(CH)4PbC12H12(NO3)2 crystallizes in the monoclinic C2/c space group. The structure consists of sixteen 02329_fluka molecules inside a PbC12H12(NO3)2 framework. In the PbC12H12(NO3)2 framework, Pb(1) is bonded in a 8-coordinate geometry to two equivalent O(2), two equivalent O(3), and four equivalent O(1) atoms. Both Pb(1)-O(2) bond lengths are 2.72 Å. Both Pb(1)-O(3) bond lengths are 2.72 Å. There are two shorter (2.60 Å) and two longer (2.70 Å) Pb(1)-O(1) bond lengths. There are six inequivalent C sites. In the first C site, C(8) is bonded in a tetrahedral geometry to one H(5), one H(6), one H(7), and one O(3) atom. The C(8)-H(5) bond length is 1.10 Å. The C(8)-H(6) bond length is 1.10 Å. The C(8)-H(7) bond length is 1.10 Å. The C(8)-O(3) bond length is 1.43 Å. In the second C site, C(1) is bonded in a distorted bent 120 degrees geometry to one C(2), one O(1), and one O(2) atom. The C(1)-C(2) bond length is 1.50 Å. The C(1)-O(1) bond length is 1.28 Å. The C(1)-O(2) bond length is 1.27 Å. In the third C site, C(2) is bonded in a trigonal planar geometry to one C(1), one C(3), and one C(7) atom. The C(2)-C(3) bond length is 1.40 Å. The C(2)-C(7) bond length is 1.41 Å. In the fourth C site, C(3) is bonded in a distorted single-bond geometry to one C(2) and one H(1) atom. The C(3)-H(1) bond length is 1.09 Å. In the fifth C site, C(7) is bonded in a distorted trigonal planar geometry to one C(2), one C(6), and one N(1) atom. The C(7)-C(6) bond length is 1.41 Å. The C(7)-N(1) bond length is 1.41 Å. In the sixth C site, C(6) is bonded in a distorted single-bond geometry to one C(7) and one H(4) atom. The C(6)-H(4) bond length is 1.09 Å. N(1) is bonded in a bent 120 degrees geometry to one C(7) and one N(1) atom. The N(1)-N(1) bond length is 1.26 Å. There are six inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one C(3) atom. In the second H site, H(4) is bonded in a single-bond geometry to one C(6) atom. In the third H site, H(5) is bonded in a single-bond geometry to one C(8) atom. In the fourth H site, H(6) is bonded in a single-bond geometry to one C(8) atom. In the fifth H site, H(7) is bonded in a single-bond geometry to one C(8) atom. In the sixth H site, H(8) is bonded in a single-bond geometry to one O(3) atom. The H(8)-O(3) bond length is 1.00 Å. There are three inequivalent O sites. In the first O site, O(1) is bonded in a single-bond geometry to two equivalent Pb(1) and one C(1) atom. In the second O site, O(2) is bonded in a distorted single-bond geometry to one Pb(1) and one C(1) atom. In the third O site, O(3) is bonded in a distorted water-like geometry to one Pb(1), one C(8), and one H(8) atom. Linkers: 2 [O]C(=O)c1ccccc1[N][N]c1ccccc1C([O])=O. Metal clusters: 2 [Pb]. RCSR code: pts. The MOF has largest included sphere 1.76 A, density 2.09 g/cm3, surface area 3652.46 m2/g, accessible volume 0.12 cm3/g