CHPb2C14NH8O10 crystallizes in the triclinic P-1 space group. The structure consists of two 02329_fluka molecules inside a Pb2C14NH8O10 framework. In the Pb2C14NH8O10 framework, there are two inequivalent Pb sites. In the first Pb site, Pb(1) is bonded in a 6-coordinate geometry to one O(6), one O(7), two equivalent O(10), and two equivalent O(2) atoms. The Pb(1)-O(6) bond length is 2.48 Å. The Pb(1)-O(7) bond length is 2.69 Å. There is one shorter (2.72 Å) and one longer (2.78 Å) Pb(1)-O(10) bond length. There is one shorter (2.49 Å) and one longer (2.70 Å) Pb(1)-O(2) bond length. In the second Pb site, Pb(2) is bonded in a 5-coordinate geometry to one O(1), one O(3), one O(5), one O(8), and one O(9) atom. The Pb(2)-O(1) bond length is 2.46 Å. The Pb(2)-O(3) bond length is 2.56 Å. The Pb(2)-O(5) bond length is 2.58 Å. The Pb(2)-O(8) bond length is 2.70 Å. The Pb(2)-O(9) bond length is 2.57 Å. There are fourteen inequivalent C sites. In the first C site, C(1) is bonded in a trigonal planar geometry to one C(13), one C(2), and one C(4) atom. The C(1)-C(13) bond length is 1.39 Å. The C(1)-C(2) bond length is 1.40 Å. The C(1)-C(4) bond length is 1.50 Å. In the second C site, C(2) is bonded in a distorted single-bond geometry to one C(1), one C(7), and one H(1) atom. The C(2)-C(7) bond length is 1.40 Å. The C(2)-H(1) bond length is 1.09 Å. In the third C site, C(3) is bonded in a trigonal planar geometry to one C(13), one C(5), and one C(6) atom. The C(3)-C(13) bond length is 1.40 Å. The C(3)-C(5) bond length is 1.40 Å. The C(3)-C(6) bond length is 1.49 Å. In the fourth C site, C(4) is bonded in a distorted bent 120 degrees geometry to one C(1), one O(3), and one O(4) atom. The C(4)-O(3) bond length is 1.29 Å. The C(4)-O(4) bond length is 1.26 Å. In the fifth C site, C(5) is bonded in a distorted single-bond geometry to one C(3), one C(7), and one H(2) atom. The C(5)-C(7) bond length is 1.40 Å. The C(5)-H(2) bond length is 1.09 Å. In the sixth C site, C(6) is bonded in a distorted bent 120 degrees geometry to one C(3), one O(5), and one O(9) atom. The C(6)-O(5) bond length is 1.28 Å. The C(6)-O(9) bond length is 1.28 Å. In the seventh C site, C(7) is bonded in a trigonal planar geometry to one C(10), one C(2), and one C(5) atom. The C(7)-C(10) bond length is 1.50 Å. In the eighth C site, C(8) is bonded in a distorted single-bond geometry to one C(9) and one H(3) atom. The C(8)-C(9) bond length is 1.40 Å. The C(8)-H(3) bond length is 1.09 Å. In the ninth C site, C(9) is bonded in a trigonal planar geometry to one C(14), one C(15), and one C(8) atom. The C(9)-C(14) bond length is 1.39 Å. The C(9)-C(15) bond length is 1.51 Å. In the tenth C site, C(10) is bonded in a distorted bent 120 degrees geometry to one C(7), one O(2), and one O(7) atom. The C(10)-O(2) bond length is 1.30 Å. The C(10)-O(7) bond length is 1.26 Å. In the eleventh C site, C(11) is bonded in a distorted bent 120 degrees geometry to one N(1) and one H(4) atom. The C(11)-N(1) bond length is 1.36 Å. The C(11)-H(4) bond length is 1.09 Å. In the twelfth C site, C(13) is bonded in a distorted single-bond geometry to one C(1), one C(3), and one H(6) atom. The C(13)-H(6) bond length is 1.09 Å. In the thirteenth C site, C(14) is bonded in a distorted bent 120 degrees geometry to one C(9), one N(1), and one H(7) atom. The C(14)-N(1) bond length is 1.35 Å. The C(14)-H(7) bond length is 1.09 Å. In the fourteenth C site, C(15) is bonded in a distorted bent 120 degrees geometry to one C(9), one O(6), and one O(8) atom. The C(15)-O(6) bond length is 1.27 Å. The C(15)-O(8) bond length is 1.27 Å. N(1) is bonded in a trigonal planar geometry to one C(11), one C(14), and one O(1) atom. The N(1)-O(1) bond length is 1.34 Å. There are eight inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one C(2) atom. In the second H site, H(2) is bonded in a single-bond geometry to one C(5) atom. In the third H site, H(3) is bonded in a single-bond geometry to one C(8) atom. In the fourth H site, H(4) is bonded in a single-bond geometry to one C(11) atom. In the fifth H site, H(6) is bonded in a single-bond geometry to one C(13) atom. In the sixth H site, H(7) is bonded in a single-bond geometry to one C(14) atom. In the seventh H site, H(8) is bonded in a single-bond geometry to one O(1) and one O(10) atom. The H(8)-O(1) bond length is 1.71 Å. The H(8)-O(10) bond length is 1.00 Å. In the eighth H site, H(9) is bonded in a single-bond geometry to one O(10) atom. The H(9)-O(10) bond length is 1.00 Å. There are ten inequivalent O sites. In the first O site, O(1) is bonded in a distorted trigonal planar geometry to one Pb(2), one N(1), and one H(8) atom. In the second O site, O(2) is bonded in a distorted single-bond geometry to two equivalent Pb(1) and one C(10) atom. In the third O site, O(3) is bonded in a distorted single-bond geometry to one Pb(2) and one C(4) atom. In the fourth O site, O(4) is bonded in a single-bond geometry to one C(4) atom. In the fifth O site, O(5) is bonded in a single-bond geometry to one Pb(2) and one C(6) atom. In the sixth O site, O(6) is bonded in a distorted single-bond geometry to one Pb(1) and one C(15) atom. In the seventh O site, O(7) is bonded in a single-bond geometry to one Pb(1) and one C(10) atom. In the eighth O site, O(8) is bonded in a single-bond geometry to one Pb(2) and one C(15) atom. In the ninth O site, O(9) is bonded in a single-bond geometry to one Pb(2) and one C(6) atom. In the tenth O site, O(10) is bonded in a water-like geometry to two equivalent Pb(1), one H(8), and one H(9) atom. Linkers: 2 [O]C(=O)c1ccc[n+]([O-])c1 ,2 [O]C(=O)c1cc(C([O])=O)cc(C([O])=O)c1. Metal clusters: 4 [Pb]. The MOF has largest included sphere 1.86 A, density 3.19 g/cm3, surface area 1981.63 m2/g, accessible volume 0.04 cm3/g