12) is bonded in a distorted bent 120 degrees geometry to one C(1), one O(1), and one O(2) atom. The C(12)-C(1) bond length is 1.50 Å. The C(12)-O(1) bond length is 1.26 Å. The C(12)-O(2) bond length is 1.29 Å. In the tenth C site, C(13) is bonded in a distorted water-like geometry to one H(9) and one O(3) atom. The C(13)-H(9) bond length is 1.11 Å. The C(13)-O(3) bond length is 1.42 Å. In the eleventh C site, C(14) is bonded in a distorted bent 120 degrees geometry to one O(4) and one O(5) atom. The C(14)-O(4) bond length is 1.28 Å. The C(14)-O(5) bond length is 1.27 Å. In the twelfth C site, C(1) is bonded in a trigonal planar geometry to one C(12), one C(2), and one C(6) atom. The C(1)-C(2) bond length is 1.40 Å. In the thirteenth C site, C(2) is bonded in a distorted single-bond geometry to one C(1), one C(3), and one H(1) atom. The C(2)-C(3) bond length is 1.39 Å. The C(2)-H(1) bond length is 1.09 Å. In the fourteenth C site, C(3) is bonded in a distorted trigonal planar geometry to one C(2), one C(4), and one H(2) atom. The C(3)-H(2) bond length is 1.09 Å. N(1) is bonded in a trigonal planar geometry to one Zn(1), one C(10), and one C(9) atom. There are nine inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one C(2) atom. In the second H site, H(2) is bonded in a single-bond geometry to one C(3) atom. In the third H site, H(3) is bonded in a single-bond geometry to one C(5) atom. In the fourth H site, H(4) is bonded in a single-bond geometry to one C(6) atom. In the fifth H site, H(5) is bonded in a single-bond geometry to one C(8) atom. In the sixth H site, H(6) is bonded in a single-bond geometry to one C(9) atom. In the seventh H site, H(7) is bonded in a single-bond geometry to one C(10) atom. In the eighth H site, H(8) is bonded in a single-bond geometry to one C(11) atom. In the ninth H site, H(9) is bonded in a single-bond geometry to one C(13) atom. There are five inequivalent O sites. In the first O site, O(4) is bonded in a 3-coordinate geometry to two equivalent Zn(1) and one C(14) atom. In the second O site, O(5) is bonded in a water-like geometry to one Zn(1) and one C(14) atom. In the third O site, O(1) is bonded in a bent 150 degrees geometry to one Zn(1) and one C(12) atom. In the fourth O site, O(2) is bonded in a bent 120 degrees geometry to one Zn(2) and one C(12) atom. In the fifth O site, O(3) is bonded in a trigonal planar geometry to one Zn(1), one Zn(2), and one C(13) atom. Linkers: 8 [O]C(=O)c1ccc(-c2ccncc2)cc1 ,4 C[C@@H]([O])C([O])=O ,4 C[C@H]([O])C([O])=O. Metal clusters: 12 [Zn]. The MOF has largest included sphere 10.53 A, density 1.07 g/cm3, surface area 4399.13 m2/g, accessible volume 0.50 cm3/g