Dy2NiC56H28(NO3)4NiH16(C8N)4(H3(C2O)2)2 is Indium-derived structured and crystallizes in the monoclinic P2_1 space group. The structure is zero-dimensional and consists of four methacrylic acid molecules, two Dy2NiC56H28(NO3)4 clusters, and two NiH16(C8N)4 clusters. In each Dy2NiC56H28(NO3)4 cluster, there are two inequivalent Dy sites. In the first Dy site, Dy(1) is bonded in a 5-coordinate geometry to one O(10), one O(11), one O(3), one O(7), and one O(8) atom. The Dy(1)-O(10) bond length is 2.22 Å. The Dy(1)-O(11) bond length is 2.24 Å. The Dy(1)-O(3) bond length is 2.31 Å. The Dy(1)-O(7) bond length is 2.40 Å. The Dy(1)-O(8) bond length is 2.55 Å. In the second Dy site, Dy(2) is bonded in a distorted pentagonal pyramidal geometry to one O(1), one O(12), one O(15), one O(16), one O(2), and one O(4) atom. The Dy(2)-O(1) bond length is 2.34 Å. The Dy(2)-O(12) bond length is 2.32 Å. The Dy(2)-O(15) bond length is 2.46 Å. The Dy(2)-O(16) bond length is 2.50 Å. The Dy(2)-O(2) bond length is 2.50 Å. The Dy(2)-O(4) bond length is 2.28 Å. Ni(1) is bonded in a rectangular see-saw-like geometry to one N(1), one N(2), one N(3), and one N(4) atom. The Ni(1)-N(1) bond length is 1.93 Å. The Ni(1)-N(2) bond length is 1.93 Å. The Ni(1)-N(3) bond length is 1.94 Å. The Ni(1)-N(4) bond length is 1.96 Å. There are fifty-six inequivalent C sites. In the first C site, C(1) is bonded in a distorted single-bond geometry to one C(2), one C(20), and one N(1) atom. The C(1)-C(2) bond length is 1.41 Å. The C(1)-C(20) bond length is 1.40 Å. The C(1)-N(1) bond length is 1.40 Å. In the second C site, C(2) is bonded in a distorted single-bond geometry to one C(1), one C(3), and one H(1) atom. The C(2)-C(3) bond length is 1.35 Å. The C(2)-H(1) bond length is 0.95 Å. In the third C site, C(3) is bonded in a distorted single-bond geometry to one C(2), one C(4), and one H(2) atom. The C(3)-C(4) bond length is 1.42 Å. The C(3)-H(2) bond length is 0.95 Å. In the fourth C site, C(4) is bonded in a distorted trigonal planar geometry to one C(3), one C(5), and one N(1) atom. The C(4)-C(5) bond length is 1.41 Å. The C(4)-N(1) bond length is 1.38 Å. In the fifth C site, C(5) is bonded in a trigonal planar geometry to one C(21), one C(4), and one C(6) atom. The C(5)-C(21) bond length is 1.49 Å. The C(5)-C(6) bond length is 1.37 Å. In the sixth C site, C(6) is bonded in a distorted trigonal planar geometry to one C(5), one C(7), and one N(2) atom. The C(6)-C(7) bond length is 1.44 Å. The C(6)-N(2) bond length is 1.39 Å. In the seventh C site, C(7) is bonded in a distorted single-bond geometry to one C(6), one C(8), and one H(3) atom. The C(7)-C(8) bond length is 1.35 Å. The C(7)-H(3) bond length is 0.95 Å. In the eighth C site, C(8) is bonded in a distorted single-bond geometry to one C(7), one C(9), and one H(4) atom. The C(8)-C(9) bond length is 1.43 Å. The C(8)-H(4) bond length is 0.95 Å. In the ninth C site, C(9) is bonded in a distorted trigonal planar geometry to one C(10), one C(8), and one N(2) atom. The C(9)-C(10) bond length is 1.39 Å. The C(9)-N(2) bond length is 1.38 Å. In the tenth C site, C(10) is bonded in a trigonal planar geometry to one C(11), one C(28), and one C(9) atom. The C(10)-C(11) bond length is 1.36 Å. The C(10)-C(28) bond length is 1.49 Å. In the eleventh C site, C(11) is bonded in a distorted trigonal planar geometry to one C(10), one C(12), and one N(3) atom. The C(11)-C(12) bond length is 1.42 Å. The C(11)-N(3) bond length is 1.39 Å. In the twelfth C site, C(12) is bonded in a distorted single-bond geometry to one C(11) and one H(5) atom. The C(12)-H(5) bond length is 0.95 Å. In the thirteenth C site, C(13) is bonded in a distorted single-bond geometry to one C(14) and one H(6) atom. The C(13)-C(14) bond length is 1.43 Å. The C(13)-H(6) bond length is 0.95 Å. In the fourteenth C site, C(14) is bonded in a distorted trigonal planar geometry to one C(13), one C(15), and one N(3) atom. The C(14)-C(15) bond length is 1.39 Å. The C(14)-N(3) bond length is 1.41 Å. In the fifteenth C site, C(15) is bonded in a trigonal planar geometry to one C(14), one C(16), and one C(35) atom. The C(15)-C(16) bond length is 1.40 Å. The C(15)-C(35) bond length is 1.49 Å. In the sixteenth C site, C(16) is bonded in a distorted trigonal planar geometry to one C(15), one C(17), and one N(4) atom. The C(16)-C(17) bond length is 1.42 Å. The C(16)-N(4) bond length is 1.38 Å. In the seventeenth C site, C(17) is bonded in a distorted single-bond geometry to one C(16) and one H(7) atom. The C(17)-H(7) bond length is 0.95 Å. In the eighteenth C site, C(18) is bonded in a distorted single-bond geometry to one C(19) and one H(8) atom. The C(18)-C(19) bond length is 1.43 Å. The C(18)-H(8) bond length is 0.95 Å. In the nineteenth C site, C(19) is bonded in a distorted trigonal planar geometry to one C(18), one C(20), and one N(4) atom. The C(19)-C(20) bond length is 1.41 Å. The C(19)-N(4) bond length is 1.38 Å. In the twentieth C site, C(20) is bonded in a trigonal planar geometry to one C(1), one C(19), and one C(42) atom. The C(20)-C(42) bond length is 1.46 Å. In the twenty-first C site, C(21) is bonded in a trigonal planar geometry to one C(22), one C(26), and one C(5) atom. The C(21)-C(22) bond length is 1.42 Å. The C(21)-C(26) bond length is 1.35 Å. In the twenty-second C site, C(22) is bonded in a distorted single-bond geometry to one C(21) and one H(9) atom. The C(22)-H(9) bond length is 0.95 Å. In the twenty-third C site, C(23) is bonded in a distorted single-bond geometry to one C(24) and one H(10,39) atom. The C(23)-C(24) bond length is 1.37 Å. The C(23)-H(10,39) bond length is 0.95 Å. In the twenty-fourth C site, C(24) is bonded in a trigonal planar geometry to one C(23), one C(25), and one C(27) atom. The C(24)-C(25) bond length is 1.34 Å. The C(24)-C(27) bond length is 1.50 Å. In the twenty-fifth C site, C(25) is bonded in a distorted single-bond geometry to one C(24) and one H(11) atom. The C(25)-H(11) bond length is 0.95 Å. In the twenty-sixth C site, C(26) is bonded in a distorted single-bond geometry to one C(21) and one H(12) atom. The C(26)-H(12) bond length is 0.95 Å. In the twenty-seventh C site, C(27) is bonded in a bent 120 degrees geometry to one C(24), one O(1), and one O(2) atom. The C(27)-O(1) bond length is 1.26 Å. The C(27)-O(2) bond length is 1.26 Å. In the twenty-eighth C site, C(28) is bonded in a trigonal planar geometry to one C(10), one C(29), and one C(33) atom. The C(28)-C(29) bond length is 1.38 Å. The C(28)-C(33) bond length is 1.40 Å. In the twenty-ninth C site, C(29) is bonded in a distorted single-bond geometry to one C(28) and one H(13) atom. The C(29)-H(13) bond length is 0.95 Å. In the thirtieth C site, C(30) is bonded in a distorted single-bond geometry to one C(31) and one H(14) atom. The C(30)-C(31) bond length is 1.35 Å. The C(30)-H(14) bond length is 0.95 Å. In the thirty-first C site, C(31) is bonded in a trigonal planar geometry to one C(30), one C(32), and one C(34) atom. The C(31)-C(32) bond length is 1.37 Å. The C(31)-C(34) bond length is 1.49 Å. In the thirty-second C site, C(32) is bonded in a distorted trigonal planar geometry to one C(31), one C(33), and one H(15) atom. The C(32)-C(33) bond length is 1.39 Å. The C(32)-H(15) bond length is 0.95 Å. In the thirty-third C site, C(33) is bonded in a distorted single-bond geometry to one C(28), one C(32), and one H(16) atom. The C(33)-H(16) bond length is 0.95 Å. In the thirty-fourth C site, C(34) is bonded in a distorted bent 120 degrees geometry to one C(31), one O(3), and one O(4) atom. The C(34)-O(3) bond length is 1.26 Å. The C(34)-O(4) bond length is 1.26 Å. In the thirty-fifth C site, C(35) is bonded in a trigonal planar geometry to one C(15), one C(36), and one C(40) atom. The C(35)-C(36) bond length is 1.35 Å. The C(35)-C(40) bond length is 1.38 Å. In the thirty-sixth C site, C(36) is bonded in a distorted single-bond geometry to one C(35) and one H(17) atom. The C(36)-H(17) bond length is 0.95 Å. In the thirty-seventh C site, C(40) is bonded in a distorted single-bond geometry to one C(35) and one H(20) atom. The C(40)-H(20) bond length is 0.95 Å. In the thirty-eighth C site, C(42) is bonded in a trigonal planar geometry to one C(20), one C(43), and one C(47) atom. The C(42)-C(43) bond length is 1.37 Å. The C(42)-C(47) bond length is 1.39 Å. In the thirty-ninth C site, C(43) is bonded in a distorted single-bond geometry to one C(42) and one H(22,25) atom. The C(43)-H(22,25) bond length is 0.95 Å. In the fortieth C site, C(44) is bonded in a distorted single-bond geometry to one C(45) and one H(23) atom. The C(44)-C(45) bond length is 1.37 Å. The C(44)-H(23) bond length is 0.95 Å. In the forty-first C site, C(45) is bonded in a trigonal planar geometry to one C(44), one C(46), and one C(48) atom. The C(45)-C(46) bond length is 1.39 Å. The C(45)-C(48) bond length is 1.51 Å. In the forty-second C site, C(46) is bonded in a distorted single-bond geometry to one C(45) and one H(24) atom. The C(46)-H(24) bond length is 0.95 Å. In the forty-third C site, C(47) is bonded in a distorted single-bond geometry to one C(42) and one H(22,25) atom. The C(47)-H(22,25) bond length is 0.95 Å. In the forty-fourth C site, C(48) is bonded in a distorted bent 120 degrees geometry to one C(45), one O(7), and one O(8) atom. The C(48)-O(7) bond length is 1.26 Å. The C(48)-O(8) bond length is 1.27 Å. In the forty-fifth C site, C(71) is bonded in a distorted single-bond geometry to one C(72) and one H(35) atom. The C(71)-C(72) bond length is 1.43 Å. The C(71)-H(35) bond length is 0.95 Å. In the forty-sixth C site, C(72) is bonded in a trigonal planar geometry to one C(71), one C(73), and one C(75) atom. The C(72)-C(73) bond length is 1.39 Å. The C(72)-C(75) bond length is 1.53 Å. In the forty-seventh C site, C(73) is bonded in a distorted single-bond geometry to one C(72) and one H(36) atom. The C(73)-H(36) bond length is 0.95 Å. In the forty-eighth C site, C(75) is bonded in a distorted bent 120 degrees geometry to one C(72), one O(10), and one O(9) atom. The C(75)-O(10) bond length is 1.24 Å. The C(75)-O(9) bond length is 1.25 Å. In the forty-ninth C site, C(78) is bonded in a distorted single-bond geometry to one C(79) and one H(10,39) atom. The C(78)-C(79) bond length is 1.42 Å. The C(78)-H(10,39) bond length is 0.95 Å. In the fiftieth C site, C(79) is bonded in a trigonal planar geometry to one C(78), one C(80), and one C(82) atom. The C(79)-C(80) bond length is 1.42 Å. The C(79)-C(82) bond length is 1.48 Å. In the fifty-first C site, C(80) is bonded in a distorted single-bond geometry to one C(79) and one H(40) atom. The C(80)-H(40) bond length is 0.95 Å. In the fifty-second C site, C(82) is bonded in a bent 120 degrees geometry to one C(79), one O(11), and one O(12) atom. The C(82)-O(11) bond length is 1.26 Å. The C(82)-O(12) bond length is 1.26 Å. In the fifty-third C site, C(92) is bonded in a distorted single-bond geometry to one C(93) and one H(48) atom. The C(92)-C(93) bond length is 1.40 Å. The C(92)-H(48) bond length is 0.95 Å. In the fifty-fourth C site, C(93) is bonded in a trigonal planar geometry to one C(92), one C(94), and one C(96) atom. The C(93)-C(94) bond length is 1.41 Å. The C(93)-C(96) bond length is 1.49 Å. In the fifty-fifth C site, C(94) is bonded in a distorted single-bond geometry to one C(93) and one H(49) atom. The C(94)-H(49) bond length is 0.95 Å. In the fifty-sixth C site, C(96) is bonded in a distorted bent 120 degrees geometry to one C(93), one O(15), and one O(16) atom. The C(96)-O(15) bond length is 1.25 Å. The C(96)-O(16) bond length is 1.27 Å. There are four inequivalent N sites. In the first N site, N(1) is bonded in a trigonal planar geometry to one Ni(1), one C(1), and one C(4) atom. In the second N site, N(2) is bonded in a trigonal planar geometry to one Ni(1), one C(6), and one C(9) atom. In the third N site, N(3) is bonded in a trigonal planar geometry to one Ni(1), one C(11), and one C(14) atom. In the fourth N site, N(4) is bonded in a trigonal planar geometry to one Ni(1), one C(16), and one C(19) atom. There are twenty-six inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one C(2) atom. In the second H site, H(2) is bonded in a single-bond geometry to one C(3) atom. In the third H site, H(3) is bonded in a single-bond geometry to one C(7) atom. In the fourth H site, H(4) is bonded in a single-bond geometry to one C(8) atom. In the fifth H site, H(5) is bonded in a single-bond geometry to one C(12) atom. In the sixth H site, H(6) is bonded in a single-bond geometry to one C(13) atom. In the seventh H site, H(7) is bonded in a single-bond geometry to one C(17) atom. In the eighth H site, H(8) is bonded in a single-bond geometry to one C(18) atom. In the ninth H site, H(9) is bonded in a single-bond geometry to one C(22) atom. In the tenth H site, H(10,39) is bonded in a single-bond geometry to one C(23) atom. In the eleventh H site, H(11) is bonded in a single-bond geometry to one C(25) atom. In the twelfth H site, H(12) is bonded in a single-bond geometry to one C(26) atom. In the thirteenth H site, H(13) is bonded in a single-bond geometry to one C(29) atom. In the fourteenth H site, H(14) is bonded in a single-bond geometry to one C(30) atom. In the fifteenth H site, H(15) is bonded in a single-bond geometry to one C(32) atom. In the sixteenth H site, H(16) is bonded in a single-bond geometry to one C(33) atom. In the seventeenth H site, H(17) is bonded in a single-bond geometry to one C(36) atom. In the eighteenth H site, H(20) is bonded in a single-bond geometry to one C(40) atom. In the nineteenth H site, H(22,25) is bonded in a single-bond geometry to one C(43) atom. In the twentieth H site, H(23) is bonded in a single-bond geometry to one C(44) atom. In the twenty-first H site, H(24) is bonded in a single-bond geometry to one C(46) atom. In the twenty-second H site, H(35) is bonded in a single-bond geometry to one C(71) atom. In the twenty-third H site, H(36) is bonded in a single-bond geometry to one C(73) atom. In the twenty-fourth H site, H(40) is bonded in a single-bond geometry to one C(80) atom. In the twenty-fifth H site, H(48) is bonded in a single-bond geometry to one C(92) atom. In the twenty-sixth H site, H(49) is bonded in a single-bond geometry to one C(94) atom. There are twelve inequivalent O sites. In the first O site, O(1) is bonded in a distorted single-bond geometry to one Dy(2) and one C(27) atom. In the second O site, O(2) is bonded in a distorted L-shaped geometry to one Dy(2) and one C(27) atom. In the third O site, O(3) is bonded in a distorted bent 120 degrees geometry to one Dy(1) and one C(34) atom. In the fourth O site, O(4) is bonded in a linear geometry to one Dy(2) and one C(34) atom. In the fifth O site, O(7) is bonded in a distorted single-bond geometry to one Dy(1) and one C(48) atom. In the sixth O site, O(8) is bonded in a distorted single-bond geometry to one Dy(1) and one C(48) atom. In the seventh O site, O(9) is bonded in a single-bond geometry to one C(75) atom. In the eighth O site, O(10) is bonded in a bent 150 degrees geometry to one Dy(1) and one C(75) atom. In the ninth O site, O(11) is bonded in a bent 150 degrees geometry to one Dy(1) and one C(82) atom. In the tenth O site, O(12) is bonded in a distorted bent 120 degrees geometry to one Dy(2) and one C(82) atom. In the eleventh O site, O(15) is bonded in a distorted single-bond geometry to one Dy(2) and one C(96) atom. In the twelfth O site, O(16) is bonded in a distorted single-bond geometry to one Dy(2) and one C(96) atom. In each NiH16(C8N)4 cluster, Ni(2) is bonded in a rectangular see-saw-like geometry to one N(5), one N(6), one N(7), and one N(8) atom. The Ni(2)-N(5) bond length is 1.93 Å. The Ni(2)-N(6) bond length is 1.95 Å. The Ni(2)-N(7) bond length is 1.94 Å. The Ni(2)-N(8) bond length is 1.94 Å. There are thirty-two inequivalent C sites. In the first C site, C(49) is bonded in a distorted single-bond geometry to one C(50), one C(68), and one N(5) atom. The C(49)-C(50) bond length is 1.42 Å. The C(49)-C(68) bond length is 1.42 Å. The C(49)-N(5) bond length is 1.36 Å. In the second C site, C(50) is bonded in a distorted single-bond geometry to one C(49), one C(51), and one H(26) atom. The C(50)-C(51) bond length is 1.35 Å. The C(50)-H(26) bond length is 0.95 Å. In the third C site, C(51) is bonded in a distorted single-bond geometry to one C(50), one C(52), and one H(27) atom. The C(51)-C(52) bond length is 1.44 Å. The C(51)-H(27) bond length is 0.95 Å. In the fourth C site, C(52) is bonded in a distorted trigonal planar geometry to one C(51), one C(53), and one N(5) atom. The C(52)-C(53) bond length is 1.39 Å. The C(52)-N(5) bond length is 1.39 Å. In the fifth C site, C(53) is bonded in a trigonal planar geometry to one C(52), one C(54), and one C(69) atom. The C(53)-C(54) bond length is 1.38 Å. The C(53)-C(69) bond length is 1.52 Å. In the sixth C site, C(54) is bonded in a distorted trigonal planar geometry to one C(53), one C(55), and one N(6) atom. The C(54)-C(55) bond length is 1.44 Å. The C(54)-N(6) bond length is 1.38 Å. In the seventh C site, C(55) is bonded in a distorted single-bond geometry to one C(54) and one H(28) atom. The C(55)-H(28) bond length is 0.95 Å. In the eighth C site, C(56) is bonded in a distorted single-bond geometry to one C(57) and one H(29) atom. The C(56)-C(57) bond length is 1.44 Å. The C(56)-H(29) bond length is 0.95 Å. In the ninth C site, C(57) is bonded in a distorted trigonal planar geometry to one C(56), one C(58), and one N(6) atom. The C(57)-C(58) bond length is 1.38 Å. The C(57)-N(6) bond length is 1.40 Å. In the tenth C site, C(58) is bonded in a trigonal planar geometry to one C(57), one C(59), and one C(76) atom. The C(58)-C(59) bond length is 1.39 Å. The C(58)-C(76) bond length is 1.50 Å. In the eleventh C site, C(59) is bonded in a distorted trigonal planar geometry to one C(58), one C(60), and one N(7) atom. The C(59)-C(60) bond length is 1.43 Å. The C(59)-N(7) bond length is 1.40 Å. In the twelfth C site, C(60) is bonded in a distorted single-bond geometry to one C(59) and one H(30) atom. The C(60)-H(30) bond length is 0.95 Å. In the thirteenth C site, C(61) is bonded in a distorted single-bond geometry to one C(62) and one H(31) atom. The C(61)-C(62) bond length is 1.42 Å. The C(61)-H(31) bond length is 0.95 Å. In the fourteenth C site, C(62) is bonded in a distorted trigonal planar geometry to one C(61), one C(63), and one N(7) atom. The C(62)-C(63) bond length is 1.40 Å. The C(62)-N(7) bond length is 1.38 Å. In the fifteenth C site, C(63) is bonded in a trigonal planar geometry to one C(62), one C(64), and one C(83) atom. The C(63)-C(64) bond length is 1.38 Å. The C(63)-C(83) bond length is 1.48 Å. In the sixteenth C site, C(64) is bonded in a distorted trigonal planar geometry to one C(63), one C(65), and one N(8) atom. The C(64)-C(65) bond length is 1.47 Å. The C(64)-N(8) bond length is 1.39 Å. In the seventeenth C site, C(65) is bonded in a distorted single-bond geometry to one C(64) and one H(32) atom. The C(65)-H(32) bond length is 0.95 Å. In the eighteenth C site, C(66) is bonded in a distorted single-bond geometry to one C(67) and one H(33) atom. The C(66)-C(67) bond length is 1.45 Å. The C(66)-H(33) bond length is 0.95 Å. In the nineteenth C site, C(67) is bonded in a distorted trigonal planar geometry to one C(66), one C(68), and one N(8) atom. The C(67)-C(68) bond length is 1.37 Å. The C(67)-N(8) bond length is 1.39 Å. In the twentieth C site, C(68) is bonded in a trigonal planar geometry to one C(49), one C(67), and one C(90) atom. The C(68)-C(90) bond length is 1.49 Å. In the twenty-first C site, C(69) is bonded in a trigonal planar geometry to one C(53), one C(70), and one C(74) atom. The C(69)-C(70) bond length is 1.35 Å. The C(69)-C(74) bond length is 1.40 Å. In the twenty-second C site, C(76) is bonded in a trigonal planar geometry to one C(58), one C(77), and one C(81) atom. The C(76)-C(77) bond length is 1.40 Å. The C(76)-C(81) bond length is 1.42 Å. In the twenty-third C site, C(70) is bonded in a distorted single-bond geometry to one C(69) and one H(34) atom. The C(70)-H(34) bond length is 0.95 Å. In the twenty-fourth C site, C(74) is bonded in a distorted single-bond geometry to one C(69) and one H(37) atom. The C(74)-H(37) bond length is 0.95 Å. In the twenty-fifth C site, C(77) is bonded in a distorted single-bond geometry to one C(76) and one H(38) atom. The C(77)-H(38) bond length is 0.95 Å. In the twenty-sixth C site, C(81) is bonded in a distorted single-bond geometry to one C(76) and one H(41) atom. The C(81)-H(41) bond length is 0.95 Å. In the twenty-seventh C site, C(83) is bonded in a trigonal planar geometry to one C(63), one C(84), and one C(88) atom. The C(83)-C(84) bond length is 1.42 Å. The C(83)-C(88) bond length is 1.37 Å. In the twenty-eighth C site, C(84) is bonded in a distorted single-bond geometry to one C(83) and one H(42) atom. The C(84)-H(42) bond length is 0.95 Å. In the twenty-ninth C site, C(88) is bonded in a distorted single-bond geometry to one C(83) and one H(45) atom. The C(88)-H(45) bond length is 0.95 Å. In the thirtieth C site, C(90) is bonded in a trigonal planar geometry to one C(68), one C(91), and one C(95) atom. The C(90)-C(91) bond length is 1.44 Å. The C(90)-C(95) bond length is 1.42 Å. In the thirty-first C site, C(91) is bonded in a distorted single-bond geometry to one C(90) and one H(47) atom. The C(91)-H(47) bond length is 0.95 Å. In the thirty-second C site, C(95) is bonded in a distorted single-bond geometry to one C(90) and one H(50) atom. The C(95)-H(50) bond length is 0.95 Å. There are four inequivalent N sites. In the first N site, N(5) is bonded in a distorted trigonal planar geometry to one Ni(2), one C(49), and one C(52) atom. In the second N site, N(6) is bonded in a trigonal planar geometry to one Ni(2), one C(54), and one C(57) atom. In the third N site, N(7) is bonded in a trigonal planar geometry to one Ni(2), one C(59), and one C(62) atom. In the fourth N site, N(8) is bonded in a trigonal planar geometry to one Ni(2), one C(64), and one C(67) atom. There are sixteen inequivalent H sites. In the first H site, H(45) is bonded in a single-bond geometry to one C(88) atom. In the second H site, H(28) is bonded in a single-bond geometry to one C(55) atom. In the third H site, H(47) is bonded in a single-bond geometry to one C(91) atom. In the fourth H site, H(29) is bonded in a single-bond geometry to one C(56) atom. In the fifth H site, H(30) is bonded in a single-bond geometry to one C(60) atom. In the sixth H site, H(31) is bonded in a single-bond geometry to one C(61) atom. In the seventh H site, H(50) is bonded in a single-bond geometry to one C(95) atom. In the eighth H site, H(26) is bonded in a single-bond geometry to one C(50) atom. In the ninth H site, H(32) is bonded in a single-bond geometry to one C(65) atom. In the tenth H site, H(33) is bonded in a single-bond geometry to one C(66) atom. In the eleventh H site, H(34) is bonded in a single-bond geometry to one C(70) atom. In the twelfth H site, H(27) is bonded in a single-bond geometry to one C(51) atom. In the thirteenth H site, H(37) is bonded in a single-bond geometry to one C(74) atom. In the fourteenth H site, H(38) is bonded in a single-bond geometry to one C(77) atom. In the fifteenth H site, H(41) is bonded in a single-bond geometry to one C(81) atom. In the sixteenth H site, H(42) is bonded in a single-bond geometry to one C(84) atom. Linkers: 1 [O]C(=O)c1ccc(cc1)C1=C2C=CC3=[N]2[Ni@@]24n5c1ccc5C(=C1[N]2=C(C=C1)C(=c1n4c(=C3c2ccc(cc2)C(=O)O)cc1)c1ccc(cc1)C(=O)[O])c1ccc(cc1)C(=O)[O] ,1 O=[C]c1ccc(cc1)C1=C2C=CC3=[N]2[Ni@]24n5c1ccc5C(=C1[N]2=C(C=C1)C(=c1n4c(=C3c2ccc(cc2)C(=O)[O])cc1)c1ccc(cc1)C(=O)O)c1ccc(cc1)C(=O)[O] ,2 [O]C(=O)c1ccc(cc1)C1=C2C=CC3=[N]2[Ni@]24n5c1ccc5C(=C1[N]2=C(C=C1)C(=c1n4c(=C3c2ccc(cc2)C(=O)[O])cc1)c1ccc(cc1)C(=O)[O])c1ccc(cc1)C(=O)O. Metal clusters: 2 O=[C]O[Dy]12(O[C]O1)O[C]O[Dy]13(O[C]O2)(O[C]O1)O[C]O3. RCSR code: rtl. The MOF has largest included sphere 5.98 A, density 1.30 g/cm3, surface area 3891.33 m2/g, accessible volume 0.29 cm3/g