Dy6C89H61O46CH crystallizes in the monoclinic Cc space group. The structure consists of four 02329_fluka molecules inside a Dy6C89H61O46 framework. In the Dy6C89H61O46 framework, there are six inequivalent Dy sites. In the first Dy site, Dy(1) is bonded in a 9-coordinate geometry to one O(15), one O(16), one O(25), one O(26), one O(29), one O(30), one O(45), one O(5), and one O(6) atom. The Dy(1)-O(15) bond length is 2.26 Å. The Dy(1)-O(16) bond length is 2.24 Å. The Dy(1)-O(25) bond length is 2.74 Å. The Dy(1)-O(26) bond length is 2.69 Å. The Dy(1)-O(29) bond length is 2.42 Å. The Dy(1)-O(30) bond length is 2.43 Å. The Dy(1)-O(45) bond length is 2.51 Å. The Dy(1)-O(5) bond length is 2.33 Å. The Dy(1)-O(6) bond length is 2.31 Å. In the second Dy site, Dy(2) is bonded in a 9-coordinate geometry to one O(13), one O(14), one O(27), one O(28), one O(31), one O(32), one O(46), one O(7), and one O(8) atom. The Dy(2)-O(13) bond length is 2.25 Å. The Dy(2)-O(14) bond length is 2.25 Å. The Dy(2)-O(27) bond length is 2.74 Å. The Dy(2)-O(28) bond length is 2.70 Å. The Dy(2)-O(31) bond length is 2.42 Å. The Dy(2)-O(32) bond length is 2.43 Å. The Dy(2)-O(46) bond length is 2.51 Å. The Dy(2)-O(7) bond length is 2.33 Å. The Dy(2)-O(8) bond length is 2.31 Å. In the third Dy site, Dy(3) is bonded in a 8-coordinate geometry to one O(1), one O(11), one O(19), one O(23), one O(25), one O(33), one O(37), and one O(41) atom. The Dy(3)-O(1) bond length is 2.30 Å. The Dy(3)-O(11) bond length is 2.33 Å. The Dy(3)-O(19) bond length is 2.45 Å. The Dy(3)-O(23) bond length is 2.36 Å. The Dy(3)-O(25) bond length is 2.30 Å. The Dy(3)-O(33) bond length is 2.27 Å. The Dy(3)-O(37) bond length is 2.66 Å. The Dy(3)-O(41) bond length is 2.41 Å. In the fourth Dy site, Dy(4) is bonded in a 9-coordinate geometry to one O(12), one O(16), one O(2), one O(20), one O(24), one O(26), one O(34), one O(38), and one O(42) atom. The Dy(4)-O(12) bond length is 2.33 Å. The Dy(4)-O(16) bond length is 2.95 Å. The Dy(4)-O(2) bond length is 2.31 Å. The Dy(4)-O(20) bond length is 2.47 Å. The Dy(4)-O(24) bond length is 2.37 Å. The Dy(4)-O(26) bond length is 2.30 Å. The Dy(4)-O(34) bond length is 2.28 Å. The Dy(4)-O(38) bond length is 2.66 Å. The Dy(4)-O(42) bond length is 2.41 Å. In the fifth Dy site, Dy(5) is bonded in a 8-coordinate geometry to one O(10), one O(17), one O(21), one O(27), one O(3), one O(35), one O(39), and one O(43) atom. The Dy(5)-O(10) bond length is 2.33 Å. The Dy(5)-O(17) bond length is 2.46 Å. The Dy(5)-O(21) bond length is 2.36 Å. The Dy(5)-O(27) bond length is 2.30 Å. The Dy(5)-O(3) bond length is 2.31 Å. The Dy(5)-O(35) bond length is 2.27 Å. The Dy(5)-O(39) bond length is 2.66 Å. The Dy(5)-O(43) bond length is 2.41 Å. In the sixth Dy site, Dy(6) is bonded in a 9-coordinate geometry to one O(13), one O(18), one O(22), one O(28), one O(36), one O(4), one O(40), one O(44), and one O(9) atom. The Dy(6)-O(13) bond length is 2.94 Å. The Dy(6)-O(18) bond length is 2.46 Å. The Dy(6)-O(22) bond length is 2.37 Å. The Dy(6)-O(28) bond length is 2.30 Å. The Dy(6)-O(36) bond length is 2.28 Å. The Dy(6)-O(4) bond length is 2.30 Å. The Dy(6)-O(40) bond length is 2.66 Å. The Dy(6)-O(44) bond length is 2.41 Å. The Dy(6)-O(9) bond length is 2.33 Å. There are eighty-eight inequivalent C sites. In the first C site, C(1) is bonded in a distorted bent 120 degrees geometry to one C(5), one O(1), and one O(5) atom. The C(1)-C(5) bond length is 1.51 Å. The C(1)-O(1) bond length is 1.26 Å. The C(1)-O(5) bond length is 1.28 Å. In the second C site, C(2) is bonded in a distorted bent 120 degrees geometry to one C(6), one O(2), and one O(6) atom. The C(2)-C(6) bond length is 1.51 Å. The C(2)-O(2) bond length is 1.27 Å. The C(2)-O(6) bond length is 1.28 Å. In the third C site, C(3) is bonded in a distorted bent 120 degrees geometry to one C(7), one O(3), and one O(7) atom. The C(3)-C(7) bond length is 1.51 Å. The C(3)-O(3) bond length is 1.26 Å. The C(3)-O(7) bond length is 1.28 Å. In the fourth C site, C(4) is bonded in a distorted bent 120 degrees geometry to one C(8), one O(4), and one O(8) atom. The C(4)-C(8) bond length is 1.51 Å. The C(4)-O(4) bond length is 1.27 Å. The C(4)-O(8) bond length is 1.28 Å. In the fifth C site, C(5) is bonded in a trigonal planar geometry to one C(1), one C(25), and one C(9) atom. The C(5)-C(25) bond length is 1.42 Å. The C(5)-C(9) bond length is 1.39 Å. In the sixth C site, C(6) is bonded in a trigonal planar geometry to one C(10), one C(2), and one C(26) atom. The C(6)-C(10) bond length is 1.40 Å. The C(6)-C(26) bond length is 1.42 Å. In the seventh C site, C(7) is bonded in a trigonal planar geometry to one C(11), one C(27), and one C(3) atom. The C(7)-C(11) bond length is 1.40 Å. The C(7)-C(27) bond length is 1.42 Å. In the eighth C site, C(8) is bonded in a trigonal planar geometry to one C(12), one C(28), and one C(4) atom. The C(8)-C(12) bond length is 1.39 Å. The C(8)-C(28) bond length is 1.42 Å. In the ninth C site, C(9) is bonded in a distorted single-bond geometry to one C(13), one C(5), and one H(21) atom. The C(9)-C(13) bond length is 1.40 Å. The C(9)-H(21) bond length is 1.09 Å. In the tenth C site, C(10) is bonded in a distorted trigonal planar geometry to one C(14), one C(6), and one H(22) atom. The C(10)-C(14) bond length is 1.40 Å. The C(10)-H(22) bond length is 1.09 Å. In the eleventh C site, C(11) is bonded in a distorted trigonal planar geometry to one C(15), one C(7), and one H(23) atom. The C(11)-C(15) bond length is 1.40 Å. The C(11)-H(23) bond length is 1.09 Å. In the twelfth C site, C(12) is bonded in a distorted single-bond geometry to one C(16), one C(8), and one H(24) atom. The C(12)-C(16) bond length is 1.40 Å. The C(12)-H(24) bond length is 1.09 Å. In the thirteenth C site, C(13) is bonded in a trigonal planar geometry to one C(17), one C(29), and one C(9) atom. The C(13)-C(17) bond length is 1.40 Å. The C(13)-C(29) bond length is 1.49 Å. In the fourteenth C site, C(14) is bonded in a trigonal planar geometry to one C(10), one C(18), and one C(30) atom. The C(14)-C(18) bond length is 1.40 Å. The C(14)-C(30) bond length is 1.49 Å. In the fifteenth C site, C(15) is bonded in a trigonal planar geometry to one C(11), one C(19), and one C(31) atom. The C(15)-C(19) bond length is 1.40 Å. The C(15)-C(31) bond length is 1.49 Å. In the sixteenth C site, C(16) is bonded in a trigonal planar geometry to one C(12), one C(20), and one C(32) atom. The C(16)-C(20) bond length is 1.40 Å. The C(16)-C(32) bond length is 1.49 Å. In the seventeenth C site, C(17) is bonded in a distorted single-bond geometry to one C(13) and one H(25,28) atom. The C(17)-H(25,28) bond length is 1.09 Å. In the eighteenth C site, C(18) is bonded in a distorted single-bond geometry to one C(14) and one H(26,27) atom. The C(18)-H(26,27) bond length is 1.09 Å. In the nineteenth C site, C(19) is bonded in a distorted single-bond geometry to one C(15) and one H(26,27) atom. The C(19)-H(26,27) bond length is 1.09 Å. In the twentieth C site, C(20) is bonded in a distorted single-bond geometry to one C(16) and one H(25,28) atom. The C(20)-H(25,28) bond length is 1.09 Å. In the twenty-first C site, C(21) is bonded in a distorted single-bond geometry to one C(25) and one H(29) atom. The C(21)-C(25) bond length is 1.41 Å. The C(21)-H(29) bond length is 1.09 Å. In the twenty-second C site, C(22) is bonded in a distorted single-bond geometry to one C(26) and one H(30) atom. The C(22)-C(26) bond length is 1.41 Å. The C(22)-H(30) bond length is 1.09 Å. In the twenty-third C site, C(23) is bonded in a distorted single-bond geometry to one C(27) and one H(31) atom. The C(23)-C(27) bond length is 1.41 Å. The C(23)-H(31) bond length is 1.09 Å. In the twenty-fourth C site, C(24) is bonded in a distorted single-bond geometry to one C(28) and one H(32) atom. The C(24)-C(28) bond length is 1.41 Å. The C(24)-H(32) bond length is 1.09 Å. In the twenty-fifth C site, C(25) is bonded in a trigonal planar geometry to one C(21), one C(33), and one C(5) atom. The C(25)-C(33) bond length is 1.48 Å. In the twenty-sixth C site, C(26) is bonded in a trigonal planar geometry to one C(22), one C(34), and one C(6) atom. The C(26)-C(34) bond length is 1.48 Å. In the twenty-seventh C site, C(27) is bonded in a trigonal planar geometry to one C(23), one C(35), and one C(7) atom. The C(27)-C(35) bond length is 1.48 Å. In the twenty-eighth C site, C(28) is bonded in a trigonal planar geometry to one C(24), one C(36), and one C(8) atom. The C(28)-C(36) bond length is 1.48 Å. In the twenty-ninth C site, C(29) is bonded in a bent 120 degrees geometry to one C(13), one O(13), and one O(9) atom. The C(29)-O(13) bond length is 1.28 Å. The C(29)-O(9) bond length is 1.27 Å. In the thirtieth C site, C(30) is bonded in a bent 120 degrees geometry to one C(14), one O(10), and one O(14) atom. The C(30)-O(10) bond length is 1.27 Å. The C(30)-O(14) bond length is 1.28 Å. In the thirty-first C site, C(31) is bonded in a bent 120 degrees geometry to one C(15), one O(11), and one O(15) atom. The C(31)-O(11) bond length is 1.27 Å. The C(31)-O(15) bond length is 1.28 Å. In the thirty-second C site, C(32) is bonded in a bent 120 degrees geometry to one C(16), one O(12), and one O(16) atom. The C(32)-O(12) bond length is 1.27 Å. The C(32)-O(16) bond length is 1.28 Å. In the thirty-third C site, C(33) is bonded in a trigonal planar geometry to one C(25), one C(37), and one C(53) atom. The C(33)-C(37) bond length is 1.40 Å. The C(33)-C(53) bond length is 1.40 Å. In the thirty-fourth C site, C(34) is bonded in a trigonal planar geometry to one C(26), one C(38), and one C(54) atom. The C(34)-C(38) bond length is 1.40 Å. The C(34)-C(54) bond length is 1.40 Å. In the thirty-fifth C site, C(35) is bonded in a trigonal planar geometry to one C(27), one C(39), and one C(55) atom. The C(35)-C(39) bond length is 1.40 Å. The C(35)-C(55) bond length is 1.40 Å. In the thirty-sixth C site, C(36) is bonded in a trigonal planar geometry to one C(28), one C(40), and one C(56) atom. The C(36)-C(40) bond length is 1.40 Å. The C(36)-C(56) bond length is 1.40 Å. In the thirty-seventh C site, C(37) is bonded in a distorted single-bond geometry to one C(33), one C(41), and one H(33) atom. The C(37)-C(41) bond length is 1.40 Å. The C(37)-H(33) bond length is 1.09 Å. In the thirty-eighth C site, C(38) is bonded in a distorted single-bond geometry to one C(34) and one H(34) atom. The C(38)-H(34) bond length is 1.09 Å. In the thirty-ninth C site, C(39) is bonded in a distorted single-bond geometry to one C(35), one C(43), and one H(35) atom. The C(39)-C(43) bond length is 1.39 Å. The C(39)-H(35) bond length is 1.09 Å. In the fortieth C site, C(40) is bonded in a distorted single-bond geometry to one C(36), one C(44), and one H(36) atom. The C(40)-C(44) bond length is 1.40 Å. The C(40)-H(36) bond length is 1.09 Å. In the forty-first C site, C(41) is bonded in a distorted trigonal planar geometry to one C(37), one C(45), and one H(37) atom. The C(41)-C(45) bond length is 1.39 Å. The C(41)-H(37) bond length is 1.09 Å. In the forty-second C site, C(43) is bonded in a distorted single-bond geometry to one C(39), one C(47), and one H(39) atom. The C(43)-C(47) bond length is 1.39 Å. The C(43)-H(39) bond length is 1.09 Å. In the forty-third C site, C(44) is bonded in a distorted single-bond geometry to one C(40), one C(48), and one H(40) atom. The C(44)-C(48) bond length is 1.39 Å. The C(44)-H(40) bond length is 1.09 Å. In the forty-fourth C site, C(45) is bonded in a distorted single-bond geometry to one C(41), one C(49), and one H(41) atom. The C(45)-C(49) bond length is 1.40 Å. The C(45)-H(41) bond length is 1.09 Å. In the forty-fifth C site, C(46) is bonded in a distorted single-bond geometry to one C(50) and one H(42) atom. The C(46)-C(50) bond length is 1.40 Å. The C(46)-H(42) bond length is 1.09 Å. In the forty-sixth C site, C(47) is bonded in a distorted single-bond geometry to one C(43), one C(51), and one H(43) atom. The C(47)-C(51) bond length is 1.40 Å. The C(47)-H(43) bond length is 1.09 Å. In the forty-seventh C site, C(48) is bonded in a distorted single-bond geometry to one C(44), one C(52), and one H(44) atom. The C(48)-C(52) bond length is 1.40 Å. The C(48)-H(44) bond length is 1.09 Å. In the forty-eighth C site, C(49) is bonded in a trigonal planar geometry to one C(45), one C(53), and one C(57) atom. The C(49)-C(53) bond length is 1.40 Å. The C(49)-C(57) bond length is 1.48 Å. In the forty-ninth C site, C(50) is bonded in a trigonal planar geometry to one C(46), one C(54), and one C(58) atom. The C(50)-C(54) bond length is 1.40 Å. The C(50)-C(58) bond length is 1.48 Å. In the fiftieth C site, C(51) is bonded in a trigonal planar geometry to one C(47), one C(55), and one C(59) atom. The C(51)-C(55) bond length is 1.40 Å. The C(51)-C(59) bond length is 1.48 Å. In the fifty-first C site, C(52) is bonded in a trigonal planar geometry to one C(48), one C(56), and one C(60) atom. The C(52)-C(56) bond length is 1.40 Å. The C(52)-C(60) bond length is 1.48 Å. In the fifty-second C site, C(53) is bonded in a distorted trigonal planar geometry to one C(33), one C(49), and one H(45) atom. The C(53)-H(45) bond length is 1.09 Å. In the fifty-third C site, C(54) is bonded in a distorted trigonal planar geometry to one C(34), one C(50), and one H(46) atom. The C(54)-H(46) bond length is 1.09 Å. In the fifty-fourth C site, C(55) is bonded in a distorted trigonal planar geometry to one C(35), one C(51), and one H(47) atom. The C(55)-H(47) bond length is 1.09 Å. In the fifty-fifth C site, C(56) is bonded in a distorted trigonal planar geometry to one C(36), one C(52), and one H(48) atom. The C(56)-H(48) bond length is 1.09 Å. In the fifty-sixth C site, C(57) is bonded in a trigonal planar geometry to one C(49), one C(61), and one C(77) atom. The C(57)-C(61) bond length is 1.40 Å. The C(57)-C(77) bond length is 1.41 Å. In the fifty-seventh C site, C(58) is bonded in a trigonal planar geometry to one C(50), one C(62), and one C(78) atom. The C(58)-C(62) bond length is 1.40 Å. The C(58)-C(78) bond length is 1.41 Å. In the fifty-eighth C site, C(59) is bonded in a trigonal planar geometry to one C(51), one C(63), and one C(79) atom. The C(59)-C(63) bond length is 1.40 Å. The C(59)-C(79) bond length is 1.41 Å. In the fifty-ninth C site, C(60) is bonded in a trigonal planar geometry to one C(52), one C(64), and one C(80) atom. The C(60)-C(64) bond length is 1.40 Å. The C(60)-C(80) bond length is 1.41 Å. In the sixtieth C site, C(61) is bonded in a distorted trigonal planar geometry to one C(57), one C(65), and one H(49) atom. The C(61)-C(65) bond length is 1.40 Å. The C(61)-H(49) bond length is 1.09 Å. In the sixty-first C site, C(62) is bonded in a distorted trigonal planar geometry to one C(58); one C(66,67); and one H(50,51) atom. The C(62)-C(66,67) bond length is 1.40 Å. The C(62)-H(50,51) bond length is 1.09 Å. In the sixty-second C site, C(63) is bonded in a distorted trigonal planar geometry to one C(59); one C(66,67); and one H(50,51) atom. The C(63)-C(66,67) bond length is 1.39 Å. The C(63)-H(50,51) bond length is 1.09 Å. In the sixty-third C site, C(64) is bonded in a distorted trigonal planar geometry to one C(60), one C(68), and one H(52) atom. The C(64)-C(68) bond length is 1.39 Å. The C(64)-H(52) bond length is 1.09 Å. In the sixty-fourth C site, C(65) is bonded in a distorted single-bond geometry to one C(61); one C(69); and one H(53,55,56) atom. The C(65)-C(69) bond length is 1.40 Å. The C(65)-H(53,55,56) bond length is 1.09 Å. In the sixty-fifth C site, C(66,67) is bonded in a distorted single-bond geometry to one C(62), one C(70), and one H(54) atom. The C(66,67)-C(70) bond length is 1.40 Å. The C(66,67)-H(54) bond length is 1.09 Å. In the sixty-sixth C site, C(68) is bonded in a distorted single-bond geometry to one C(64); one C(72); and one H(53,55,56) atom. The C(68)-C(72) bond length is 1.40 Å. The C(68)-H(53,55,56) bond length is 1.09 Å. In the sixty-seventh C site, C(69) is bonded in a trigonal planar geometry to one C(65), one C(73), and one C(81) atom. The C(69)-C(73) bond length is 1.40 Å. The C(69)-C(81) bond length is 1.49 Å. In the sixty-eighth C site, C(70) is bonded in a trigonal planar geometry to one C(66,67); one C(74); and one C(82) atom. The C(70)-C(74) bond length is 1.40 Å. The C(70)-C(82) bond length is 1.49 Å. In the sixty-ninth C site, C(71) is bonded in a trigonal planar geometry to one C(66,67); one C(75); and one C(83) atom. The C(71)-C(66,67) bond length is 1.40 Å. The C(71)-C(75) bond length is 1.40 Å. The C(71)-C(83) bond length is 1.49 Å. In the seventieth C site, C(72) is bonded in a trigonal planar geometry to one C(68), one C(76), and one C(84) atom. The C(72)-C(76) bond length is 1.40 Å. The C(72)-C(84) bond length is 1.49 Å. In the seventy-first C site, C(73) is bonded in a distorted single-bond geometry to one C(69); one C(77); and one H(57,59) atom. The C(73)-C(77) bond length is 1.39 Å. The C(73)-H(57,59) bond length is 1.09 Å. In the seventy-second C site, C(74) is bonded in a distorted single-bond geometry to one C(70); one C(78); and one H(58,60) atom. The C(74)-C(78) bond length is 1.39 Å. The C(74)-H(58,60) bond length is 1.09 Å. In the seventy-third C site, C(75) is bonded in a distorted single-bond geometry to one C(71); one C(79); and one H(57,59) atom. The C(75)-C(79) bond length is 1.39 Å. The C(75)-H(57,59) bond length is 1.09 Å. In the seventy-fourth C site, C(76) is bonded in a distorted single-bond geometry to one C(72); one C(80); and one H(58,60) atom. The C(76)-C(80) bond length is 1.39 Å. The C(76)-H(58,60) bond length is 1.09 Å. In the seventy-fifth C site, C(77) is bonded in a trigonal planar geometry to one C(57), one C(73), and one C(85) atom. The C(77)-C(85) bond length is 1.49 Å. In the seventy-sixth C site, C(78) is bonded in a trigonal planar geometry to one C(58), one C(74), and one C(86) atom. The C(78)-C(86) bond length is 1.49 Å. In the seventy-seventh C site, C(79) is bonded in a trigonal planar geometry to one C(59), one C(75), and one C(87) atom. The C(79)-C(87) bond length is 1.49 Å. In the seventy-eighth C site, C(80) is bonded in a trigonal planar geometry to one C(60), one C(76), and one C(88) atom. The C(80)-C(88) bond length is 1.49 Å. In the seventy-ninth C site, C(81) is bonded in a bent 120 degrees geometry to one C(69), one O(17), and one O(21) atom. The C(81)-O(17) bond length is 1.27 Å. The C(81)-O(21) bond length is 1.29 Å. In the eightieth C site, C(82) is bonded in a bent 120 degrees geometry to one C(70), one O(18), and one O(22) atom. The C(82)-O(18) bond length is 1.27 Å. The C(82)-O(22) bond length is 1.29 Å. In the eighty-first C site, C(83) is bonded in a bent 120 degrees geometry to one C(71), one O(19), and one O(23) atom. The C(83)-O(19) bond length is 1.27 Å. The C(83)-O(23) bond length is 1.29 Å. In the eighty-second C site, C(84) is bonded in a bent 120 degrees geometry to one C(72), one O(20), and one O(24) atom. The C(84)-O(20) bond length is 1.27 Å. The C(84)-O(24) bond length is 1.29 Å. In the eighty-third C site, C(85) is bonded in a distorted bent 120 degrees geometry to one C(77), one O(25), and one O(29) atom. The C(85)-O(25) bond length is 1.27 Å. The C(85)-O(29) bond length is 1.27 Å. In the eighty-fourth C site, C(86) is bonded in a distorted bent 120 degrees geometry to one C(78), one O(26), and one O(30) atom. The C(86)-O(26) bond length is 1.27 Å. The C(86)-O(30) bond length is 1.27 Å. In the eighty-fifth C site, C(87) is bonded in a distorted bent 120 degrees geometry to one C(79), one O(27), and one O(31) atom. The C(87)-O(27) bond length is 1.27 Å. The C(87)-O(31) bond length is 1.27 Å. In the eighty-sixth C site, C(88) is bonded in a distorted bent 120 degrees geometry to one C(80), one O(28), and one O(32) atom. The C(88)-O(28) bond length is 1.27 Å. The C(88)-O(32) bond length is 1.27 Å. In the eighty-seventh C site, C(89) is bonded in a trigonal planar geometry to one H(61), one O(33), and one O(34) atom. The C(89)-H(61) bond length is 1.12 Å. The C(89)-O(33) bond length is 1.26 Å. The C(89)-O(34) bond length is 1.26 Å. In the eighty-eighth C site, C(90) is bonded in a trigonal planar geometry to one H(62), one O(35), and one O(36) atom. The C(90)-H(62) bond length is 1.12 Å. The C(90)-O(35) bond length is 1.26 Å. The C(90)-O(36) bond length is 1.26 Å. There are fifty-four inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one O(37) atom. The H(1)-O(37) bond length is 0.97 Å. In the second H site, H(2) is bonded in a single-bond geometry to one O(38) atom. The H(2)-O(38) bond length is 0.97 Å. In the third H site, H(3) is bonded in a single-bond geometry to one O(39) atom. The H(3)-O(39) bond length is 0.97 Å. In the fourth H site, H(4) is bonded in a single-bond geometry to one O(40) atom. The H(4)-O(40) bond length is 0.97 Å. In the fifth H site, H(5) is bonded in a single-bond geometry to one O(37) atom. The H(5)-O(37) bond length is 0.98 Å. In the sixth H site, H(6) is bonded in a single-bond geometry to one O(38) atom. The H(6)-O(38) bond length is 0.98 Å. In the seventh H site, H(7) is bonded in a single-bond geometry to one O(39) atom. The H(7)-O(39) bond length is 0.98 Å. In the eighth H site, H(8) is bonded in a single-bond geometry to one O(40) atom. The H(8)-O(40) bond length is 0.98 Å. In the ninth H site, H(9) is bonded in a single-bond geometry to one O(41) atom. The H(9)-O(41) bond length is 0.97 Å. In the tenth H site, H(10) is bonded in a single-bond geometry to one O(42) atom. The H(10)-O(42) bond length is 0.97 Å. In the eleventh H site, H(11) is bonded in a single-bond geometry to one O(43) atom. The H(11)-O(43) bond length is 0.97 Å. In the twelfth H site, H(12) is bonded in a single-bond geometry to one O(44) atom. The H(12)-O(44) bond length is 0.97 Å. In the thirteenth H site, H(13) is bonded in a distorted single-bond geometry to one O(30) and one O(41) atom. The H(13)-O(30) bond length is 1.65 Å. The H(13)-O(41) bond length is 1.00 Å. In the fourteenth H site, H(14) is bonded in a distorted single-bond geometry to one O(29) and one O(42) atom. The H(14)-O(29) bond length is 1.67 Å. The H(14)-O(42) bond length is 1.00 Å. In the fifteenth H site, H(15) is bonded in a distorted single-bond geometry to one O(32) and one O(43) atom. The H(15)-O(32) bond length is 1.65 Å. The H(15)-O(43) bond length is 1.00 Å. In the sixteenth H site, H(16) is bonded in a distorted single-bond geometry to one O(31) and one O(44) atom. The H(16)-O(31) bond length is 1.67 Å. The H(16)-O(44) bond length is 1.00 Å. In the seventeenth H site, H(17) is bonded in a single-bond geometry to one O(45) atom. The H(17)-O(45) bond length is 0.98 Å. In the eighteenth H site, H(18) is bonded in a single-bond geometry to one O(45) atom. The H(18)-O(45) bond length is 0.97 Å. In the nineteenth H site, H(19) is bonded in a single-bond geometry to one O(46) atom. The H(19)-O(46) bond length is 0.97 Å. In the twentieth H site, H(20) is bonded in a single-bond geometry to one O(46) atom. The H(20)-O(46) bond length is 0.97 Å. In the twenty-first H site, H(21) is bonded in a single-bond geometry to one C(9) atom. In the twenty-second H site, H(22) is bonded in a single-bond geometry to one C(10) atom. In the twenty-third H site, H(23) is bonded in a single-bond geometry to one C(11) atom. In the twenty-fourth H site, H(24) is bonded in a single-bond geometry to one C(12) atom. In the twenty-fifth H site, H(25,28) is bonded in a single-bond geometry to one C(17) atom. In the twenty-sixth H site, H(26,27) is bonded in a single-bond geometry to one C(18) atom. In the twenty-seventh H site, H(29) is bonded in a single-bond geometry to one C(21) atom. In the twenty-eighth H site, H(30) is bonded in a single-bond geometry to one C(22) atom. In the twenty-ninth H site, H(31) is bonded in a single-bond geometry to one C(23) atom. In the thirtieth H site, H(32) is bonded in a single-bond geometry to one C(24) atom. In the thirty-first H site, H(33) is bonded in a single-bond geometry to one C(37) atom. In the thirty-second H site, H(34) is bonded in a single-bond geometry to one C(38) atom. In the thirty-third H site, H(35) is bonded in a single-bond geometry to one C(39) atom. In the thirty-fourth H site, H(36) is bonded in a single-bond geometry to one C(40) atom. In the thirty-fifth H site, H(37) is bonded in a single-bond geometry to one C(41) atom. In the thirty-sixth H site, H(39) is bonded in a single-bond geometry to one C(43) atom. In the thirty-seventh H site, H(40) is bonded in a single-bond geometry to one C(44) atom. In the thirty-eighth H site, H(41) is bonded in a single-bond geometry to one C(45) atom. In the thirty-ninth H site, H(42) is bonded in a single-bond geometry to one C(46) atom. In the fortieth H site, H(43) is bonded in a single-bond geometry to one C(47) atom. In the forty-first H site, H(44) is bonded in a single-bond geometry to one C(48) atom. In the forty-second H site, H(45) is bonded in a single-bond geometry to one C(53) atom. In the forty-third H site, H(46) is bonded in a single-bond geometry to one C(54) atom. In the forty-fourth H site, H(47) is bonded in a single-bond geometry to one C(55) atom. In the forty-fifth H site, H(48) is bonded in a single-bond geometry to one C(56) atom. In the forty-sixth H site, H(49) is bonded in a single-bond geometry to one C(61) atom. In the forty-seventh H site, H(50,51) is bonded in a single-bond geometry to one C(62) atom. In the forty-eighth H site, H(52) is bonded in a single-bond geometry to one C(64) atom. In the forty-ninth H site, H(53,55,56) is bonded in a single-bond geometry to one C(65) atom. In the fiftieth H site, H(54) is bonded in a single-bond geometry to one C(66,67) atom. In the fifty-first H site, H(57,59) is bonded in a single-bond geometry to one C(73) atom. In the fifty-second H site, H(58,60) is bonded in a single-bond geometry to one C(74) atom. In the fifty-third H site, H(61) is bonded in a single-bond geometry to one C(89) atom. In the fifty-fourth H site, H(62) is bonded in a single-bond geometry to one C(90) atom. There are forty-six inequivalent O sites. In the first O site, O(1) is bonded in a distorted bent 150 degrees geometry to one Dy(3) and one C(1) atom. In the second O site, O(2) is bonded in a distorted bent 150 degrees geometry to one Dy(4) and one C(2) atom. In the third O site, O(3) is bonded in a distorted bent 150 degrees geometry to one Dy(5) and one C(3) atom. In the fourth O site, O(4) is bonded in a distorted bent 150 degrees geometry to one Dy(6) and one C(4) atom. In the fifth O site, O(5) is bonded in a 2-coordinate geometry to one Dy(1) and one C(1) atom. In the sixth O site, O(6) is bonded in a distorted bent 120 degrees geometry to one Dy(1) and one C(2) atom. In the seventh O site, O(7) is bonded in a 2-coordinate geometry to one Dy(2) and one C(3) atom. In the eighth O site, O(8) is bonded in a distorted bent 120 degrees geometry to one Dy(2) and one C(4) atom. In the ninth O site, O(9) is bonded in a water-like geometry to one Dy(6) and one C(29) atom. In the tenth O site, O(10) is bonded in a bent 120 degrees geometry to one Dy(5) and one C(30) atom. In the eleventh O site, O(11) is bonded in a bent 120 degrees geometry to one Dy(3) and one C(31) atom. In the twelfth O site, O(12) is bonded in a water-like geometry to one Dy(4) and one C(32) atom. In the thirteenth O site, O(13) is bonded in a distorted linear geometry to one Dy(2), one Dy(6), and one C(29) atom. In the fourteenth O site, O(14) is bonded in a distorted linear geometry to one Dy(2) and one C(30) atom. In the fifteenth O site, O(15) is bonded in a distorted linear geometry to one Dy(1) and one C(31) atom. In the sixteenth O site, O(16) is bonded in a distorted linear geometry to one Dy(1), one Dy(4), and one C(32) atom. In the seventeenth O site, O(17) is bonded in a distorted single-bond geometry to one Dy(5) and one C(81) atom. In the eighteenth O site, O(18) is bonded in a distorted single-bond geometry to one Dy(6) and one C(82) atom. In the nineteenth O site, O(19) is bonded in a distorted single-bond geometry to one Dy(3) and one C(83) atom. In the twentieth O site, O(20) is bonded in a distorted single-bond geometry to one Dy(4) and one C(84) atom. In the twenty-first O site, O(21) is bonded in a distorted L-shaped geometry to one Dy(5) and one C(81) atom. In the twenty-second O site, O(22) is bonded in a distorted L-shaped geometry to one Dy(6) and one C(82) atom. In the twenty-third O site, O(23) is bonded in a distorted L-shaped geometry to one Dy(3) and one C(83) atom. In the twenty-fourth O site, O(24) is bonded in a distorted L-shaped geometry to one Dy(4) and one C(84) atom. In the twenty-fifth O site, O(25) is bonded in a 1-coordinate geometry to one Dy(1), one Dy(3), and one C(85) atom. In the twenty-sixth O site, O(26) is bonded in a 1-coordinate geometry to one Dy(1), one Dy(4), and one C(86) atom. In the twenty-seventh O site, O(27) is bonded in a 1-coordinate geometry to one Dy(2), one Dy(5), and one C(87) atom. In the twenty-eighth O site, O(28) is bonded in a 1-coordinate geometry to one Dy(2), one Dy(6), and one C(88) atom. In the twenty-ninth O site, O(29) is bonded in a 3-coordinate geometry to one Dy(1), one C(85), and one H(14) atom. In the thirtieth O site, O(30) is bonded in a 3-coordinate geometry to one Dy(1), one C(86), and one H(13) atom. In the thirty-first O site, O(31) is bonded in a 3-coordinate geometry to one Dy(2), one C(87), and one H(16) atom. In the thirty-second O site, O(32) is bonded in a 3-coordinate geometry to one Dy(2), one C(88), and one H(15) atom. In the thirty-third O site, O(33) is bonded in a distorted bent 120 degrees geometry to one Dy(3) and one C(89) atom. In the thirty-fourth O site, O(34) is bonded in a distorted bent 120 degrees geometry to one Dy(4) and one C(89) atom. In the thirty-fifth O site, O(35) is bonded in a distorted bent 120 degrees geometry to one Dy(5) and one C(90) atom. In the thirty-sixth O site, O(36) is bonded in a distorted bent 120 degrees geometry to one Dy(6) and one C(90) atom. In the thirty-seventh O site, O(37) is bonded in a distorted water-like geometry to one Dy(3), one H(1), and one H(5) atom. In the thirty-eighth O site, O(38) is bonded in a distorted water-like geometry to one Dy(4), one H(2), and one H(6) atom. In the thirty-ninth O site, O(39) is bonded in a distorted water-like geometry to one Dy(5), one H(3), and one H(7) atom. In the fortieth O site, O(40) is bonded in a distorted water-like geometry to one Dy(6), one H(4), and one H(8) atom. In the forty-first O site, O(41) is bonded in a distorted water-like geometry to one Dy(3), one H(13), and one H(9) atom. In the forty-second O site, O(42) is bonded in a distorted water-like geometry to one Dy(4), one H(10), and one H(14) atom. In the forty-third O site, O(43) is bonded in a distorted water-like geometry to one Dy(5), one H(11), and one H(15) atom. In the forty-fourth O site, O(44) is bonded in a distorted water-like geometry to one Dy(6), one H(12), and one H(16) atom. In the forty-fifth O site, O(45) is bonded in a distorted water-like geometry to one Dy(1), one H(17), and one H(18) atom. In the forty-sixth O site, O(46) is bonded in a distorted water-like geometry to one Dy(2), one H(19), and one H(20) atom. Linkers: 8 [O]C(=O)c1ccc(-c2cccc(-c3ccc(C([O])=O)cc3C([O])=O)c2)c(C([O])=O)c1. Metal clusters: 12 [Dy]. The MOF has largest included sphere 6.09 A, density 1.47 g/cm3, surface area 3153.35 m2/g, accessible volume 0.29 cm3/g