Ni2C36N8H24O9(CH)4 crystallizes in the triclinic P1 space group. The structure consists of eight 02329_fluka molecules inside a Ni2C36N8H24O9 framework. In the Ni2C36N8H24O9 framework, there are four inequivalent Ni sites. In the first Ni site, Ni(1) is bonded to one N(16), one N(9), one O(1), one O(13), one O(3), and one O(8) atom to form corner-sharing NiN2O4 octahedra. The corner-sharing octahedral tilt angles are 55°. The Ni(1)-N(16) bond length is 2.01 Å. The Ni(1)-N(9) bond length is 2.07 Å. The Ni(1)-O(1) bond length is 1.78 Å. The Ni(1)-O(13) bond length is 2.07 Å. The Ni(1)-O(3) bond length is 2.00 Å. The Ni(1)-O(8) bond length is 2.09 Å. In the second Ni site, Ni(2) is bonded to one N(10), one N(15), one O(1), one O(14), one O(4), and one O(7) atom to form corner-sharing NiN2O4 octahedra. The corner-sharing octahedral tilt angles are 55°. The Ni(2)-N(10) bond length is 2.07 Å. The Ni(2)-N(15) bond length is 2.00 Å. The Ni(2)-O(1) bond length is 1.78 Å. The Ni(2)-O(14) bond length is 2.08 Å. The Ni(2)-O(4) bond length is 2.00 Å. The Ni(2)-O(7) bond length is 2.08 Å. In the third Ni site, Ni(3) is bonded to one N(11), one N(14), one O(10), one O(11), one O(2), and one O(5) atom to form corner-sharing NiN2O4 octahedra. The corner-sharing octahedral tilt angles are 55°. The Ni(3)-N(11) bond length is 2.07 Å. The Ni(3)-N(14) bond length is 2.01 Å. The Ni(3)-O(10) bond length is 2.09 Å. The Ni(3)-O(11) bond length is 2.08 Å. The Ni(3)-O(2) bond length is 1.78 Å. The Ni(3)-O(5) bond length is 2.00 Å. In the fourth Ni site, Ni(4) is bonded to one N(12), one N(13), one O(12), one O(2), one O(6), and one O(9) atom to form corner-sharing NiN2O4 octahedra. The corner-sharing octahedral tilt angles are 55°. The Ni(4)-N(12) bond length is 2.07 Å. The Ni(4)-N(13) bond length is 2.00 Å. The Ni(4)-O(12) bond length is 2.08 Å. The Ni(4)-O(2) bond length is 1.78 Å. The Ni(4)-O(6) bond length is 1.99 Å. The Ni(4)-O(9) bond length is 2.09 Å. There are seventy-one inequivalent C sites. In the first C site, C(1) is bonded in a trigonal planar geometry to one C(13), one C(17), and one C(25) atom. The C(1)-C(13) bond length is 1.40 Å. The C(1)-C(17) bond length is 1.40 Å. The C(1)-C(25) bond length is 1.50 Å. In the second C site, C(2) is bonded in a trigonal planar geometry to one C(14), one C(18), and one C(26) atom. The C(2)-C(14) bond length is 1.40 Å. The C(2)-C(18) bond length is 1.40 Å. The C(2)-C(26) bond length is 1.50 Å. In the third C site, C(3) is bonded in a trigonal planar geometry to one C(15), one C(19), and one C(27) atom. The C(3)-C(15) bond length is 1.40 Å. The C(3)-C(19) bond length is 1.40 Å. The C(3)-C(27) bond length is 1.50 Å. In the fourth C site, C(4) is bonded in a trigonal planar geometry to one C(16), one C(20), and one C(28) atom. The C(4)-C(16) bond length is 1.40 Å. The C(4)-C(20) bond length is 1.40 Å. The C(4)-C(28) bond length is 1.50 Å. In the fifth C site, C(5) is bonded in a distorted single-bond geometry to one C(9) and one H(1,2,3) atom. The C(5)-C(9) bond length is 1.40 Å. The C(5)-H(1,2,3) bond length is 1.09 Å. In the sixth C site, C(6) is bonded in a distorted single-bond geometry to one C(10) and one H(1,2,3) atom. The C(6)-C(10) bond length is 1.40 Å. The C(6)-H(1,2,3) bond length is 1.09 Å. In the seventh C site, C(7) is bonded in a distorted single-bond geometry to one C(11) and one H(1,2,3) atom. The C(7)-C(11) bond length is 1.40 Å. The C(7)-H(1,2,3) bond length is 1.09 Å. In the eighth C site, C(8) is bonded in a distorted single-bond geometry to one C(12) and one H(4) atom. The C(8)-C(12) bond length is 1.40 Å. The C(8)-H(4) bond length is 1.09 Å. In the ninth C site, C(9) is bonded in a trigonal planar geometry to one C(33), one C(41), and one C(5) atom. The C(9)-C(33) bond length is 1.40 Å. The C(9)-C(41) bond length is 1.52 Å. In the tenth C site, C(10) is bonded in a trigonal planar geometry to one C(34), one C(42), and one C(6) atom. The C(10)-C(34) bond length is 1.40 Å. The C(10)-C(42) bond length is 1.52 Å. In the eleventh C site, C(11) is bonded in a trigonal planar geometry to one C(35), one C(43), and one C(7) atom. The C(11)-C(35) bond length is 1.40 Å. The C(11)-C(43) bond length is 1.52 Å. In the twelfth C site, C(12) is bonded in a trigonal planar geometry to one C(36), one C(44), and one C(8) atom. The C(12)-C(36) bond length is 1.40 Å. The C(12)-C(44) bond length is 1.52 Å. In the thirteenth C site, C(13) is bonded in a distorted single-bond geometry to one C(1); one C(33); and one H(5,6,8) atom. The C(13)-C(33) bond length is 1.39 Å. The C(13)-H(5,6,8) bond length is 1.09 Å. In the fourteenth C site, C(14) is bonded in a distorted single-bond geometry to one C(2); one C(34); and one H(5,6,8) atom. The C(14)-C(34) bond length is 1.39 Å. The C(14)-H(5,6,8) bond length is 1.09 Å. In the fifteenth C site, C(15) is bonded in a distorted single-bond geometry to one C(3), one C(35), and one H(7) atom. The C(15)-C(35) bond length is 1.39 Å. The C(15)-H(7) bond length is 1.09 Å. In the sixteenth C site, C(16) is bonded in a distorted single-bond geometry to one C(36); one C(4); and one H(5,6,8) atom. The C(16)-C(36) bond length is 1.39 Å. The C(16)-H(5,6,8) bond length is 1.09 Å. In the seventeenth C site, C(17) is bonded in a distorted single-bond geometry to one C(1) and one H(9,10,11,12) atom. The C(17)-H(9,10,11,12) bond length is 1.09 Å. In the eighteenth C site, C(18) is bonded in a distorted single-bond geometry to one C(2) and one H(9,10,11,12) atom. The C(18)-H(9,10,11,12) bond length is 1.09 Å. In the nineteenth C site, C(19) is bonded in a distorted single-bond geometry to one C(3) and one H(9,10,11,12) atom. The C(19)-H(9,10,11,12) bond length is 1.09 Å. In the twentieth C site, C(20) is bonded in a distorted single-bond geometry to one C(4) and one H(9,10,11,12) atom. The C(20)-H(9,10,11,12) bond length is 1.09 Å. In the twenty-first C site, C(21) is bonded in a distorted single-bond geometry to one N(5) atom. The C(21)-N(5) bond length is 1.42 Å. In the twenty-second C site, C(22) is bonded in a distorted single-bond geometry to one N(6,7) atom. The C(22)-N(6,7) bond length is 1.42 Å. In the twenty-third C site, C(23) is bonded in a distorted single-bond geometry to one N(6,7) atom. The C(23)-N(6,7) bond length is 1.42 Å. In the twenty-fourth C site, C(24) is bonded in a distorted single-bond geometry to one N(8) atom. The C(24)-N(8) bond length is 1.42 Å. In the twenty-fifth C site, C(25) is bonded in a distorted bent 120 degrees geometry to one C(1), one O(3), and one O(7) atom. The C(25)-O(3) bond length is 1.27 Å. The C(25)-O(7) bond length is 1.27 Å. In the twenty-sixth C site, C(26) is bonded in a distorted bent 120 degrees geometry to one C(2), one O(4), and one O(8) atom. The C(26)-O(4) bond length is 1.27 Å. The C(26)-O(8) bond length is 1.27 Å. In the twenty-seventh C site, C(27) is bonded in a distorted bent 120 degrees geometry to one C(3), one O(5), and one O(9) atom. The C(27)-O(5) bond length is 1.27 Å. The C(27)-O(9) bond length is 1.27 Å. In the twenty-eighth C site, C(28) is bonded in a distorted bent 120 degrees geometry to one C(4), one O(10), and one O(6) atom. The C(28)-O(10) bond length is 1.27 Å. The C(28)-O(6) bond length is 1.27 Å. In the twenty-ninth C site, C(29) is bonded in a trigonal planar geometry to one N(5), one N(9), and one H(13) atom. The C(29)-N(5) bond length is 1.37 Å. The C(29)-N(9) bond length is 1.32 Å. The C(29)-H(13) bond length is 1.08 Å. In the thirtieth C site, C(30) is bonded in a trigonal planar geometry to one N(10); one N(6,7); and one H(14,15) atom. The C(30)-N(10) bond length is 1.32 Å. The C(30)-N(6,7) bond length is 1.37 Å. The C(30)-H(14,15) bond length is 1.08 Å. In the thirty-first C site, C(31) is bonded in a trigonal planar geometry to one N(11); one N(6,7); and one H(14,15) atom. The C(31)-N(11) bond length is 1.32 Å. The C(31)-N(6,7) bond length is 1.37 Å. The C(31)-H(14,15) bond length is 1.08 Å. In the thirty-second C site, C(32) is bonded in a trigonal planar geometry to one N(12), one N(8), and one H(16) atom. The C(32)-N(12) bond length is 1.32 Å. The C(32)-N(8) bond length is 1.37 Å. The C(32)-H(16) bond length is 1.08 Å. In the thirty-third C site, C(33) is bonded in a distorted trigonal planar geometry to one C(13); one C(9); and one H(17,19) atom. The C(33)-H(17,19) bond length is 1.09 Å. In the thirty-fourth C site, C(34) is bonded in a distorted trigonal planar geometry to one C(10), one C(14), and one H(18) atom. The C(34)-H(18) bond length is 1.09 Å. In the thirty-fifth C site, C(35) is bonded in a distorted trigonal planar geometry to one C(11); one C(15); and one H(17,19) atom. The C(35)-H(17,19) bond length is 1.09 Å. In the thirty-sixth C site, C(36) is bonded in a distorted trigonal planar geometry to one C(12), one C(16), and one H(20) atom. The C(36)-H(20) bond length is 1.09 Å. In the thirty-seventh C site, C(37) is bonded in a trigonal planar geometry to one N(1); one N(13); and one H(21,24) atom. The C(37)-N(1) bond length is 1.37 Å. The C(37)-N(13) bond length is 1.32 Å. The C(37)-H(21,24) bond length is 1.08 Å. In the thirty-eighth C site, C(38) is bonded in a trigonal planar geometry to one N(14), one N(2), and one H(22) atom. The C(38)-N(14) bond length is 1.32 Å. The C(38)-N(2) bond length is 1.37 Å. The C(38)-H(22) bond length is 1.08 Å. In the thirty-ninth C site, C(39) is bonded in a trigonal planar geometry to one N(15), one N(3), and one H(23) atom. The C(39)-N(15) bond length is 1.32 Å. The C(39)-N(3) bond length is 1.37 Å. The C(39)-H(23) bond length is 1.08 Å. In the fortieth C site, C(40) is bonded in a trigonal planar geometry to one N(16); one N(4); and one H(21,24) atom. The C(40)-N(16) bond length is 1.32 Å. The C(40)-N(4) bond length is 1.37 Å. The C(40)-H(21,24) bond length is 1.08 Å. In the forty-first C site, C(41) is bonded in a distorted bent 120 degrees geometry to one C(9); one O(11); and one O(15,16) atom. The C(41)-O(11) bond length is 1.29 Å. The C(41)-O(15,16) bond length is 1.25 Å. In the forty-second C site, C(42) is bonded in a distorted bent 120 degrees geometry to one C(10); one O(12); and one O(15,16) atom. The C(42)-O(12) bond length is 1.29 Å. The C(42)-O(15,16) bond length is 1.25 Å. In the forty-third C site, C(43) is bonded in a distorted bent 120 degrees geometry to one C(11), one O(13), and one O(17) atom. The C(43)-O(13) bond length is 1.29 Å. The C(43)-O(17) bond length is 1.25 Å. In the forty-fourth C site, C(44) is bonded in a distorted bent 120 degrees geometry to one C(12), one O(14), and one O(18) atom. The C(44)-O(14) bond length is 1.29 Å. The C(44)-O(18) bond length is 1.25 Å. In the forty-fifth C site, C(45) is bonded in a distorted single-bond geometry to one C(53) and one H(25,33) atom. The C(45)-C(53) bond length is 1.40 Å. The C(45)-H(25,33) bond length is 1.09 Å. In the forty-sixth C site, C(46) is bonded in a distorted single-bond geometry to one C(54) and one H(26,27,28,34,35,36) atom. The C(46)-C(54) bond length is 1.40 Å. The C(46)-H(26,27,28,34,35,36) bond length is 1.09 Å. In the forty-seventh C site, C(47) is bonded in a distorted single-bond geometry to one C(55) and one H(26,27,28,34,35,36) atom. The C(47)-C(55) bond length is 1.40 Å. The C(47)-H(26,27,28,34,35,36) bond length is 1.09 Å. In the forty-eighth C site, C(48) is bonded in a distorted single-bond geometry to one C(56) and one H(26,27,28,34,35,36) atom. The C(48)-C(56) bond length is 1.40 Å. The C(48)-H(26,27,28,34,35,36) bond length is 1.09 Å. In the forty-ninth C site, C(53) is bonded in a distorted trigonal planar geometry to one C(45), one C(57), and one N(1) atom. The C(53)-C(57) bond length is 1.40 Å. The C(53)-N(1) bond length is 1.42 Å. In the fiftieth C site, C(54) is bonded in a distorted trigonal planar geometry to one C(46), one C(58), and one N(2) atom. The C(54)-C(58) bond length is 1.40 Å. The C(54)-N(2) bond length is 1.42 Å. In the fifty-first C site, C(55) is bonded in a distorted trigonal planar geometry to one C(47), one C(59), and one N(3) atom. The C(55)-C(59) bond length is 1.40 Å. The C(55)-N(3) bond length is 1.42 Å. In the fifty-second C site, C(56) is bonded in a distorted trigonal planar geometry to one C(48), one C(60), and one N(4) atom. The C(56)-C(60) bond length is 1.40 Å. The C(56)-N(4) bond length is 1.42 Å. In the fifty-third C site, C(57) is bonded in a distorted single-bond geometry to one C(53) and one H(25,33) atom. The C(57)-H(25,33) bond length is 1.09 Å. In the fifty-fourth C site, C(58) is bonded in a distorted single-bond geometry to one C(54) and one H(26,27,28,34,35,36) atom. The C(58)-H(26,27,28,34,35,36) bond length is 1.09 Å. In the fifty-fifth C site, C(59) is bonded in a distorted single-bond geometry to one C(55) and one H(26,27,28,34,35,36) atom. The C(59)-H(26,27,28,34,35,36) bond length is 1.09 Å. In the fifty-sixth C site, C(60) is bonded in a distorted single-bond geometry to one C(56) and one H(26,27,28,34,35,36) atom. The C(60)-H(26,27,28,34,35,36) bond length is 1.09 Å. In the fifty-seventh C site, C(65) is bonded in a distorted bent 120 degrees geometry to one C(77); one N(13); and one H(41,44) atom. The C(65)-C(77) bond length is 1.37 Å. The C(65)-N(13) bond length is 1.38 Å. The C(65)-H(41,44) bond length is 1.08 Å. In the fifty-eighth C site, C(66) is bonded in a distorted bent 120 degrees geometry to one C(78), one N(14), and one H(42) atom. The C(66)-C(78) bond length is 1.37 Å. The C(66)-N(14) bond length is 1.38 Å. The C(66)-H(42) bond length is 1.08 Å. In the fifty-ninth C site, C(67) is bonded in a distorted bent 120 degrees geometry to one C(79), one N(15), and one H(43) atom. The C(67)-C(79) bond length is 1.37 Å. The C(67)-N(15) bond length is 1.38 Å. The C(67)-H(43) bond length is 1.08 Å. In the sixtieth C site, C(68) is bonded in a distorted bent 120 degrees geometry to one C(80); one N(16); and one H(41,44) atom. The C(68)-C(80) bond length is 1.37 Å. The C(68)-N(16) bond length is 1.38 Å. The C(68)-H(41,44) bond length is 1.08 Å. In the sixty-first C site, C(69) is bonded in a distorted bent 120 degrees geometry to one N(5) and one H(45,48) atom. The C(69)-N(5) bond length is 1.39 Å. The C(69)-H(45,48) bond length is 1.08 Å. In the sixty-second C site, C(70) is bonded in a distorted bent 120 degrees geometry to one N(6,7) and one H(46,47) atom. The C(70)-N(6,7) bond length is 1.39 Å. The C(70)-H(46,47) bond length is 1.08 Å. In the sixty-third C site, C(71) is bonded in a distorted bent 120 degrees geometry to one N(6,7) and one H(46,47) atom. The C(71)-N(6,7) bond length is 1.39 Å. The C(71)-H(46,47) bond length is 1.08 Å. In the sixty-fourth C site, C(72) is bonded in a distorted bent 120 degrees geometry to one N(8) and one H(45,48) atom. The C(72)-N(8) bond length is 1.39 Å. The C(72)-H(45,48) bond length is 1.08 Å. In the sixty-fifth C site, C(73,75) is bonded in a distorted bent 120 degrees geometry to one N(9) and one H(49) atom. The C(73,75)-N(9) bond length is 1.38 Å. The C(73,75)-H(49) bond length is 1.08 Å. In the sixty-sixth C site, C(74) is bonded in a distorted bent 120 degrees geometry to one N(10) and one H(50,51) atom. The C(74)-N(10) bond length is 1.38 Å. The C(74)-H(50,51) bond length is 1.08 Å. In the sixty-seventh C site, C(76) is bonded in a distorted bent 120 degrees geometry to one N(12) and one H(52) atom. The C(76)-N(12) bond length is 1.38 Å. The C(76)-H(52) bond length is 1.08 Å. In the sixty-eighth C site, C(77) is bonded in a distorted bent 120 degrees geometry to one C(65); one N(1); and one H(53,54,56) atom. The C(77)-N(1) bond length is 1.39 Å. The C(77)-H(53,54,56) bond length is 1.08 Å. In the sixty-ninth C site, C(78) is bonded in a distorted bent 120 degrees geometry to one C(66); one N(2); and one H(53,54,56) atom. The C(78)-N(2) bond length is 1.39 Å. The C(78)-H(53,54,56) bond length is 1.08 Å. In the seventieth C site, C(79) is bonded in a distorted bent 120 degrees geometry to one C(67), one N(3), and one H(55) atom. The C(79)-N(3) bond length is 1.39 Å. The C(79)-H(55) bond length is 1.08 Å. In the seventy-first C site, C(80) is bonded in a distorted bent 120 degrees geometry to one C(68); one N(4); and one H(53,54,56) atom. The C(80)-N(4) bond length is 1.39 Å. The C(80)-H(53,54,56) bond length is 1.08 Å. There are fifteen inequivalent N sites. In the first N site, N(1) is bonded in a trigonal planar geometry to one C(37), one C(53), and one C(77) atom. In the second N site, N(2) is bonded in a trigonal planar geometry to one C(38), one C(54), and one C(78) atom. In the third N site, N(3) is bonded in a trigonal planar geometry to one C(39), one C(55), and one C(79) atom. In the fourth N site, N(4) is bonded in a trigonal planar geometry to one C(40), one C(56), and one C(80) atom. In the fifth N site, N(5) is bonded in a trigonal planar geometry to one C(21), one C(29), and one C(69) atom. In the sixth N site, N(6,7) is bonded in a trigonal planar geometry to one C(22), one C(30), and one C(70) atom. In the seventh N site, N(8) is bonded in a trigonal planar geometry to one C(24), one C(32), and one C(72) atom. In the eighth N site, N(9) is bonded in a trigonal planar geometry to one Ni(1); one C(29); and one C(73,75) atom. In the ninth N site, N(10) is bonded in a trigonal planar geometry to one Ni(2), one C(30), and one C(74) atom. In the tenth N site, N(11) is bonded in a trigonal planar geometry to one Ni(3); one C(31); and one C(73,75) atom. The N(11)-C(73,75) bond length is 1.38 Å. In the eleventh N site, N(12) is bonded in a trigonal planar geometry to one Ni(4), one C(32), and one C(76) atom. In the twelfth N site, N(13) is bonded in a trigonal planar geometry to one Ni(4), one C(37), and one C(65) atom. In the thirteenth N site, N(14) is bonded in a trigonal planar geometry to one Ni(3), one C(38), and one C(66) atom. In the fourteenth N site, N(15) is bonded in a trigonal planar geometry to one Ni(2), one C(39), and one C(67) atom. In the fifteenth N site, N(16) is bonded in a trigonal planar geometry to one Ni(1), one C(40), and one C(68) atom. There are twenty-six inequivalent H sites. In the first H site, H(1,2,3) is bonded in a single-bond geometry to one C(5) atom. In the second H site, H(4) is bonded in a single-bond geometry to one C(8) atom. In the third H site, H(5,6,8) is bonded in a single-bond geometry to one C(13) atom. In the fourth H site, H(7) is bonded in a single-bond geometry to one C(15) atom. In the fifth H site, H(9,10,11,12) is bonded in a single-bond geometry to one C(17) atom. In the sixth H site, H(13) is bonded in a single-bond geometry to one C(29) atom. In the seventh H site, H(14,15) is bonded in a single-bond geometry to one C(30) atom. In the eighth H site, H(16) is bonded in a single-bond geometry to one C(32) atom. In the ninth H site, H(17,19) is bonded in a single-bond geometry to one C(33) atom. In the tenth H site, H(18) is bonded in a single-bond geometry to one C(34) atom. In the eleventh H site, H(20) is bonded in a single-bond geometry to one C(36) atom. In the twelfth H site, H(21,24) is bonded in a single-bond geometry to one C(37) atom. In the thirteenth H site, H(22) is bonded in a single-bond geometry to one C(38) atom. In the fourteenth H site, H(23) is bonded in a single-bond geometry to one C(39) atom. In the fifteenth H site, H(25,33) is bonded in a single-bond geometry to one C(45) atom. In the sixteenth H site, H(26,27,28,34,35,36) is bonded in a single-bond geometry to one C(46) atom. In the seventeenth H site, H(41,44) is bonded in a single-bond geometry to one C(65) atom. In the eighteenth H site, H(42) is bonded in a single-bond geometry to one C(66) atom. In the nineteenth H site, H(43) is bonded in a single-bond geometry to one C(67) atom. In the twentieth H site, H(45,48) is bonded in a single-bond geometry to one C(69) atom. In the twenty-first H site, H(46,47) is bonded in a single-bond geometry to one C(70) atom. In the twenty-second H site, H(49) is bonded in a single-bond geometry to one C(73,75) atom. In the twenty-third H site, H(50,51) is bonded in a single-bond geometry to one C(74) atom. In the twenty-fourth H site, H(52) is bonded in a single-bond geometry to one C(76) atom. In the twenty-fifth H site, H(53,54,56) is bonded in a single-bond geometry to one C(77) atom. In the twenty-sixth H site, H(55) is bonded in a single-bond geometry to one C(79) atom. There are seventeen inequivalent O sites. In the first O site, O(1) is bonded in a bent 120 degrees geometry to one Ni(1) and one Ni(2) atom. In the second O site, O(2) is bonded in a bent 120 degrees geometry to one Ni(3) and one Ni(4) atom. In the third O site, O(3) is bonded in a bent 120 degrees geometry to one Ni(1) and one C(25) atom. In the fourth O site, O(4) is bonded in a bent 120 degrees geometry to one Ni(2) and one C(26) atom. In the fifth O site, O(5) is bonded in a bent 120 degrees geometry to one Ni(3) and one C(27) atom. In the sixth O site, O(6) is bonded in a bent 120 degrees geometry to one Ni(4) and one C(28) atom. In the seventh O site, O(7) is bonded in a bent 120 degrees geometry to one Ni(2) and one C(25) atom. In the eighth O site, O(8) is bonded in a bent 120 degrees geometry to one Ni(1) and one C(26) atom. In the ninth O site, O(9) is bonded in a bent 120 degrees geometry to one Ni(4) and one C(27) atom. In the tenth O site, O(10) is bonded in a bent 120 degrees geometry to one Ni(3) and one C(28) atom. In the eleventh O site, O(11) is bonded in a bent 120 degrees geometry to one Ni(3) and one C(41) atom. In the twelfth O site, O(12) is bonded in a bent 120 degrees geometry to one Ni(4) and one C(42) atom. In the thirteenth O site, O(13) is bonded in a bent 120 degrees geometry to one Ni(1) and one C(43) atom. In the fourteenth O site, O(14) is bonded in a bent 120 degrees geometry to one Ni(2) and one C(44) atom. In the fifteenth O site, O(15,16) is bonded in a single-bond geometry to one C(41) atom. In the sixteenth O site, O(17) is bonded in a single-bond geometry to one C(43) atom. In the seventeenth O site, O(18) is bonded in a single-bond geometry to one C(44) atom. Linkers: 4 [O]C(=O)c1ccc(C([O])=O)cc1 ,3 c1cn(-c2ccc(-n3ccnc3)cc2)cn1. Metal clusters: 4 [Ni]. RCSR code: dia-f. The MOF has largest included sphere 5.43 A, density 0.99 g/cm3, surface area 4524.31 m2/g, accessible volume 0.48 cm3/g