NiH8(CO4)2(CH)4(C3H2)2(CH2CO)2 is Indium-derived structured and crystallizes in the triclinic P-1 space group. The structure is zero-dimensional and consists of four 02329_fluka molecules; one 2,3-dimethyl-1,3-butadiene molecule; two dimethyl ether molecules; and one formic acid;nickel;tetrahydrate molecule. Linkers: 2 [O]C(=O)COc1ccc(-c2ccc(OC[C]=O)cc2)cc1. Metal clusters: 1 O.O.O.O.O=[C]O[Ni]O[C]=O. The MOF has largest included sphere 1.77 A, density 1.75 g/cm3, surface area 4287.44 m2/g, accessible volume 0.09 cm3/g