Mn14In9(C55O38)3 crystallizes in the trigonal P-3 space group. There are six inequivalent Mn sites. In the first Mn site, Mn(1) is bonded in a distorted rectangular see-saw-like geometry to one O(27), one O(29), one O(36), and one O(37) atom. The Mn(1)-O(27) bond length is 2.11 Å. The Mn(1)-O(29) bond length is 2.17 Å. The Mn(1)-O(36) bond length is 2.16 Å. The Mn(1)-O(37) bond length is 2.32 Å. In the second Mn site, Mn(2) is bonded in a 3-coordinate geometry to one O(27), one O(30), and one O(33) atom. The Mn(2)-O(27) bond length is 2.11 Å. The Mn(2)-O(30) bond length is 2.19 Å. The Mn(2)-O(33) bond length is 2.11 Å. In the third Mn site, Mn(3) is bonded in a distorted rectangular see-saw-like geometry to one O(28), one O(31), one O(35), and one O(38) atom. The Mn(3)-O(28) bond length is 2.14 Å. The Mn(3)-O(31) bond length is 2.09 Å. The Mn(3)-O(35) bond length is 2.32 Å. The Mn(3)-O(38) bond length is 2.07 Å. In the fourth Mn site, Mn(4) is bonded in a 3-coordinate geometry to one O(28), one O(32), and one O(34) atom. The Mn(4)-O(28) bond length is 2.08 Å. The Mn(4)-O(32) bond length is 2.14 Å. The Mn(4)-O(34) bond length is 2.04 Å. In the fifth Mn site, Mn(5) is bonded in a distorted trigonal non-coplanar geometry to three equivalent O(4) atoms. All Mn(5)-O(4) bond lengths are 2.00 Å. In the sixth Mn site, Mn(6) is bonded in a distorted T-shaped geometry to three equivalent O(3) atoms. All Mn(6)-O(3) bond lengths are 2.00 Å. There are three inequivalent In sites. In the first In site, In(1) is bonded in a distorted hexagonal bipyramidal geometry to one O(10), one O(14), one O(15), one O(16), one O(18), one O(2), one O(6), and one O(7) atom. The In(1)-O(10) bond length is 2.24 Å. The In(1)-O(14) bond length is 2.26 Å. The In(1)-O(15) bond length is 2.21 Å. The In(1)-O(16) bond length is 2.23 Å. The In(1)-O(18) bond length is 2.26 Å. The In(1)-O(2) bond length is 2.23 Å. The In(1)-O(6) bond length is 2.47 Å. The In(1)-O(7) bond length is 2.43 Å. In the second In site, In(2) is bonded in a distorted hexagonal bipyramidal geometry to one O(1), one O(17), one O(19), one O(22), one O(23), one O(24), one O(5), and one O(8) atom. The In(2)-O(1) bond length is 2.41 Å. The In(2)-O(17) bond length is 2.30 Å. The In(2)-O(19) bond length is 2.34 Å. The In(2)-O(22) bond length is 2.22 Å. The In(2)-O(23) bond length is 2.27 Å. The In(2)-O(24) bond length is 2.23 Å. The In(2)-O(5) bond length is 2.27 Å. The In(2)-O(8) bond length is 2.41 Å. In the third In site, In(3) is bonded in a 8-coordinate geometry to one O(11), one O(12), one O(13), one O(20), one O(21), one O(25), one O(26), and one O(9) atom. The In(3)-O(11) bond length is 2.31 Å. The In(3)-O(12) bond length is 2.29 Å. The In(3)-O(13) bond length is 2.60 Å. The In(3)-O(20) bond length is 2.18 Å. The In(3)-O(21) bond length is 2.20 Å. The In(3)-O(25) bond length is 2.38 Å. The In(3)-O(26) bond length is 2.25 Å. The In(3)-O(9) bond length is 2.55 Å. There are fifty-five inequivalent C sites. In the first C site, C(1) is bonded in a distorted bent 150 degrees geometry to one C(2), one O(13), and one O(25) atom. The C(1)-C(2) bond length is 1.48 Å. The C(1)-O(13) bond length is 1.39 Å. The C(1)-O(25) bond length is 1.19 Å. In the second C site, C(2) is bonded in a trigonal planar geometry to one C(1), one C(3), and one C(7) atom. The C(2)-C(3) bond length is 1.45 Å. The C(2)-C(7) bond length is 1.45 Å. In the third C site, C(3) is bonded in a bent 120 degrees geometry to one C(2) and one C(4) atom. The C(3)-C(4) bond length is 1.45 Å. In the fourth C site, C(4) is bonded in a trigonal planar geometry to one C(3), one C(5), and one C(8) atom. The C(4)-C(5) bond length is 1.45 Å. The C(4)-C(8) bond length is 1.45 Å. In the fifth C site, C(5) is bonded in a bent 120 degrees geometry to one C(4) and one C(6) atom. The C(5)-C(6) bond length is 1.45 Å. In the sixth C site, C(6) is bonded in a 3-coordinate geometry to one C(5), one C(7), and one C(9) atom. The C(6)-C(7) bond length is 1.45 Å. The C(6)-C(9) bond length is 1.45 Å. In the seventh C site, C(7) is bonded in a bent 120 degrees geometry to one C(2) and one C(6) atom. In the eighth C site, C(8) is bonded in a bent 120 degrees geometry to one C(4), one O(3), and one O(4) atom. The C(8)-O(3) bond length is 1.23 Å. The C(8)-O(4) bond length is 1.23 Å. In the ninth C site, C(9) is bonded in a 2-coordinate geometry to one C(6), one O(26), and one O(9) atom. The C(9)-O(26) bond length is 1.14 Å. The C(9)-O(9) bond length is 1.53 Å. In the tenth C site, C(10) is bonded in a trigonal planar geometry to one C(20), one C(24), and one C(25) atom. The C(10)-C(20) bond length is 1.37 Å. The C(10)-C(24) bond length is 1.22 Å. The C(10)-C(25) bond length is 1.40 Å. In the eleventh C site, C(11) is bonded in a trigonal planar geometry to one C(18), one C(21), and one C(29) atom. The C(11)-C(18) bond length is 1.50 Å. The C(11)-C(21) bond length is 1.64 Å. The C(11)-C(29) bond length is 1.21 Å. In the twelfth C site, C(12) is bonded in a trigonal planar geometry to one C(24), one C(26), and one C(30) atom. The C(12)-C(24) bond length is 1.49 Å. The C(12)-C(26) bond length is 1.69 Å. The C(12)-C(30) bond length is 1.29 Å. In the thirteenth C site, C(13) is bonded in a distorted bent 120 degrees geometry to one C(35), one O(10), and one O(7) atom. The C(13)-C(35) bond length is 1.46 Å. The C(13)-O(10) bond length is 1.24 Å. The C(13)-O(7) bond length is 1.27 Å. In the fourteenth C site, C(14) is bonded in a distorted bent 120 degrees geometry to one C(34), one O(2), and one O(6) atom. The C(14)-C(34) bond length is 1.35 Å. The C(14)-O(2) bond length is 1.34 Å. The C(14)-O(6) bond length is 1.21 Å. In the fifteenth C site, C(15) is bonded in a bent 120 degrees geometry to one O(1) and one O(5) atom. The C(15)-O(1) bond length is 1.26 Å. The C(15)-O(5) bond length is 1.35 Å. In the sixteenth C site, C(16) is bonded in a trigonal planar geometry to one C(23), one C(28), and one C(29) atom. The C(16)-C(23) bond length is 1.43 Å. The C(16)-C(28) bond length is 1.72 Å. The C(16)-C(29) bond length is 1.28 Å. In the seventeenth C site, C(17) is bonded in a trigonal planar geometry to one C(20), one C(22), and one C(30) atom. The C(17)-C(20) bond length is 1.52 Å. The C(17)-C(22) bond length is 1.68 Å. The C(17)-C(30) bond length is 1.16 Å. In the eighteenth C site, C(18) is bonded in a water-like geometry to one C(11) and one C(19) atom. The C(18)-C(19) bond length is 1.35 Å. In the nineteenth C site, C(19) is bonded in a trigonal planar geometry to one C(18), one C(23), and one C(27) atom. The C(19)-C(23) bond length is 1.22 Å. The C(19)-C(27) bond length is 1.51 Å. In the twentieth C site, C(20) is bonded in a water-like geometry to one C(10) and one C(17) atom. In the twenty-first C site, C(21) is bonded in a bent 120 degrees geometry to one C(11), one O(19), and one O(24) atom. The C(21)-O(19) bond length is 1.24 Å. The C(21)-O(24) bond length is 1.27 Å. In the twenty-second C site, C(22) is bonded in a bent 120 degrees geometry to one C(17), one O(17), and one O(22) atom. The C(22)-O(17) bond length is 1.26 Å. The C(22)-O(22) bond length is 1.28 Å. In the twenty-third C site, C(23) is bonded in a bent 120 degrees geometry to one C(16) and one C(19) atom. In the twenty-fourth C site, C(24) is bonded in a bent 120 degrees geometry to one C(10) and one C(12) atom. In the twenty-fifth C site, C(25) is bonded in a distorted water-like geometry to one C(10), one O(11), and one O(20) atom. The C(25)-O(11) bond length is 1.27 Å. The C(25)-O(20) bond length is 1.29 Å. In the twenty-sixth C site, C(26) is bonded in a bent 120 degrees geometry to one C(12), one O(14), and one O(16) atom. The C(26)-O(14) bond length is 1.19 Å. The C(26)-O(16) bond length is 1.22 Å. In the twenty-seventh C site, C(27) is bonded in a bent 120 degrees geometry to one C(19), one O(12), and one O(21) atom. The C(27)-O(12) bond length is 1.25 Å. The C(27)-O(21) bond length is 1.25 Å. In the twenty-eighth C site, C(28) is bonded in a bent 120 degrees geometry to one C(16), one O(15), and one O(18) atom. The C(28)-O(15) bond length is 1.22 Å. The C(28)-O(18) bond length is 1.16 Å. In the twenty-ninth C site, C(29) is bonded in a bent 120 degrees geometry to one C(11) and one C(16) atom. In the thirtieth C site, C(30) is bonded in a bent 120 degrees geometry to one C(12) and one C(17) atom. In the thirty-first C site, C(31) is bonded in a bent 120 degrees geometry to one O(23) and one O(8) atom. The C(31)-O(23) bond length is 1.35 Å. The C(31)-O(8) bond length is 1.25 Å. In the thirty-second C site, C(32) is bonded in a 4-coordinate geometry to one C(36), one C(37), one C(40), and one C(41) atom. The C(32)-C(36) bond length is 1.52 Å. The C(32)-C(37) bond length is 1.49 Å. The C(32)-C(40) bond length is 1.45 Å. The C(32)-C(41) bond length is 1.46 Å. In the thirty-third C site, C(33) is bonded in a bent 120 degrees geometry to one C(34) and one C(35) atom. The C(33)-C(34) bond length is 1.55 Å. The C(33)-C(35) bond length is 1.47 Å. In the thirty-fourth C site, C(34) is bonded in a 4-coordinate geometry to one C(14), one C(33), one C(46), and one C(47) atom. The C(34)-C(46) bond length is 1.45 Å. The C(34)-C(47) bond length is 1.46 Å. In the thirty-fifth C site, C(35) is bonded in a 4-coordinate geometry to one C(13), one C(33), one C(44), and one C(45) atom. The C(35)-C(44) bond length is 1.40 Å. The C(35)-C(45) bond length is 1.38 Å. In the thirty-sixth C site, C(36) is bonded in a distorted single-bond geometry to one C(32), one C(37), and one C(38) atom. The C(36)-C(37) bond length is 1.08 Å. The C(36)-C(38) bond length is 1.27 Å. In the thirty-seventh C site, C(37) is bonded in a single-bond geometry to one C(32), one C(36), and one C(39) atom. The C(37)-C(39) bond length is 1.46 Å. In the thirty-eighth C site, C(38) is bonded in a distorted trigonal non-coplanar geometry to one C(36), one C(39), and one C(50) atom. The C(38)-C(39) bond length is 1.69 Å. The C(38)-C(50) bond length is 1.64 Å. In the thirty-ninth C site, C(39) is bonded in a distorted trigonal non-coplanar geometry to one C(37), one C(38), and one C(51) atom. The C(39)-C(51) bond length is 1.43 Å. In the fortieth C site, C(40) is bonded in a distorted single-bond geometry to one C(32), one C(41), and one C(43) atom. The C(40)-C(41) bond length is 1.14 Å. The C(40)-C(43) bond length is 1.36 Å. In the forty-first C site, C(41) is bonded in a distorted single-bond geometry to one C(32), one C(40), and one C(42) atom. The C(41)-C(42) bond length is 1.44 Å. In the forty-second C site, C(42) is bonded in a distorted trigonal non-coplanar geometry to one C(41), one C(43), and one C(51) atom. The C(42)-C(43) bond length is 1.72 Å. The C(42)-C(51) bond length is 1.49 Å. In the forty-third C site, C(43) is bonded in a distorted trigonal non-coplanar geometry to one C(40), one C(42), and one C(50) atom. The C(43)-C(50) bond length is 1.45 Å. In the forty-fourth C site, C(44) is bonded in a 3-coordinate geometry to one C(35), one C(45), and one C(54) atom. The C(44)-C(45) bond length is 1.15 Å. The C(44)-C(54) bond length is 1.54 Å. In the forty-fifth C site, C(45) is bonded in a 3-coordinate geometry to one C(35), one C(44), and one C(55) atom. The C(45)-C(55) bond length is 1.41 Å. In the forty-sixth C site, C(46) is bonded in a 3-coordinate geometry to one C(34), one C(47), and one C(54) atom. The C(46)-C(47) bond length is 1.17 Å. The C(46)-C(54) bond length is 1.62 Å. In the forty-seventh C site, C(47) is bonded in a 3-coordinate geometry to one C(34), one C(46), and one C(55) atom. The C(47)-C(55) bond length is 1.51 Å. In the forty-eighth C site, C(48) is bonded in a distorted bent 120 degrees geometry to one C(50), one O(31), and one O(32) atom. The C(48)-C(50) bond length is 1.45 Å. The C(48)-O(31) bond length is 1.19 Å. The C(48)-O(32) bond length is 1.56 Å. In the forty-ninth C site, C(49) is bonded in a distorted water-like geometry to one C(51), one O(29), and one O(30) atom. The C(49)-C(51) bond length is 1.45 Å. The C(49)-O(29) bond length is 1.28 Å. The C(49)-O(30) bond length is 1.64 Å. In the fiftieth C site, C(50) is bonded in a trigonal planar geometry to one C(38), one C(43), and one C(48) atom. In the fifty-first C site, C(51) is bonded in a trigonal planar geometry to one C(39), one C(42), and one C(49) atom. In the fifty-second C site, C(52) is bonded in a 4-coordinate geometry to one C(53), one C(55), one O(34), and one O(38) atom. The C(52)-C(53) bond length is 1.76 Å. The C(52)-C(55) bond length is 1.32 Å. The C(52)-O(34) bond length is 1.61 Å. The C(52)-O(38) bond length is 1.54 Å. In the fifty-third C site, C(53) is bonded in a 2-coordinate geometry to one C(52), one C(54), one O(33), and one O(36) atom. The C(53)-C(54) bond length is 1.28 Å. The C(53)-O(33) bond length is 1.48 Å. The C(53)-O(36) bond length is 1.43 Å. In the fifty-fourth C site, C(54) is bonded in a 4-coordinate geometry to one C(44), one C(46), one C(53), and one C(55) atom. The C(54)-C(55) bond length is 1.75 Å. In the fifty-fifth C site, C(55) is bonded in a distorted trigonal pyramidal geometry to one C(45), one C(47), one C(52), and one C(54) atom. There are thirty-eight inequivalent O sites. In the first O site, O(1) is bonded in a distorted L-shaped geometry to one In(2) and one C(15) atom. In the second O site, O(2) is bonded in a distorted L-shaped geometry to one In(1) and one C(14) atom. In the third O site, O(3) is bonded in a distorted bent 150 degrees geometry to one Mn(6) and one C(8) atom. In the fourth O site, O(4) is bonded in a distorted bent 150 degrees geometry to one Mn(5) and one C(8) atom. In the fifth O site, O(5) is bonded in a distorted L-shaped geometry to one In(2) and one C(15) atom. In the sixth O site, O(6) is bonded in a distorted L-shaped geometry to one In(1) and one C(14) atom. In the seventh O site, O(7) is bonded in a distorted L-shaped geometry to one In(1) and one C(13) atom. In the eighth O site, O(8) is bonded in a distorted single-bond geometry to one In(2) and one C(31) atom. In the ninth O site, O(9) is bonded in a distorted single-bond geometry to one In(3) and one C(9) atom. In the tenth O site, O(10) is bonded in a distorted L-shaped geometry to one In(1) and one C(13) atom. In the eleventh O site, O(11) is bonded in an L-shaped geometry to one In(3) and one C(25) atom. In the twelfth O site, O(12) is bonded in an L-shaped geometry to one In(3) and one C(27) atom. In the thirteenth O site, O(13) is bonded in a distorted single-bond geometry to one In(3) and one C(1) atom. In the fourteenth O site, O(14) is bonded in an L-shaped geometry to one In(1) and one C(26) atom. In the fifteenth O site, O(15) is bonded in an L-shaped geometry to one In(1) and one C(28) atom. In the sixteenth O site, O(16) is bonded in an L-shaped geometry to one In(1) and one C(26) atom. In the seventeenth O site, O(17) is bonded in an L-shaped geometry to one In(2) and one C(22) atom. In the eighteenth O site, O(18) is bonded in an L-shaped geometry to one In(1) and one C(28) atom. In the nineteenth O site, O(19) is bonded in an L-shaped geometry to one In(2) and one C(21) atom. In the twentieth O site, O(20) is bonded in a water-like geometry to one In(3) and one C(25) atom. In the twenty-first O site, O(21) is bonded in a water-like geometry to one In(3) and one C(27) atom. In the twenty-second O site, O(22) is bonded in an L-shaped geometry to one In(2) and one C(22) atom. In the twenty-third O site, O(23) is bonded in a distorted L-shaped geometry to one In(2) and one C(31) atom. In the twenty-fourth O site, O(24) is bonded in an L-shaped geometry to one In(2) and one C(21) atom. In the twenty-fifth O site, O(25) is bonded in a distorted L-shaped geometry to one In(3) and one C(1) atom. In the twenty-sixth O site, O(26) is bonded in an L-shaped geometry to one In(3) and one C(9) atom. In the twenty-seventh O site, O(27) is bonded in a bent 120 degrees geometry to one Mn(1) and one Mn(2) atom. In the twenty-eighth O site, O(28) is bonded in a bent 120 degrees geometry to one Mn(3) and one Mn(4) atom. In the twenty-ninth O site, O(29) is bonded in a distorted single-bond geometry to one Mn(1) and one C(49) atom. In the thirtieth O site, O(30) is bonded in a distorted bent 120 degrees geometry to one Mn(2) and one C(49) atom. In the thirty-first O site, O(31) is bonded in a distorted single-bond geometry to one Mn(3) and one C(48) atom. In the thirty-second O site, O(32) is bonded in a distorted bent 120 degrees geometry to one Mn(4) and one C(48) atom. In the thirty-third O site, O(33) is bonded in a distorted single-bond geometry to one Mn(2) and one C(53) atom. In the thirty-fourth O site, O(34) is bonded in a distorted bent 150 degrees geometry to one Mn(4) and one C(52) atom. In the thirty-fifth O site, O(35) is bonded in a 3-coordinate geometry to one Mn(3) atom. In the thirty-sixth O site, O(36) is bonded in a single-bond geometry to one Mn(1) and one C(53) atom. In the thirty-seventh O site, O(37) is bonded in a 3-coordinate geometry to one Mn(1) atom. In the thirty-eighth O site, O(38) is bonded in a distorted single-bond geometry to one Mn(3) and one C(52) atom. Linkers: 1 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O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O].[O][C]=O.[O][C]=O.[O][C]=O.[O][C]O[In].[O][C]O[In].[O][C]O[In][O].[O][C][O].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In].[O][In]([O])[C]O[In].[O][In][O].[c]1c2c3c4c5c1[C]5[C]4[C]23 ,3 [O]C(=O)[C@]12[C][C@@]3(C([O])=O)[C]4[C]3[C@]35[C]1[C]2[C@]43C([O])([O])C5([O])[O]. Metal clusters: 12 [Mn] ,3 [In] ,3 [C]1O[Mn]2O[C]3O[Mn@](O1)(OO[Mn@]14O[C]O[Mn](O[C]3O1)O4)O2 ,2 [C]1O[Mn]2O[C]O[Mn](O1)O[C]O2. The MOF has largest included sphere 18.31 A, density 0.88 g/cm3, surface area 3310.90 m2/g, accessible volume 0.78 cm3/g