DyAgC15H11(NO6)2 crystallizes in the triclinic P-1 space group. Dy(1) is bonded in a 8-coordinate geometry to one O(10), one O(12), one O(2), one O(3), one O(4), one O(6), one O(8), and one O(9) atom. The Dy(1)-O(10) bond length is 2.41 Å. The Dy(1)-O(12) bond length is 2.29 Å. The Dy(1)-O(2) bond length is 2.43 Å. The Dy(1)-O(3) bond length is 2.35 Å. The Dy(1)-O(4) bond length is 2.38 Å. The Dy(1)-O(6) bond length is 2.46 Å. The Dy(1)-O(8) bond length is 2.34 Å. The Dy(1)-O(9) bond length is 2.33 Å. Ag(1) is bonded in a 2-coordinate geometry to one N(1) and one N(2) atom. The Ag(1)-N(1) bond length is 2.14 Å. The Ag(1)-N(2) bond length is 2.14 Å. There are fifteen inequivalent C sites. In the first C site, C(1) is bonded in a trigonal planar geometry to one C(14), one C(4), and one C(7) atom. The C(1)-C(14) bond length is 1.39 Å. The C(1)-C(4) bond length is 1.39 Å. The C(1)-C(7) bond length is 1.49 Å. In the second C site, C(2) is bonded in a distorted bent 120 degrees geometry to one C(12), one N(1), and one H(6) atom. The C(2)-C(12) bond length is 1.39 Å. The C(2)-N(1) bond length is 1.35 Å. The C(2)-H(6) bond length is 1.09 Å. In the third C site, C(3) is bonded in a trigonal planar geometry to one C(10), one C(6), and one C(9) atom. The C(3)-C(10) bond length is 1.50 Å. The C(3)-C(6) bond length is 1.40 Å. The C(3)-C(9) bond length is 1.40 Å. In the fourth C site, C(4) is bonded in a distorted single-bond geometry to one C(1), one C(5), and one H(7) atom. The C(4)-C(5) bond length is 1.39 Å. The C(4)-H(7) bond length is 1.09 Å. In the fifth C site, C(5) is bonded in a trigonal planar geometry to one C(13), one C(15), and one C(4) atom. The C(5)-C(13) bond length is 1.40 Å. The C(5)-C(15) bond length is 1.51 Å. In the sixth C site, C(6) is bonded in a distorted trigonal planar geometry to one C(3), one N(1), and one H(8) atom. The C(6)-N(1) bond length is 1.35 Å. The C(6)-H(8) bond length is 1.09 Å. In the seventh C site, C(7) is bonded in a distorted bent 120 degrees geometry to one C(1), one O(3), and one O(9) atom. The C(7)-O(3) bond length is 1.28 Å. The C(7)-O(9) bond length is 1.26 Å. In the eighth C site, C(8) is bonded in a distorted bent 120 degrees geometry to one O(10) and one O(6) atom. The C(8)-O(10) bond length is 1.27 Å. The C(8)-O(6) bond length is 1.26 Å. In the ninth C site, C(9) is bonded in a distorted single-bond geometry to one C(12), one C(3), and one H(9) atom. The C(9)-C(12) bond length is 1.39 Å. The C(9)-H(9) bond length is 1.09 Å. In the tenth C site, C(10) is bonded in a distorted bent 120 degrees geometry to one C(3), one O(1), and one O(7) atom. The C(10)-O(1) bond length is 1.33 Å. The C(10)-O(7) bond length is 1.23 Å. In the eleventh C site, C(11) is bonded in a distorted bent 120 degrees geometry to one C(12), one O(5), and one O(8) atom. The C(11)-C(12) bond length is 1.50 Å. The C(11)-O(5) bond length is 1.28 Å. The C(11)-O(8) bond length is 1.26 Å. In the twelfth C site, C(12) is bonded in a trigonal planar geometry to one C(11), one C(2), and one C(9) atom. In the thirteenth C site, C(13) is bonded in a distorted trigonal planar geometry to one C(5), one N(2), and one H(10) atom. The C(13)-N(2) bond length is 1.35 Å. The C(13)-H(10) bond length is 1.09 Å. In the fourteenth C site, C(14) is bonded in a distorted bent 120 degrees geometry to one C(1), one N(2), and one H(11) atom. The C(14)-N(2) bond length is 1.35 Å. The C(14)-H(11) bond length is 1.09 Å. In the fifteenth C site, C(15) is bonded in a distorted bent 120 degrees geometry to one C(5), one O(11), and one O(12) atom. The C(15)-O(11) bond length is 1.26 Å. The C(15)-O(12) bond length is 1.28 Å. There are two inequivalent N sites. In the first N site, N(1) is bonded in a trigonal planar geometry to one Ag(1), one C(2), and one C(6) atom. In the second N site, N(2) is bonded in a trigonal planar geometry to one Ag(1), one C(13), and one C(14) atom. There are eleven inequivalent H sites. In the first H site, H(1) is bonded in a bent 150 degrees geometry to one O(1) and one O(5) atom. The H(1)-O(1) bond length is 1.02 Å. The H(1)-O(5) bond length is 1.55 Å. In the second H site, H(2) is bonded in a single-bond geometry to one O(2) atom. The H(2)-O(2) bond length is 0.99 Å. In the third H site, H(3) is bonded in a single-bond geometry to one O(2) atom. The H(3)-O(2) bond length is 0.99 Å. In the fourth H site, H(4) is bonded in a single-bond geometry to one O(4) atom. The H(4)-O(4) bond length is 0.99 Å. In the fifth H site, H(5) is bonded in a single-bond geometry to one O(4) atom. The H(5)-O(4) bond length is 0.99 Å. In the sixth H site, H(6) is bonded in a single-bond geometry to one C(2) atom. In the seventh H site, H(7) is bonded in a single-bond geometry to one C(4) atom. In the eighth H site, H(8) is bonded in a single-bond geometry to one C(6) atom. In the ninth H site, H(9) is bonded in a single-bond geometry to one C(9) atom. In the tenth H site, H(10) is bonded in a single-bond geometry to one C(13) atom. In the eleventh H site, H(11) is bonded in a single-bond geometry to one C(14) atom. There are twelve inequivalent O sites. In the first O site, O(1) is bonded in a bent 120 degrees geometry to one C(10) and one H(1) atom. In the second O site, O(2) is bonded in a water-like geometry to one Dy(1), one H(2), and one H(3) atom. In the third O site, O(3) is bonded in a distorted single-bond geometry to one Dy(1) and one C(7) atom. In the fourth O site, O(4) is bonded in a distorted water-like geometry to one Dy(1), one H(4), and one H(5) atom. In the fifth O site, O(5) is bonded in a distorted bent 120 degrees geometry to one C(11) and one H(1) atom. In the sixth O site, O(6) is bonded in a distorted single-bond geometry to one Dy(1) and one C(8) atom. In the seventh O site, O(7) is bonded in a single-bond geometry to one C(10) atom. In the eighth O site, O(8) is bonded in a distorted single-bond geometry to one Dy(1) and one C(11) atom. In the ninth O site, O(9) is bonded in a distorted single-bond geometry to one Dy(1) and one C(7) atom. In the tenth O site, O(10) is bonded in a distorted bent 120 degrees geometry to one Dy(1) and one C(8) atom. In the eleventh O site, O(11) is bonded in a single-bond geometry to one C(15) atom. In the twelfth O site, O(12) is bonded in a bent 150 degrees geometry to one Dy(1) and one C(15) atom. Linkers: 2 [O]C(=O)c1cncc(C([O])=O)c1 ,2 [O]C(=O)c1cncc(C(=O)O)c1 ,1 [O]C(=O)C([O])=O. Metal clusters: 2 [Dy] ,2 [Ag]. The MOF has largest included sphere 1.61 A, density 2.68 g/cm3, surface area 2400.01 m2/g, accessible volume 0.03 cm3/g