text:
Mad Dog Moonlight Paperback
by Pauline Fisk
Mad Dog Moonlight is only a young boy when he is picked up by the police on a lonely Welsh mountain road with a baby in his arms, and nothing from his past except the memory of the name his mother gave him, and a silver-topped walking cane upon which is engraved a secret word.
Fostered by a local family, the Lewises, Mad Dog is renamed 'Ryan', but he struggles to accept this most ordinary of names and families.
He longs to find the answer to who he is and what happened to his parents - and so sets off on an extraordinary adventure to uncover the lost secrets in his life.
From the streets of Aberystwyth to the lonely hillocks of Plynlimon Mountain, Mad Dog encounters hidden adversaries and unexpected allies in a thrilling journey to discover just who he really is.
- Format: Paperback
- Pages: 256 pages
- Publisher: Bloomsbury Publishing PLC
- Publication Date: 02/02/2009
- Category: General
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Review by sirfurboy
Pauline Fisk writes strange books. She is not alone in this, and she is not alone in writing strange books very well! So I don't hold the strangeness against her. This story follows a boy who turns up in Aberystwyth with his brother knowing only that his name is Mad Dog Moonlight, and that his brother is Elvis Preseli (he is about 5 years old at this point). Unsurprisingly his foster parents are less than thrilled with this name, and he is given the name Ryan Lewis instead. We see the boy's struggles as he grows up with the mystery of what happened to his parents hanging over him. His only possession to remind him of his parents is his ffon (Welsh for a staff) with its strange inscription. He refuses adoption as he does not want to be stolen from his parents, but the foster family continue to foster him. Eventually the falls hotel at Devil's Bridge is inherited by the family and the focus of the story shifts from Aberystwyth to the length of the Rheidol valley and the mountain of Plynlimon. This leads into a magical mystery steeped in the legends that surround this place, and ultimately to a kind of resolution of the mystery.But this is Pauline Fisk, so that resolution still leaves you asking questions, and thinking about what the book says to you. Some readers will conclude it and put it down and that will be the end of it. Others will consider its themes and enjoy it more for that.This book is actually set where I live. I did not buy it for that reason - it was a surprise to read the word "Aberystwyth" in the book, but that added to my enjoyment of it I think. On the other hand, it also took a few things away as occasionally I was aware the geography did not quite match the flow of the story (although Pauline Fisk is obviously familiar with the area as she describes much of it exactly as it is).Some things she plays with deliberately. There are no houses in the harbour gap in Aberystwyth, although some back onto it. Indeed, the house that could be number 3 - Ryan's fictional home - is a guesthouse that used to be owned by a family who foster children! Elsewhere I could slot real people into the story, but that rather spoils it. Ultimately its a work of fiction, and a very good one.
Also by Pauline Fisk | View all


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This property has been removed by the agent. It may be sold or temporarily removed from the market
3 bedroom terraced house for saleGainsborough Gardens, Edgware, Middlesex, HA8
Property Description
Key features
- Family home
- Terraced house
- Secluded rear garden with patio area
- Good decorative order
- Fitted kitchen
- Located on tree lined avenue
- Gas central heating
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A three bedroom mid terrace family house in a quiet residential road with two reception rooms off street parking to rear and is chain free.The property comprises two double bedrooms and a single room bathroom wc and a fitted kitchen . The property further benefits from double glazing and gas fired central heating.
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Our client is a leading Financial Institution in Kenya. They wish to recruit a highly competent individual to fill the position of ICT Manager.
The sought after individual should have excellent work ethics, be result oriented and a team player.
Job Ref: MN 7108
Purpose: Reporting to General Manager Operations, the incumbent will be responsible for leading, directing, overseeing and ensuring effectiveness and continuous operation of the organization's Information Technology Systems in order to achieve efficiency and reliability.
The incumbent will be the Head of ICT.
Job Profile
- Developing, maintaining and reviewing ICT Policy and procedures which supports its needs and strategic objectives.
- Evaluate technology developments and ensuring that the organization has appropriate, effective, efficient and up to date ICT systems.
- Ensuring confidentiality, integrity and availability of ICT systems.
- Design and implement controls and procedures that ensure accuracy and reliability in Data capture, Data processing and Dissemination of information.
- Design and implement information security procedures based on standard best practice and Corporate ICT security policies covering information system applications and infrastructure.
- Responsible for developing processes and assigning resources to provide support to all users in a timely manner.
- Managing, monitoring and reviewing the performance of all ICT supply contracts to ensure that the agreed standards and performance criteria are met.
- Preparing and managing annual ICT budget in a view to ensuring value for money is achieved.
- Review, develop and implement an ICT Strategy that is aligned to overall business strategy of the organization.
- Responsible for Planning and designing of disaster recovery plans to ensure service continuity in case of a disaster.
Person Profile
- Applicants should be holders of a Master's and a Bachelor's degree in Computer Science / Information Systems or related fields from a recognized university.
- Applicants should have certification of CISA, CCNA/CCNP, MCSE, MCSD, PMP, DB administration or other ICT related professional qualifications.
- At least 6 years' experience with at least 3 years of which should have been at Manager level overseeing relevant functions.
- Knowledge of operations in the financial services sector and application of technology in this sector is desirable.
- Proven knowledge of ERP systems an added advantage.
Email your application including your CV and application letter indicating your current or past salary and your expected remuneration to [email protected] so as to reach us by 4pm, 28th October 2016.


text:
Girls' Lacrosse
Saints' Jenkins Marks Milestones
Thursday, June 12, 2008
St. Stephen's/St. Agnes Coach Kathy Jenkins recorded her 500th career victory last month during the Saints' run to another Virginia Independent Schools title, a milestone achievement for a coach who has become a respected presence in the Washington area, across the country and on the international lacrosse stage.
When the Saints defeated Episcopal, 19-3, in the VIS semifinals, Jenkins was presented with flowers and balloons, and her players put on T-shirts celebrating victory No. 500, a culmination of 32 years guiding one of the nation's elite lacrosse programs. The following day, the Saints capped a 26-0 season with a win over Collegiate of Richmond in the final. They ended the season ranked No. 1 in The Post's Top 10.
Jenkins's success at the Alexandria school is unrivaled in this region. Her teams have won 20 league titles, including the past 14 straight Independent School League crowns, and gone undefeated five times. Her career record is 501-41-9.
"One of the reasons for Kathy's wonderful success is that she works 24-7, 365 days a year," said Maggie Vaughan, who played for Jenkins from 1984 to '86 and was a two-year all-American at Harvard. "She never stops learning. She calls college coaches, former players. If she sees something [new] on TV, she asks somebody. She still goes to clinics to this day. She is a wonderful ambassador for the game."
Jenkins was recognized for her 500th win during the U.S. Lacrosse Women's Division National Tournament in Baltimore last month. Both she and Phyllis Kilgore, the longtime Radnor (Pa.) High coach who also earned her 500th win this season, were on the field coaching in the tournament's all-star game for high school seniors. Jenkins is a member of the U.S. National Lacrosse Hall of Fame's Potomac and Virginia chapters, and is a lock to be inducted into the National Hall of Fame in Baltimore once her coaching career is finished.
Jenkins, 57, came to all-girls St. Agnes School as a physical education teacher in 1971 (it merged with St. Stephen's in 1991). She started the girls' lacrosse program, along with Alix Fellows, in 1976. Fellows, 74, is still involved with the team.
Jenkins never played lacrosse as a girl. She grew up playing basketball in Erie, Pa., formerly coached the Saints' varsity basketball team and continues to coach the middle school teams.
"I knew some drills to do from basketball and Alix knew the catch-and-throw drills and that's how we started the program." Jenkins said.
Over the years, Jenkins has sent hundreds of players on to college lacrosse teams. Nine of her seniors from this year's squad will play at Division I schools next year, and 10 players from the 2007 team were freshmen on Division I rosters this spring.
"They bought into the Saints program and the attitude that I brought into it," Jenkins said. "Basic skills -- good throwing and catching, good stick skills, good defensive positioning and good team offense."
Saints All-Met Kelly Austin, one of the nation's most-recruited juniors, has known Jenkins since she started at St. Stephen's/St. Agnes as a kindergartener. Jenkins also coached Austin as a middle school basketball player.
"I grew up with a lot of respect for her," Austin said. "She teaches you. We learn how to be great lacrosse players and how to be a great person, with sportsmanship. It's an honor to play for her. She coaches in life and sports."


text:
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I have one of Katara coming up


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Our church family invites you to join us in worship and see why we believe Fletcher First Baptist is a great place to call home. We want to love you, pray for you and encourage you during your earthly pilgrimage.
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|Publication number
|Publication type
|Publication date
|Jul 6, 1971
|Filing date
|Apr 9, 1968
|Priority date
|Apr 9, 1968
|Publication number
|James Plakunov
|Original Assignee
|Eastman Kodak Co
|Export Citation
|BiBTeX, EndNote, RefMan
|Referenced by (32), Classifications (15)
|External Links: USPTO, USPTO Assignment, Espacenet
United States Patent U.S. Cl. 96-50 13 Claims ABSTRACT OF THE DISCLOSURE Photographic elements such as, for example, X-ray film, comprising a support, one or more photographic silver halide layers, and one or more protective overcoat layers and a composition of matter which has utility in such overcoat layers are disclosed. The photographic elements are characterized by having a good combination of photographic properties such as, for example, sensitivity and contrast, resistance to abrasion and low haze; and are more particularly characterized in the use of at least one overcoat layer having the disclosed composition comprising gelatin, and at least one other hydrophilic colloid and finely divided colloidal silica or silica gel having an average particle size below 50 millimicrons.
BACKGROUND OF THE INVENTION Field of the invention This invention relates to photographic materials and their preparation. In another aspect, it relates to a composition of matter which has been found to be particularly desirable as a protective overcoat layer for silver halide emulsion layers in photographic elements. This invention also relates to photographic elements which have one or more of such overcoat layers. In another embodiment, the invention relates to an improved X-ray film having overcoat layers comprising the composition.
The prior art The use of gelatin, a hydrophilic colloid, as the binding agent or vehicle in photographic silver halide emulsions and elements is well known. Attempts have been made to substitute various synthetic and natural materials for all or a part of the gelatin to improve certain photographic and physical properties. However, improvement in one property is generally achieved at the expense of another and often more important property. For example, the use of gelatin and at least one other hydrophilic colloid as the vehicle or binding agent in a silver halide emulsion layer increases the covering power, thus yielding a higher density upon development for the same amount of silver per unit area. Such layers do not have good abrasion resistance and must therefore usually be coated with an overcoat layer. It has also been found that overcoat layers, containing gelatin and mixtures of gelatin and other hydrophilic colloids are suitable for this purpose. I have disclosed the concept of adding hydrophilic colloids to the gelatin vehicle or binding agent in either or both the silver halide emulsion layer or the overcoat layer and a specific application of this concept is shown in my US. application Ser. No. 506,831 filed Nov. 18, 1965. Elements of the type disclosed in the aforementioned application have improved resistance to abrasion particularly when processed in automatic processing equipment, for example, of the type described in Russell and Kunz U.S. Pats. 3,147,090 issued Sept. 1, 1964, and 3,025,779 issued Mar. 20, 1962. The need for increased resistance, such as is afforded by the addition of at least two other colloids besides gelatin to the overcoat layer, is particularly acute where the element is to be processed by such machines because of the 3,591,379 Patented July 6, 1971 great amount of roller contact in such machines and also because the higher temperatures under which such machines operate causes a softening of the gelatin layers. However, the addition of hydrophilic colloids to the gelatin vehicle, whether in the emulsion layer or overcoat layer, produces an undesirable increase in haze in that layer which renders the processed element or film more difficult to read. This haze can be ascribed to a light scattering within that layer and/or at the interfaces of that layer.
The prior art has attempted to solve this problem by the use of heavy gelatin overcoatsz such as taught by US. Pat. 3,05 8,826 of Meerkamper, Bank and Umberger, issued Oct. 16, 1962. The overcoat solution of the prior art does reduce the amount of haze but unfortunately creates a new problem since the use of such coats requires a substantial increase in the amount of time required to dry the processed unit. This is, of course, particularly objectionable in photographic elements which, because of the particular photographic materials used, are designed for and/ or require rapid processing. This heavy overcoat is particularly objectionable in X-ray film designed for machine processing since one of the primary functions of such machines is to decrease processing time.
It would, therefore, be highly desirable to provide the art with photographic elements having a layer or layers containing gelatin and at least one, and for best results at least two, other hydrophilic colloidsand thus possessing good photographic properties, abrasion resistance, and also low haze-which do not require an increase in processing time.
In an aspect of the invention of this application, such elements are obtained by the use of an overcoat layer comprising gelatin, at least one other hydrophilic colloid, and colloidal silica having an average particle size below 50 millimicrons. The addition of coarse particulate materials including silica to gelatin vehicles as inert matting agents is known to the art. However, the silica used for this purpose has a particle size on the order of 500 millimicrons and increases rather than decreases haze.
It is also known to the art to add small particle size silica to gelatin emulsions and overcoat layers-but not to overcoat layers comprising gelatin and at least one other hydrophilic colloid-as antistatic agents; note, for example, US. Pat. 3,053,662 of Mackey and Rice, issued Sept. 11, 1962.
OBJECTS AND SUMMARY It is, therefore, an object of the invention to provide photographic elements having good photographic properties, resistance to abrasion, and low haze, which can be rapidly processed and also to provide means for obtaining such elements. It is a further object to provide X-ray film having such photographic and physical properties which can be rapidly processed.
It is a still further object of the invention to provide a composition of matter comprising gelatin and at least one other hydrophilic colloid and finely divided colloidal silica or silica gel which can be used 'as an overcoat layer in such elements or X-ray film to achieve low haze without requiring an increase in processing time.
It is another object of the invention to provide photographic elements having at least one layer comprising gelatin and a hydrophilic colloid which is 'a carboxymethylated protein and having at least one overcoat layer containing gelatin and at least one other hydrophilic colloid and finely divided colloidal silica or silica gel. It is still a further object to provide such photographic elements in which said layer comprising carboxymethylated pnotein comprises another hydrophilic colloid which is a water-soluble vinyl polymer.
Additional objects will be disclosed and will become apparent, and in part obvious, from the following description and the appended claims.
SUMMARY In accordance with my invention, I have found that the above and other objectives can be attained by the use of an overcoat layer comprising gelatin and at least one other hydrophilic colloid and finely divided silica gel or colloidal silica having an average particle size below 50 millimicrons.
In summary, the overcoat composition of my invention comprises gelatin, a second hydnophilic colloid, and colloidal silica or silica gel in a weight ratio of 0.05 to 0.7 gram of the secondhydrophilic colloid per gram of gelatin and 0.05 to 2 grams of colloidal silica per gram of gelatin. For best results, the quantity of colloidal silica should be in the range of from 0.2 to 0.5 gram of colloidal silica per gram of gelatin. It should, of course, be appreciated that the overcoat composition is applied to the silver halide or other layer, dispersed within a volatile solvent or carrier, usually water, and that such dispersions are encompassed by the invention.
In summary, the photographic element of the invention comprises a support, one or more silver halide layers covering either side or both sides of the support, and one or more protective overcoat layers of the invention covering at least one of said silver halide layers and usually at least all of the silver halide layers which would otherwise form the exterior surface of the photographic element. In a further embodiment of the invention, at least one of the layers comprises as a second hydrophilic colloid in addition to gelatin a carboxymethylated protein and in a still further embodiment of the invention at least one of the layers comprises in addition to gelatin both a carboxymethylated protein and a water-soluble vinyl polymer.
DESCRIPTION OF THE INVENTION AND PREFERRED EMBODIMENTS In practicing the instant invention, finely divided silica gel or colloidal silica is added to an overcoat composition comprising gelatin and at least one other hydrophilic colloid. I have found that such an addition surprisingly results in the production of a low haze photographic element having a good combination of photographic properties and abrasion resistance and which does not require an increase in processing time.
The overcoat composition of the invention can be conveniently prepared by admixing colloidal silica or silica gel to a solvent dispersion, usually an aqueous dispersion, of gelatin and at least one other hydrophilic colloid in a sufficient quantity, based on the quantity of dry gelatin, to provide from 0.05 to 2 grams and for best results from 0.20 to 0.5 gram of silica gel or colloidal silica per gram of gelatin (dry basis). It must be stressed that in order for the silica gel or colloidal silica to be effective in reducing haze it must have an average particle size below 50 millimicrons. This is necessary because coarse particlesized silica will not reduce haze and will in many cases actually increase the amount of light scattering and thus resultin an increase in haze rather than a decrease. In practicing the invention, any of the silica gels or colloidal silicas can be used so long as it possesses the required particle size. For purposes of simplicity, the haze reducing agent will hereafter and in the claims be referred to as colloidal silicathis should be taken as referring to any of the silica family having the required particle size regardless of the degree of hydration. One form of colloidal silica which is particularly suitable in the practice of the invention is the modified (by the chemical bonding through oxygen atoms of an amphoteric metal, such as aluminum, to silicon atoms in the surface of the silica particle) form described in US. Pat. 2,892,797 of Alexander and Iler issued June 30, 1959, and sold under the 4 trademark Ludox AM by E. I. du Bont de Nemours and Company.
Considering the photographic element of the invention in greater detail, such elements comprise (1) a support, (2) one or more photographic (silver halide) layers, and (3) one or more protectve overcoat layers. The photographic element can also contain other auxiliary layers such as are generally found in photographic elements, for example, subbing layers, antihalation layers, etc.
The particular support material used in the invention is not critical though desirably the support material should be firm, stable, inert, transparent, and preferably flexible. The following materials are suitable support materials: cellulose nitrate film, cellulose ester film, polyvinyl acetal film, polystyrene film, polyethylene terephthalate film and other polyester film as well as glass, paper, metal, wood and the like. Supports such as paper which are coated with a-olefin polymers, particularly polymers of a-olefins containing two 101 more carbon atoms, as exemplified by polyethylene, polypropylene, ethylenebutene copolymers, and the like, give good results. The above materials are, of course, only explanatory and not limiting, as other materials having the desired properties can be used. Further, it is contemplated that additional suitable support materials will be developed in the future. As before mentioned, the support can be coated on either or both sides.
Any of the gelatin photographic silver halide emulsions can be employed in practicing this invention, including, for example, photographic silver halide emulsions used in X-ray and camera films and the like. Suitable photographic emulsions contain silver halides such as silver chloride, silver bromide, silver bromoiodide, silver chloroiodide, silver chlorobromide and the like. Particularly good results are obtained with silver bromoiodide emulsions in which the average grain size of the silver bromoiodide crystals is in the range of about 0.5 to about 5 microns.
The photographic emulsions used in the elements described herein can be chemically sensitized with compounds of the sulfur group, noble metal salts such as gold salts, reduction sensitized with reducing agents, and combinations of these.
The photographic silver halide emulsions can also contain additional additives, particularly those known to be beneficial in photographic emulsions. For example, the emulsion can contain spee increasing compounds, for ex ample, onium salts, such as quaternary ammonium or ternary sulfonium salts, polyalkylene glycols, thioethers, and the like. The photographic silver halide emulsions can be stabilized with mercury compounds, azeindenes, quaternary benzothiazolium compounds, hydroxy substituted aromatic compounds, and the like.
The photographic silver halide elements described herein can contain absorbing dyes in the emulsion layer or in an auxiliary layer such as a layer coated between the support and the emulsion layer or the absorbing dyes can be included in both the emulsion and the auxiliary layer. These elements can also contain coarse inert particles such as those often employed as matting agents in photographic elements. Suitable materials of his type include, for example, particles of silicon dioxide, glass, stare, polymethyl methacrylate, and the like. Such inert particles are often included in an emulsion layer and/or auxiliary layers coated over and/or under an emulsion propionates of the type described in U.S. Pat. 3,133,816 of Ben-Ezra issued May 19, 1964. The emulsions and photographic elements described herein can contain incorporated developing agents such as polyhydroxy benzenes, aminophenols and 1,3-pyrazolidones. The photographic emulsions can also contain spectral sensitizers such as cyanines, merocyanines, complex (trinuclear) cyanines and complex (trinuclear) merocyanines, styryls and hemicyanines. These emulsions can be blue sensitive emulsions or they can be orthochromatic, panchromatic or X-ray emulsions.
Considering now the emulsion layer and protective overcoat layer together for purposes of describing the binding agent or vehicle which is used in each and which is basically the same with the exception of the particular additives used in each.
The binding agent or vehicle employed in the overcoat layers of this invention and also desirably in the silver halide emulsion comprises gelatin which is a hydrophilic colloid, and at least one hydrophilic colloid other than gelatin in the protective overcoat. The second hydrophilic colloid usually is present at a concentration of about to about 70% by weight based on the gelatin (dry basis) used in the binding agent. One of the hydrophilic colloids which can be conveniently employed for this purpose is a carboxymethylated protein. carboxymethylated proteins which can be employed in the practice of this invention include those described in U.S. Pat. 3,011,890 of Gates et al. issued Dec. 5, 1961. Some of the naturally occurring amino containing vegetable and animal proteins which can be carboxymethylated and used in practicing this invention include, for example, soybean protein, casein, globulin, and the like. The carboxymethylation of such proteins can be conveniently accomplished by reaction upon the protein with an alpha halo fatty acid such as bromoacetic acid at a pH of 9-12, such as is obtained by the presence of an alkaline buifer material in the reaction mass. The degree of carboxymethylation is subject to variation but will usually be in the range of about 5 to about 25% by weight. Many proteins such as gelatin can ordinarily be carboxymethylated without any prior treatment and used in practicing this invention. However, some proteins contain naturally occurring sulfur compounds which are desirably destroyed or removed by oxidation prior to carboxymethylation. A suitable method which can be for this purpose is treatment with hydrogen peroxide as described in U.S. Pat. 2,691,582 of Lowe and Gates issued Oct. 12, 1954. As already indicated, the carboxymethylated protein can be used in combination with a diiferent hydrophilic colloid other than gelatin. In the preferred case, the combination of hydrophilic colloids other than gelatin is a mixture of a carboxymethylated protein, e.g., carboxymethylated casein, with a water-soluble vinyl polymer, e.g., polyacrylamide.
As noted above, in practicing this invention, preferably a third ingredient of the binding agent is a hydrophilic colloid which is different from both the gelatin and the carboxymethylated protein. This hydrophilic colloid should not contain substantially any free amino or carboxy groups and be compatible With gelatin. The preferred hydrophilic colloid which is difierent from both the gelatin and the carboxymethylated protein is preferabl a water-soluble vinyl polymer such as a water soluble polyacrylamide of the type described in U.S. Pat. 3,271,158 of Allentofl and Minsk issued Sept. 6, 1966. While particularly efiicacious results are obtained with water-soluble polyacrylamide, other hydrophilic colloids can be used in the binding agent with carboxymethylated protein and gelatin. Such other hydrophilic colloids which can be employed with gelatin and the carboxymethylated protein and with or in place of the preferred polyacrylamide, include any of the hydrophilic water-permeable colloids, particularly the materials generally employed in the preparation of photographic silver halide emulsions as binding materials or vehicles, as exemplified by colloidal albumin, cellulose derivatives, synthetic resins, particularly water-soluble vinyl polymers and the like. Specific examples include water-soluble polymers such as polysaccharides, e.g., dextran, as disclosed in U.S. Pat. 3,063,838 of Jennings issued Nov. 13, 1962; vinyl polymers, e.g., poly-N-vinyl pyrrolidones, as disclosed in U.S. Pat. 3,043,- 697 of Forsgard issued July 10, 1962; polyvinyl alcohol derivatives, e.g., acid derivatives such as succinoylated polyvinyl alcohol, as described in U.S. Pat. 3,165,412 of Minsk and Abel issued Jan. 12, 1965; proteins, protein derivatives, as described in U.S. Pat. 2,852,382 of Illingsworth, Dann and Gates issued Sept. 16, 1958; cellulose derivatives, e.g., hydroxyethyl cellulose, as disclosed in U.S. Pat. 3,003,878 of Illingsworth and Minsk issued Oct. 10, 1961; and like compounds.
Also the emulsion and/or overcoat layer can contain hydrophilic colloids which are acrylic interpolymers, i.e., those interpolymers prepared from polymerizable acrylic monomers containing the characteristic acrylic group Such polymers are conveniently prepared by the interpolymerization of an acrylic monomer with at least one dissimilar monomer which can be another acrylic monomer or some other dilferent polymerizable ethylenically unsaturated monomer. Preferably these acrylic interpolyrners are compatible with gelatin and have a T g of less than 20 C. (Tg can be calculated by differential thermal analysis as disclosed in Techniques and Methods of Polymer Evaluation, Volume 1, Marcel Dekker Inc., New York, 1966.) A similar increase in physical and photographic properties is not achieved when polymers having a Tg of above about 20 C. are employed in the emulsions. Interpolymers which can be used comprise units of an alkyl acrylate such as, for example, methyl acrylate, ethyl acrylate, propyl acrylate, butyl acrylates (e.g., n-butyl or t-butyl acrylates), amyl acrylates, hexyl acrylates and the like. Acrylic interpolymers containing units of acrylic acid or a sulfoester acrylate are especially useful. Typical polymers of this type are copoly(butyl acrylate-acrylic acid), copoly(methyl acrylate-acrylic acid), copoly(ethyl acrylate-acrylic acid), copoly(butyl acrylate-sulfopropyl acrylate) and the like. High ratios of solubilizing groups, such as the acrylic acid groups or the sulfoester groups produce a more soluble solution type polymer with respect to water carrier solvents. Mixtures of the more soluble solution type polymers and the latex polymers can be used, if desired, to achieve the desired emulsion characteristics. The acrylic interpolymer generally comprises at least 25% to about 75% by weight of the binder vehicle for the emulsion and from about 75 to about 25 by weight gelatin of the total binder.
The silver halide layers, gelatin overcoat or other layers in the photographic elements of this invention can also contain plasticizers or lubricating materials such as long chain fatty acids, silicone resins, N-alkyl B amino propionates, palmityl palmitate, and the like. Further, the emulsion layers and other layers present in photographic elements made according to this invention can be hardened with any suitable hardener such as aldehyde hardeners, aziridine hardeners, hardeners which are derivatives of dioxane, oxypolysaccharides such as oxystarch, oxy plant gums, inorganic hardeners such as. chromium salts, hardeners having reactive vinyl groups such as the vinyl sulfonyl ethers and the like.
The photographic element is prepared in the conventional manner by coating the support with the emulsion and overcoat layers in the sequence required to give the desired photographic element layer combination. It should be noted that the particular sequence is not critical to the invention and can be varied in any manner to give the particular combination dictated by the use to which the element is to be put.
The gelatin overcoats of this invention are particularly efiective when used with medical X-ray films having emulsion layers containing about 300-600 milligrams of silver per square foot and about 100-600 milligrams of hydrophilic colloid per square foot. The characteristics of processed materials of this type are improved to a considerable degree when such materials containing the overcoats of this invention are processed through roller transport processors, particularly when hardening developers are used as described in Barnes and Rees US. application Ser. No. 561,265, filed June 28, 1966.
Further, although, as is evident from the above, the silver halide layer will be usually applied as what is referred to by the art as an emulsion, it can also be applied by other means, such as, for example, by vapor deposition.
A further understanding of the invention can be had from the following examples.
EXAMPLE 1 This example illustrates the reduction in the haze which can be obtained in a photographic element comprising a support, silver halide emulsion layer, and an overcoat layer comprising gelatin and at least one other hydrophilic colloid, by the addition of finely divided colloidal silica to said overcoat layer. In this example, a coarse grain silver bromo-iodide used in medical X-ray film is coated on a polyethylene terephthalate film support at a coverage of 470 milligrams per square foot. Based on the weight of silver, the emulsion contains 100 grams gelatin, 11 grams carboxymethyl casein (a hydrophilic colloid), and 22 grams of polyacrylamide per gram mole of silver. For purposes of comparison, samples are then taken of the silver emulsion coated film and each sample is then respectively coated with an overcoat layer, at the same coverage, having the composition set forth below in Table I. The samples are then exposed on an intensity sensitometer and then processed in an automatic processing machine of the type described in US. Pat. 3,147,090 of Russell and Kunz issued Sept. 1, 1964, using a hardening developer of the type described in US. Pat. 3,232,761 of Allen and Burness issued Feb. 1, 196 6, with a total processing time of 7 minutes. The process samples are then tested for haze .(percent of light scatter). The results of these tests are summarized in the following Table 1.
1B of Example 1, but using a coarse silica, having an average particle size of 500 millimicrons, in place of the colloidal silica. The sample is then'exposed, processed and tested for haze in the same manner as in Example 1. This sample is observed to possess not only more haze than sample 113 but also more haze than sample 1A (i.e'., the sample not containing silica).
In addition to producing processed coatings having low haze, the colloidal silica containing overcoat layers of the invention also have good coatability and produce photographic materials having increased speed, improved abrasion resistance, improved resistance to water spotting during processing, reduced tackiness, improved hardness, increased electrical conductivity and reduced electrical charging when in contact with X-ray intensifying screens.
Although the invention has been described in consider} able detail with reference to certain preferred embodiments thereof, it will be understood that variations and modifications can be effected without departing from the spirit and scope of the invention as described hereinbefore and as set forth in the appended claims.
I claim:
1. In a photographic element comprising a support, at least one silver halide layer, and at least one overcoat layer protecting the exterior surface of at least one silver halide layer which is furthermost from said support, the improvement wherein at least one overcoat layer comprises gelatin and at least one other hydrophilic colloid and colloidal silica having an average particle size below millimicrons, said colloidal silica being present in a weight ratio range with respect to gelatin of from about 0.05 to about 2 grams of colloidal silica per gram of gelatin (dry basis).
2. The element of claim 1 wherein at least one of said other hydrophilic colloids is a carboxymethylated protein.
3. The element of claim 2 where the carboxymethylated protein is present in a concentration of from 0.05 to 0.7 gram per gram of gelatin.
4. The element of claim 3 wherein the carboxymethylated protein is carboxymethyl casein.
5. The element of claim 2 wherein said other hydrophilic colloid also comprises a water-soluble vinyl polymer.
6. The element of claim 2 wherein one of said other TABLE I Percent Overcoat composition (dry coverage, mg./lt. haze decrease Carboxy- Haze from ad Colloidal l methyl Polyaeryl- (percent dition of silica, Gelatin, casein, amide, light colloidal Sample mgJft. nag/ft. mgJit. mg./1t. scatter) silica 1A 91 13 13 24. 6 36 91 13 l3 l4. 8 40 2A 91 38 31. 3 36 91 38 27. 9 11 A 91 38 20. 3 36 91 38 14. 4 29 and Iler, issued June 30, 1959,
From the above table it is readily apparent that the addition of colloidal silica to the overcoat layer produces an advantageous reduction in haze, especially so where the overcoat layer in addition to gelatin contains two other hydrophilic colloids (e.g., carboxymethyl casein and polyacrylamide). Further, although the silver halide emulsion layer used for the above samples also contains, in addition to gelatin, carboxymethyl casein and polyacrylamide, similar results are obtained where the silver halide layer contains only a single hydrophilic colloid (e.g., gelatin).
Similar reductions in haze are obtained with gelatinsilica overcoat layers containing additional hydrophilic colloids other than carboxymethyl casein and/or polyacrylamide.
EXAMPLE 2 An additional sample is prepared following the same having an average particle size less than 50 millimlcrons and sold under the trademark Ludox AM by E. I. du Pont de N emours dz O0.
hydrophilic colloids also comprises a water-soluble acrylic interpolymer and wherein said acrylic interpolymer is present in a concentration of from about 25 percent to about percent based on gelatin.
7. The element of claim 1 wherein said weight ratio range of colloidal silica is from about 0.2 to 0.5 gram of colloidal silica per gram of gelatin.
8. The photographic element of claim 1 wherein the support is coated on both sides with at least one silver halide layer.
9. The phototgraphic element of claim 1 wherein the support material is an inert, firm, flexible, stable, transparent material selected from the group consisting of cellulose acetates and polyethylene terephthalates.
10. The photographic element of claim 1 wherein the silver halide layer comprises gelatin, carboxymethylated procedure and with the same composition as with sample 75 casein and polyaerylamide.
11. In an X-ray element comprising a support, at least one silver halide layer on each side of said support, and wherein at least one overcoat layer protects the exterior surface of the silver halide layer on each side of said support which layer is :Eurthermost from said support; the improvement wherein at least one overcoat layer comprises gelatin and at least one other hydrophilic colloid and colloidal silica having an average particle size below 50 millimicrons, said colloidal silica being present in a weight ratio range with respect to gelatin of from about 0.05 to about 2 grams of colloidal silica per gram of gelatin (dry basis), and wherein at least one silver halide layer on each side of said support comprises gelatin, carboxymethylated casein and polyacrylamide.
12. The X-ray element of claim 11 wherein at least one auxiliary layer is interposed between at least one of said silver halide layers furthermost from said support and an overcoat layer protecting that silver halide layer.
13. The X-ray element of claim 11 wherein said silver 10 halide layers comprise silver bromoiodide and wherein each side of said element has a silver coverage of about from 300 to 600 milligrams per square foot.
References Cited UNITED STATES PATENTS NORMAN G. TORCHIN, Primary Examiner M. F. KELLEY, Assistant Examiner US Cl. X.R. 9667, 87
|Citing Patent
|Filing date
|Publication date
|Jul 17, 1972
|Jun 11, 1974
|Eastman Kodak Co
|Photographic element and process of developing
|Apr 23, 1974
|Apr 15, 1975
|Fuji Photo Film Co Ltd
|Method of forming photographic images
|Jul 17, 1973
|Jul 22, 1975
|Asahi Chemical Ind
|Photosensitive element comprising photopolymerizable layer and protective layer
|Feb 14, 1974
|Dec 2, 1975
|Fuji Photo Film Co Ltd
|Method for rapidly forming photographic images
|Jun 25, 1974
|Jun 15, 1976
|Eastman Kodak Company
|Silver halide element containing an organic semiconductor
|Feb 2, 1976
|May 24, 1977
|Eastman Kodak Company
|Organic semiconductors used in photoconductor element
|Feb 2, 1976
|May 24, 1977
|Eastman Kodak Company
|Organic semiconductor compositions
|Feb 2, 1976
|May 24, 1977
|Eastman Kodak Company
|Organic semiconductor element
|Dec 29, 1975
|Sep 13, 1977
|Agfa-Gevaert N.V.
|Method of coating multi-layer graphic film
|May 16, 1975
|Nov 1, 1977
|Fuji Photo Film Co., Ltd.
|Layers used to prevent reticulation in photographic elements
|Mar 24, 1978
|Feb 26, 1980
|Fuji Photo Film Co., Ltd.
|Antiadhesive photographic materials and method of improving antiadhesive property of photographic light-sensitive materials
|Oct 11, 1977
|Nov 4, 1980
|Fuji Photo Film Co., Ltd.
|Photographic photosensitive element with protective layer and image forming method using same
|Jun 4, 1979
|Apr 28, 1981
|Fuji Photo Film Co., Ltd.
|Method for preventing adhesion of silver halide photographic light-sensitive material
|Sep 13, 1977
|May 5, 1981
|Minnesota Mining And Manufacturing Company
|Light sensitive materials with fluorinated polymer antistats
|Aug 1, 1980
|Nov 3, 1981
|Eastman Kodak Company
|Photographic element having overcoating of ionic polyester in hydrophilic colloid
|Mar 16, 1981
|Aug 24, 1982
|Eastman Kodak Company
|Two-sheet diffusion transfer elements
|Oct 16, 1981
|Aug 16, 1983
|Konishiroku Photo Industry Co., Ltd.
|Silver halide photosensitive photographic material
|May 28, 1987
|Oct 11, 1988
|Fuji Photo Film Co., Ltd.
|Silver halide photographic material containing a silica containing overlayer and specific hydrazine derivatives
|Apr 19, 1990
|Feb 4, 1992
|Agfa-Gevaert Aktiengesellschaft
|Photographic silver halide element with protective layer
|May 1, 1990
|Apr 14, 1992
|Eastman Kodak Company
|Photographic element having both a filter dye layer and a matte layer
|Dec 17, 1992
|Mar 14, 1995
|Diafoil Hoescht Company Limited
|Radiation sensitized paper
|Oct 6, 1993
|May 16, 1995
|Polaroid Corporation
|Image-receiving element for diffusion transfer photographic film products
|Jun 28, 1996
|May 27, 1997
|Polaroid Corporation
|Image-receiving element with particle containing overcoat for diffusion transfer film products
|Jan 8, 1993
|Mar 16, 1999
|Imation Corp.
|Infrared sensitive photographic elements
|Mar 26, 2003
|Jan 27, 2004
|Eastman Kodak Company
|Radiographic imaging assembly with blue-sensitive film
|Mar 26, 2003
|Feb 3, 2004
|Eastman Kodak Company
|Blue spectrally sensitized film for radiography, imaging assembly and method
|Mar 26, 2003
|Feb 3, 2004
|Eastman Kodak Company
|Blue-sensitive film for radiography with reduced dye stain
|Mar 26, 2003
|Feb 3, 2004
|Eastman Kodak Company
|Blue-sensitive film for radiography and imaging assembly and method
|May 29, 2003
|Feb 3, 2004
|Eastman Kodak Company
|Blue-sensitive film for radiography and imaging assembly and method
|Dec 16, 2005
|Jul 20, 2006
|Fuji Photo Film B.V.
|Ink-jet recording medium
|Apr 3, 2006
|Oct 5, 2006
|Fuji Photo Film B.V.
|Recording medium
|Apr 3, 2006
|Oct 5, 2006
|Fuji Photo Film B.V.
|Recording medium
|U.S. Classification
|430/502, 430/537, 430/950, 430/966, 430/539, 430/961
|International Classification
|Cooperative Classification
|European Classification


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Udaipur, Tripura, Feb 19 (UNI) Prime Minister Manmohan Singh today reiterated that the UPA Government was fully committed to the uplift of the Northeast and working for the betterment of the poor and backward.
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For more information on enrollment with our Commercial Agriculture Program please see below. You will be added to our mailing list to receive event notices and publications/e-alerts specific to your needs. Two ways to enroll:
Complete this printable enrollment form and send to our office along with the enrollment fee.
1. https://reg.cce.cornell.edu/2017-Ag-Enrollment_251.
2. Fill out an enrollment form at https://www.surveymonkey.com/r/2017-Ag-Enrollment or use the printable form above.
For more information contact Carrie at 845-340-3990 x311 or email email@example.com.
Note: If you do not wish to enroll but do want to be added to our mailing list, please fill out the form here: https://www.surveymonkey.com/r/Ag-Program-Mailing-List.
What is Ag Enrollment?
Becoming a member of the Cornell Cooperative Extension of Ulster County Commercial Agriculture Program helps to support our agriculture programs for farmers, land owners and people interested in supporting a vibrant farm industry in Ulster County. Benefits of Ag Enrollment to your farm or family:
*Enrollment in the CCE Ulster County Agriculture Program does not enroll you in ENYCHP, our regional fruit and vegetable program, funded in part by CCE Ulster County, which offers ENYCHP enrollees timely commodity-specific newsletters and e-alerts. For more information on that program visit http://enych.cce.cornell.edu/.
CCE Ulster County strives to make programs accessible regardless of ability to pay. If you are an Ulster County commercial fruit or vegetable farmer, and cannot afford the enrollment fee for ENYCHP, contact CCE Ulster County directly at (845) 340-3990.
Last updated May 26, 2017


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On Thu, Aug 03, 2017 at 10:10:55AM -0400, Mikulas Patocka wrote: > That dm-crypt commit that uses bio integrity payload came 3 months before > 7c20f11680a441df09de7235206f70115fbf6290 and it was already present in > 4.12.
And on it's own that isn't an argument if your usage is indeed wrong, and that's why we are having this discussion. > The patch 7c20f11680a441df09de7235206f70115fbf6290 changes it so that > bio->bi_end_io is not changed and bio_integrity_endio is called directly > from bio_endio if the bio has integrity payload. The unintended > consequence of this change is that when a request with integrity payload > is finished and bio_endio is called for each cloned bio, the verification > routine bio_integrity_verify_fn is called for every level in the stack (it > used to be called only for the lowest level in 4.12). At different levels > in the stack, the bio may have different bi_sector value, so the repeated > verification can't succeed. We can simply add another bio flag to get back to the previous behavior. That being said thing to do in the end is to verify it at the top of the stack, and not the bottom eventuall. I can cook up a patch for that. > I think the patch 7c20f11680a441df09de7235206f70115fbf6290 should be > reverted and it should be reworked for the next merge window, so that it > calls bio_integrity_verify_fn only for the lowest level. And with this you will just reintroduce the memory leak for on-stack bios we've fixed. I'll take a look at not calling the verify function for every level, which is wrong, and in the meantime we can discuss the uses and abuses of the bio integrity code by dm in the separate subthread.


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FROM Aaron Snipe
What's Next for Libya and America's Role in Foreign Adventures? Moammar Gadhafi is still at large, but the US, NATO and neighboring countries are already preparing for Libya's next regime. We update action on the ground and in the world of diplomacy.
What's Next for Libya and America's Role in Foreign Adventures? When last heard from, Moammar Gadhafi threatened a fight to the death. Now, NATO is helping rebels to find him, while his loyalists continue to put up a fight. At a conference in Turkey, the US urged donor nations to unfreeze Libyan assets the rebels need to show they can govern the country. Nobody thinks that will be easy, given religious and tribal differences after 42 years of one-man rule and six months of civil war. Will the Obama "lead from behind" strategy be seen as successful? Has a retreat from Bush-style unilateralism been dictated by America's economic struggles? Photo: Libyan leader Moammar Gadhafi walking into a press briefing on February 5, 2011, at the same spot as the banner image above, with the iconic golden fist statue behind him, depicting a fist crushing a US jet fighter after Kadhafi's former residence was bombed in 1986 by US aircraft.
White House budget proposal slashes and burns President Trump's first budget request is considered dead on arrival in Congress — a familiar development in Capitol Hill. We hear what it reveals about the priorities of the new administration. What's likely to die… and what might survive?
Trump plays scolder-in-chief with NATO allies At the opening of NATO's dramatic new headquarters in Brussels today, President Trump acknowledged that Article 5 — promising that "an attack on one nation is an attack on all" -- has only been invoked one time: in the aftermath of September 11. But the President failed to provide what 27 other Alliance members have been waiting for: a re-commitment by America's new leader to Article 5. Instead, they got a scolding.
Trump's new look at civil rights and global warming President Trump is reportedly ready to pull the US out of the Paris Agreement on Climate Change. We look at the possible consequences. On the second half of the program, we hear about cuts in Obama-Era civil rights programs called for by the Trump Administration's first budget plan.
The Trump agenda: where's the beef? President Trump says big things are happening. After celebrating a House bill on health care, he doesn't yet have Senate agreement. With James Comey's public testimony scheduled tomorrow, the President today tweeted his selection of a new FBI Director. Is the Chief Executive all style and no substance? Later, terror attacks in Iran and conflicting claims about who's behind them.


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The family of a missing Auckland man is shocked that he has disappeared without with a trace.
Arthur Cooper, 62, has not been seen since he left his North Shore home on 22 November.
Stepson Corey Jull said he went to get a part for the waterblaster from the car and never returned. He left his wallet, phone and keys behind.
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Mr Jull said they have posted 100 fliers in the area.
Mr Cooper has short grey hair, a ginger-coloured goatee, and was wearing blue jeans and a blue short-sleeved collared shirt at the time he disappeared.


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I've stopped Risperdal but side effects continue. New psychiatrist appt tomorrow (2nd appt)... Old psychiatrist prescribed Invega but I never took it because of side effects list... its same as Risperdal. Input? Comments? Suggestions? Thanks!
What Risperdal side effects are you suffering with?
- Asked
- 8 Jul 2011 by margarethammaker
- Active
- 8 Jul 2011
- Topics
- invega, risperdal, depression, mania, schizophrenia, bipolar disorder, tardive dyskinesia, side effect, borderline personality disorder, schizoaffective disorder
Responses (1)
Hi, sorry, do you mean risperidone? how long ago did you stop it? If only recently and if you stopped taking it suddenly (without tapering) then the side effects can linger for a little while and you may be even experiencing some withdrawal effects? Are you hoping to be switched to a different medication at your appt?
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Lots of options for the rope climbs in today's wod, make sure you selected the best option for your skill level/goals. For those doing the full rope climbs, look to stagger your start by about a minute or so, especially if you are working on a touch and go skill set.
For the power snatches, feel free to move up in weight if your form and speed can keep up. Use that first pull to really get into a good position and look to maximize your hip drive and snap under the bar in a strong receiving position
Workout of the Day
Context: Competition
Mobility: Shoulder
Skill Practice Warm Up: fun game to warm up
Strength: 7×1 Power Snatch – 7 of 14, same weight across, approximately 80 – 90% of max power snatch
Super Set: 7×3 Half Kneeling Single Arm DB Shoulder Press, "across," scale to the same challenge
Metabolic Conditioning: "Broken Capstan"
In 7 minutes
3 Rope climb
then max rounds:
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Performance: 85/135
Athletic: 2 rope climbs, 55/85
Health: 6 lay down rope climbs or 10 assisted pull-ups, 35/55
Scaling Guide: 6 – 10 rounds, about 60s for the rope climbs, and 0:45 per round after.
Scale Up: 105/155
Compare to: NEW WORKOUT!
Optional 'Cash Out': 10 toes to bar, 15 wall ball, 4 min


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