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sage spa The University Club of Washington, DC
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1 sage spa The University Club of Washington, DC
2 Elevate the mind, soothe the soul, indulge the body at the university club
3 The University Club is recognized as one of the premier private city clubs in the United States. Sage Spa is the embodiment of what our members seek from their Club. An urban oasis of relaxation, Sage Spa provides members and guests with healing hands that make a difference in their day-to-day wellness. Peel back the stress of your work day. Cleanse. Relax. Rejuvenate. Invest in the quality of your life. Maintain a wellness routine through one of Sage s exclusive treatments. Take a moment to escape the conference calls, the client meetings and new client presentations. Productivity enhanced, mind cleared, body alert.
4 A special event is made more memorable at Sage Spa. There isn t a better way to enjoy a spa treatment than to share it with friends or associates. Sage can host your business associates, bridal parties, birthdays for teenage daughters or grandaughters, all complete with food and beverage. Your day is special. spend it with friends Sage Spa gift certificates are the perfect way to say you care. Select from a list of signature packages or a dollar denomination.
5 Menu of services Massage Therapy Stress Relief Concentrating on the back, neck and shoulders to relieve muscle tension and reduce stress. 25-minute massage $55* $65 Swedish A full-body massage combining multiple techniques to relieve tension and recharge the body. 50-minute massage $75* $90 80-minute massage $100* $120 Scalp, Hands and Feet The perfect tension reliever! Thorough massage of the scalp, hands and feet with warm oil. 25-minute massage $65* $75 Paraffin hand treatment $10* $15 Reflexology Warm oil is used to massage pressure sensors in the hands and feet to reduce stress and tension throughout the body. 25-minute massage $60* $70 * Member Price. Aromatherapy A deep, therapeutic holistic treatment using pure aromatic essential oils blended to create a tranquil atmosphere, which appeals to the senses, calming and clearing the mind. 50-minute massage $80* $95 80-minute massage $100* $120 Pre/Post Natal This total-body treatment has been carefully designed for pregnant and nursing mothers to aid in relaxation and tonicity of the skin during this special time. We recommend this experience only after the first trimester of pregnancy. 50-minute massage $95* $115 Deep Tissue An intensive massage designed to aid in the recovery of muscle tissue usually associated with sports activities. 50-minute massage $80* $95 80-minute massage $120* $140 Hot Stone Smooth stones are warmed and massaged all over the body to relax tissue and open energy channels. 50-minute massage $95* $115
6 Skin Care Executive Facial for Men A cleansing and hydrating facial for skin irritated by shaving or environmental effects. This revitalizing treatment leaves skin toned, smooth and well-conditioned. 50 minutes $85* $100 Sage Signature Facial A European facial uniquely personalized for your skin type. 50 minutes $80* $95 Deep Cleansing A deep herbal cleansing of the pores, followed by a thorough exfoliation and extraction, finished with a clarifying mask. 50 minutes $100* $120 Multivitamin Power Treatment Deep penetrating vitamins and antioxidants are applied to improve the overall health and appearance of the skin. Essential nutrients are restored, resulting in smooth, re-textured, supple skin. 50 minutes $120* $140 The Skin Brightener This rejuvenating facial is perfect for all skin conditions, particularly when lack of sleep, business demands or environmental stress leave you with dull skin. A special application of Skin Brightener, rich in antioxidants, soften, smooth and visibly improve the appearance and texture of the skin. 60 minutes $100* $120 Hungarian Organic Facial Healing herbs, fruits and vegetables create an organic facial that tantalizes the senses and treats the skin a truly unique experience. 50 minutes $115* $135 Hands and Feet Sport Manicure Good grooming is a necessity for any man in the business world. Cuticles are pushed back, nails are trimmed and buffed. A hand and forearm massage is the finishing touch. $20* $25 Manicures Hands are transformed with a gentle exfoliation, aromatherapy hand massage, mask and a dip in warm paraffin wax. Basic Manicure $30* $35 French Spa Manicure $40* $45 Polish Change Only $15* $20 Sport Pedicure Normal maintenance of the feet to combat roughness from daily wear, promoting healthy nail growth and leaving your toes clean and feeling refreshed. Complimentary shoe shine. $50* $60 Sage Spa Pedicure A pedicure to soothe and restore. Includes an extended leg massage, mask and paraffin treatment. Sage Spa Pedicure $40* $50 French Spa Pedicure $50* $60 Waxing and Tinting Services Waxing Brow $20* $25 Lip $10* $15 Chin $15* $20 Sideburns $15* $20 Back of Neck $15* $20 Full Arm $45* $60 Half Arm $30* $45 Underarms $25* $35 Full Back $50* $60 Bikini $25* $35 Lower Leg $30* $40 Thigh $40* $50 Full Leg $55* $65 Tinting Eyelash $20* $25 Brow $15* $20 Eyelash & Brow $25* $30 Body Treatments Essential Body Polishing Scrub Full-body exfoliating treatment using carefully blended sea salts or sugar and essential oils combined to help remove dead skin cells and improve tonicity. 30 minutes $60* $65 Detoxifying Mud Body Wrap Enzymatic sea mud will release toxins and impurities in the skin, improve elasticity, hydration and cellular regeneration. 60 minutes $110* $130 California Body Bronzer Full-body exfoliation followed by a sunless tanning treatment that will leave skin with a wonderful glow. 30 minutes $80* $105 Sage Spa Cancellation Policy: To ensure ample time to contact those on our waiting list, cancellation of services must be received by a Sage Spa associate 24 hours in advance. Should you need to cancel your appointment within 24 hours you will be charged 50% of the cost of your service. * Member Price.
7 A tradition of relaxation at The University Club Sage Spa Hours Monday & Tuesday 11 am 9 pm, Wednesday & Thursday 11 am 10 pm Friday 11 am 7 pm, Saturday 10 am 5 pm Sunday Noon 5 pm The University Club of Washington, DC 1135 Sixteenth Street NW, Washington, DC (202)
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Wednesday, August 23, 2017
Sammy Tavares Claims That St. Anthony Of Padua Helped Him Track The Murderer Of The Irish Girl
Saturday - Mar 18, 2017
A police officer who led the probe into the brutal murder of an Irish tourist in Goa on March 13 has claimed that his patron saint, St. Anthony of Padua, helped him track the killer. In a Facebook post uploaded late on Wednesday, Deputy Superintendent of Police (Canacona) Sammy Tavares said that praying to St. Anthony, a Portuguese-born Francisan Catholic priest from 1200, helped him find a clue in the sensational case, with which the police tracked down the killer within 24 hours.
"On March 13 morning at about 9 a.m., I received a shocking news about a naked dead body of a dead foreigner female at Canacona. The first thing I did was to pray Jesus and St. Anthony who is my patron. It was a Tuesday, St. Anthony's day. I demanded with St. Anthony to intervene and help me in solving this sensational case," Tavares said in his Facebook post.
While 26 per cent of Goa is Roman Catholic in religious orientation, Ireland is also dominated by Roman Catholics.
Tavares claims he got to the clue immediately leading to the arrest of Vikas Bhagat, a history sheeter, who has been booked under Section 302 of the Indian Penal Code. "Within few hours of investigations, we came across a clue, upon which we worked out and within four hours the suspect was put behind bars. On further investigations, he confessed of having involved in the gruesome murder of the innocent lady," Tavares said, thanking Jesus Christ and St. Antony for leading him to the clue.
The slain Irish tourist Danielle McLaughlin was found naked and sprawled, with injuries to her head and face in a desolate area in Devbaug in Canacona, a sub-district located 95 km south of Panjim.
A forensic team is also expected to examine whether the victim, who was vacationing in Goa with a friend, was raped. "I also assure all, that no stone will be left upturned to give justice to the near and dear ones of the victim," Tavares also said, even as Irish consular officials have established contact with the state home department to work out the arrangements for ferrying the victim's remains to Ireland.
Comments (14)
Albert Fereira
Friday - Apr 7, 2017
These Koknees who have squatted in Goa have spoilt the good name Goa which Goans have hard earned for generations during the last 5 centuries. They have brought all sorts of vices of bribery, corruption, crime, prostitution, drugs, rapes, murders, Nigerians, casinos, name all the evil on the planet earth. They have defiled and destroyed our peaceful Goa which was pure and Holy.
Saturday - Apr 1, 2017
Goencho Patraum
Wednesday - Mar 29, 2017
May the same St.Anthony give you wisdom and specially guts to face the "orders from the top" and conduct an impartial inquiry. Does your mobile has a call recording facility? If so record the call giving you "instructions" on how to conduct the investigation, as this may come in handy later if you defy the "orders" and the Porvorim Rat-hole masters take revenge on you... Have a little shame when people say "nothing will happen to the alleged murderer..." Imagine the same - May God forbid that - could have happened to your own daughter...
Monday - Mar 27, 2017
The NGO represented by Tara Kerkar, Canacona Municipal Council (CMC) Chairperson Prathana Naik Gaunkar and Goenkar President Jack Fernandes feels that more than one person murdered this Irish tourist. I also feel that police are covering up some of the facts of this brutal murder. Most of us Goans have no confidence in our police.
Friday - Mar 24, 2017
If Goa Human Rights Commission is genuine why does it not fight for those foreigners seeking justice to their innocent murdered kin? Are only Marathis, the alien ethnic majority in Goa, they basically look after are human beings? And the foreigners are dogs?
Friday - Mar 24, 2017
It shows that Parrikar's police is incapable to conduct the investigation independently. They need NGOs, which amounts to third party interference into independent police investigation.
Thursday - Mar 23, 2017
Our NGO Goenkar has found serious mistakes in the police investigation into the rape and murder of this Irish tourist. Parrikar Sir has promised us a proper investigation into Irish girl killing.
Thursday - Mar 23, 2017
Good for Mr. Tavares. A good story for another Tiatr!
Derrick D'Souza, Canada, ex-Karachi
Wednesday - Mar 22, 2017
Nothing will happen. Goa will sink into murders, prostitution and increasing drug infested menace under the successive Koknee Governments who have no clue of the outside civilized world that surrounds us. It will a dangerous place not only for Goans but also for foreigners to trample upon Goa. The very fact these Konknees, who run the Government, have horded the large Nigerian Community from Africa whose presence only affirms that it is for this purpose. These Koknees (Marathis mainly originating around the Konkan Range) are not historically part of Goa.
These Koknees are primitives by many aspects of the modern accepted civilized society standard. These are the products of the very low social society of manual workers who came into Goa in poor destitute condition to escape from the persistent drought and famine in the neighbouring British India, the sort of condition you now see in Somalia. They were of the stock which the British dubbed as 'Junglees' thus their present behaviour in Goa depicts. These are people not meant for Goa.
They don't have the slightest glimpse of the world because none of their generation has ventured or has seen the outside world, unlike the Goans who for half a millennium have contributed to the length and breadth of world's civilization and discoveries, for which Goa is best recognized for its role. These present Koknee are totally caged clowns in their own realm of domain, as you can see in the present Goa Government, a fully Kokno ministerial 'cabinet'.
Be Koknees from Maharashtra or Nigerians from Africa, these are the true actors on the centre stage of Goa and the naïve Goans as spectators all applauding hilariously the tiatr!
The whole irresponsibility allowing this to flourish lies on the doorstep of the Goans themselves.
It is their irresponsibility negligence, inaction and lethargy or laziness that has driven Goa into decadence. The Goans will have to live and sink with orgies of Sodom and Gomorrah with added murders.
Tuesday - Mar 21, 2017
Does anyone trust goa police to do a proper investigation? Police chief is saying murdered Irish tourist Danielle McLaughlin was 'loitering' with her murderer. When Goa Deputy IG uses words like 'loitering' for the murder victim you know they are not serious about the murder investigation. The House Committee on politician police drug mafia nexus showed how corrupt our police are.
Tuesday - Mar 21, 2017
The mishandling of the Scarlett Keeling case by the authorities helped the murderer to commit this crime. It sent a reassuring message to all rapists.
Monday - Mar 20, 2017
She is lucky that her body was found strewn in the field. Her body could have thrown into the river for the Kokne police of Goa to declare that her death was by drowning.
Goan Fredom
Monday - Mar 20, 2017
Nothing will happen! He will walk free like a king on the street of Goa, under the Supreme Kokne Rule of Goa!
sad Goan Diaspora
Sunday - Mar 19, 2017
The Goans in the UK have an obligation to take out ads in the papers warning the local British people not to vacation in Goa as it is a very dangerous place. With the exception of this case, every tourist was murdered under mysterious circumstances. Please advise you new hosts of the countries you all live in all through Europe, to NOT to holiday in Goa. It is dangerous place. Please do your duty to the hosts that have taken you or even anything negative happens again they will blame you. It is best to tell all of Europe NOT to travel to Goa. Do your part. Soon Hindutva will require a full sari to go to the beach.
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subset: commoncrawl


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Yash Birthday Special: Making Video Of Gajakesari
Rocking Star Yash, who is celebrating his 27th Birthday today, January 8, has got a biggest feast. The makers of Sandalwood's forthcoming movie Gajakesari have released the exclusive making video of the movie. Continue reading the story on slide show...
Birthday Gift For Yash
Director Krishna has revealed that the making video is the Birthday gift for Yash. It is also a biggest feast for Yash's fans, who were eagerly waiting for the video.
Featured On Cast And Crew
The 3 minutes 12 seconds video is featured on the whole technical team, cast and crew which is working for Gajakesari.
Yash In New Avatar
Yash, who sported long hairs for the movie, is his recent new avatar. It is said that the hair weaving technology is introduced for the first time in Kannada.
Designed By Alex
The long hairs has been designed by Alex, who had earlier worked for Bollywood Superstar Shahrukh Khan in Don 2 and Telugu Superstar Allu Arjun in Badrinath.
Rs 8 Lakhs Spent
It is reported that the producer has spent Rs 8 lakhs for the hair design, which took more than 20 hours to do.
Yash In Dual Roles!
Yash will be seen in the dual roles for the first time in his career along with a domestic elephant Arjuna.
Arjuna was found in Waynad forest, Kerala. The elephant is reported to be very mischievous by nature.
Yash Tackled Arjuna
As the script demands Yash and Arjuna together in most of the scenes, Yash learned few tricks from mahout and became very friendly with Arjuna.
Yash And Amoolya
Yash, who is basking in the success of Drama, Googly and Raja Huli, is paired opposite Golden Queen Amoolya in the movie.
Ravi Verma
Ravi Verma, who has become the most wanted stunt choreographer in Bollywood, is composing stunts for Gajakesari. He has won the best stunt choreographer award for Darshan starrer Kranthiveera Sangolli Raayanna.
Underwater Scenes
Gajakesari has few scenes, which is shot in underwater. Hence, Yash and Amoolya has received underwater training for the same.
Supporting Roles
The movie also features Sadhu Kokila, Shabaz Khan, Hyderabad Prabhakar, Chennai Johnny Vijay and others in the significant roles.
Directorial Debut Of Krishna
Gajakesari is the directorial debut of cinematographer Krishna, which is being produced by Jayanna and Bhogendra under Jayanna combines.


text:
With First Tutors: Music you can search for a Hockley baritone horn tutor. Baritone Horn lessons are a great way to start a fun new hobby, acquire a new talent and attain confidence with baritone horn. Use our site to find Hockley baritone horn teachers and select which suits your needs so you can enjoy your baritone horn lessons in Hockley today!
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It is a truth that MacBook Pro (in fact, all the Mac, including MacBook, MacBook Air, iMac) can't play Blu-ray discs deirectly. Since Sony has license on Blu-ray and Apple products don't ship with Blu-ray drive. It's a pity that you have an awesome MacBook Pro with a fantastic screen but can't enjoy your Blu-ray discs with it. However, you don't have to feel depressed for we proviod you the best solution here to play Blu-ray on Macbook Pro.
The first method is play with Blu-ray Player
Just download a free Blu-ray Player on your MacBook Pro, such as Bluraymaster, you can search on Google and install other player you think that is the best.
Connect the Blu-ray drive with your MacBook Pro, a Blu-ray drive is needed, due to MacBook Pro lacks
Open the Blu-ray Player you have installed and then insert Blu-ray Disc to the Blu-ray drive, most Blu-ray player will automatically load the disc information and play.
Note: Most of the free Blu-ray Player not support all the Blu-rays, especially the latest Blu-rays, some of them have a watermark on your screen.
The second method is back up Blu-ray as digital copy
Here Blu-ray Ripper comes out - Brorsoft Blu-ray Ripper for Mac (macOS Sierra supported). It is one of the best Blu-ray Ripper for macOS Sierra, with ability to crack Blu-ray anti-copying system AACS and other similar built-in protections that prevent straight-up copying. With this Powerful Blu-ray Ripper, you can do the things included but not limited to below:
|1:1 backup Blu-ray with original video structure
|Copy Blu-ray main title to remove extra information and advertisement
|Rip Blu-ray to H.265/H.264 codec MP4, MOV, M4V, etc format for Mac
|Convert Blu-ray to iPhone, iPad optimized preset.
|Migrate Blu-ray to NAS, Seagate Wireless Plus, WD MyCloud and other personal cloud storage in Home Theater.
|Allows users to adjust video/audio codec, size, bitrate, frame rate, channel, sample rate, etc.
|Trim video into several segments and crop unwanted and black area.
|Supported Mac OS 10.5 or above.
The trail version available, follow the guide below to access Blu-ray playback on MacBook Pro.
(Note: Click here for OS X 10.5)
> Click the disc-like button to load your Blu-ray files.
The Blu-ray titles and chapters will be listed on the program within a few seconds.
This Blu-ray ripper can detect the main title to convert instead of checking it on your own.
Note: Before loading Blu-ray content, a BD drive is needed and pls keep networked.
a. How to make lossless Blu-ray copy with original structure
> Click "Browse" button to select a destination folder for the output files.
> Click quick button "Copy the entire disc" to starts copying the DVD disc to hard drive maintaining the original structure.
As soon as the copying task finished, you can click "Open" button to get the output videos.
b. Directly copy Blu-ray main title on MacBook Pro
> Navigate to "Format" > "Copy" > "Directly copy"
> Click red big "Convert" button at the bottom right corner to start to copy Blu-ray main title.
c. Backup Blu-ray to MP4/MKV digital file on MacBook Pro
> Press on "Format" button to open the drop-down list.
Here you should choose the output format according to the ultimate usage.
|If you want to transfer Blu-ray and DVD to iPhone, iPad, you can select the target format in "iPhone"/"iPad" profile.
|If you just want to put the Blu-ray rips to Home Network, NAS and some other centralized location, you can simply choose MP4 in "Common Video" or "HD Video".
> Set the target folder by clicking "Browse" and finally start the Blu-ray backup process using "Convert" button.
Anyway, it can shows the fact that a Blu-ray ripper can backup your Blu-ray discs and give your portability of movies to entertain your media life.
Copyright © Brorsoft Studio. All Rights Reserved.


text:
Previously, I've noted the following blogs that display the MedLib Blog badge in their sidebars:
- Biomedbiblog
- Clinical Evidence, Searching Tidbits, and Other Minutiae
- DigiCMB
- JMLA Case Studies in Health Sciences Librarianship
- medinfo
- Professional Notes
- Women's Health News
I noticed a couple more excellent blogs that are using the badge, and wanted to make note of them here:
MGAS News
(News from the Biomedical Library, Katholieke Universiteit Leuven, Belgium)
Musings of a Medical Librarian Maven
(Alexia Estabrook's place to lay down the learnin')
If I've missed the badge on your blog or if you've just added it, please let me know so I can link to you here.
What's this all about?
The badge links back to the masterlist of MedLib blogs to indicate the blog's membership in the growing community (and sense of community) of MedLib blogs(/bloggers).
To add this badge to your own blog, just copy and paste this code:

Not sure how to do this with your particular blogging software? Email me at david[DOT]rothman[AT]gmail[DOT]com and we'll figure it out together.


text:
About the Book
"To escape is not to run away. It is to organize your thoughts.
To distance yourself from fear and chaos. And when you come back, you feel that you found the light that makes us special".
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text:
The Rosco
Designer Pattern range offers over 1000 standard gobo designs,
many of which have been created by the worlds leading lighting
designers. Each gobo in our catalogue is displayed with its
Rosco number and name in the bottom left hand corner and if its a specialist
gobo it will also have a letter in the upper
left hand corner as in the gobo pictured on the left. The letters
we use are...
= Meshed, C
= Colorizers, P
= Prismatics, SP = Spectrumgobos, SS = Signature Series.
standard steel gobos are available in sizes A, B, D, E and


text:
What is JotForm?
JotForm is a free online form builder which helps you create online forms without writing a single line of code. No sign-up required.
At JotForm, we want to make sure that you're getting the online form builder help that you need. Our friendly customer support team is available 24/7.
We believe that if one user has a question, there could be more users who may have the same question. This is why many of our support forum threads are public and available to be searched and viewed. If you'd like help immediately, feel free to search for a similar question, or submit your question or concern.
Heading field is not displaying properlyAsked by pardop1 on April 10, 2016 at 01:15 AM
please check out my form and correct the following issue:
Heading - Athlete information and the sub heading to follow is not deploying properly. It is almost like the a highlight feature.
JotForm Support
The problem is with the text color. Please use the Form Designer and change the text color of the heading. Here are the steps:
1. Click the "Form Designer" button in the top toolbar.
2. In the Form Designer, select the heading field. After that, make sure you are in the Design tab. Here you'll see the Header Styles and a color drop down selection. Choose the color you preferred and then click the Select button.
3. When you're done, make sure to save the changes.
Hope that helps. Thank you.


text:
Looks like The Remington Apartments Homes is no longer available on Rent.com which means this information is likely out of date.
Contact for details
The Remington is located in Northwest Austin, off of 620 with access to the 45 Toll & Hwy 183. An ideal location only minutes from some of the city's finest entertainment and shopping, such as Alamo Draft House Lake Line Mall, IFly and The Domain. We are also convenient to major employers like Freescale, Apple and PayPal. The Remington is also surrounded by exemplary Round Rock schools. Welcome home welcome to The Remington.
Our lease terms are: 1 month, 2 months, 3 months, 4 months, 5 months, 6 months, 7 months, 8 months, 9 months, 10 months, 11 months, 12 months, 13 months, 14 months, 15 months (Please note that lease terms may vary, are subject to change without notice, and are based on availability. Inquire with property staff for complete details).
Pet Policy: A maximum of two pets per apartment home are permitted unless used as an assistance animal. Restricted dog breeds are as follows: Doberman, Chow-Chow, Doberman Pinscher, Rottweiler, Pit Bull (also known as American Staffordshire, American Pit Bull Terrier, Staffordshire Bull Terrier) and all mixes of the above breeds.
Dogs Allowed. Cats Allowed. Pets Accepted. Call for service animal policy.
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These primary sources document the Japanese American experience from immigration in the early 1900s through redress in the 1980s with a strong focus on the World War II mass incarceration. The archives are growing as Densho continues to record life histories and collect images and records. We provide these resources to students, teachers, researchers, and the general public for educational purposes.
There are two options for exploring Densho's rich archival material:
Densho Digital Archive
Consult the Digital Archive if you are primarily interested in viewing our extensive collection of interviews. The archive includes more than 900 visual histories (over 1,700 hours of recorded video interviews). The video interviews are fully transcribed and segmented for ease of viewing. The interviews and images are indexed by topic, location and chronology, and can be searched using keywords. The Digital Archive also includes some, but not all, of our collections of photographs and documents.
Simply log on as a guest to enjoy the full benefits of our our Digital Archive.
Densho Digital Repository
Consult the Digital Repository if you are primarily interested in images and documents. Search or browse through thousands of historic photographs, documents, newspapers, letters and other primary source materials that tell the story of the Japanese American community from immigration to the WWII incarceration and its aftermath.


text:
|Publication number
|Publication type
|Publication date
|Aug 12, 1952
|Filing date
|Jul 6, 1948
|Priority date
|Jul 6, 1948
|Publication number
|Sam P Robinson
|Original Assignee
|Phillips Petroleum Co
|Export Citation
|BiBTeX, EndNote, RefMan
|Patent Citations (4), Referenced by (10), Classifications (11)
|External Links: USPTO, USPTO Assignment, Espacenet
Aug. 12, 1952 5 p, RQB|N$QN 2,606,938
CONTINUOUS SEPARATION OF HYDROCARBONS WITH CUPROUS HALIDE 'ABSORBENTS Filed July 6, 1948 I6 TAIL GASES i. 26 PRODUCT A 28 PRODUCT GASES TAIL GASES 4| 42 INVENiOR. S.P.ROBINSON FEED GASES ATTORNEYS Patented Aug. 12, 1952 CONTINUOUS SEPARATION OF HYDRO- CARBONS WITH CUPROUS HALIDE ABSORBENTS Sam P. Robinson, Bartlesville, Okla, assignor to Phillips Petroleum Company, a corporation of Delaware Application July 6, 1948, Serial No. 37,168
9 Claims. (01. 260 -6815) This invention relates to a process and apparatus for separating a gaseous mixture into two fractions by a sequence of steps involving absorption of one fraction on a finely divided solid absorbent followed by Stripping of the absorbed fraction in a separate zone. This invention is a continuation-in-part. of my copending application, Serial No. 710,468, filed November 18, 1946, now Patent No. 2,527,964.
I. Louis Wolk in Patent No. 2,386,734 discloses a process wherein diolefins are separated from mixtures containing more saturated hydrocarbons by absorbing the diolefins with cuprous halides in a fluidized state. The absorbed diolefin is stripped from the absorbent with a heated inert gas. The stripped absorbent is cooled with an inert gas and recycled back to the absorption step. My present invention is an improvement over Wolks process in that the absorbed unsaturated hydrocarbon is desorbed by a heated stream of product gas and the absorbent to be recycled to the absorption step is cooled by a recycle stream of unabsorbed tail gas. The many improvements over the prior art will become apparent from the accompanying disclosure.
The principal object of the present invention is to provide an improved absorption process for separating gases into several fractions. Another object is to provide such a process wherein far reater utilization of the absorbent is attained than has heretofore been known. Another object is to effect great savings in initial construction costs and in operation of such a separation system. Another object is to effect improved absorption, stripping and cooling of solid absorbent in a process of the foregoing type. Another object is to eifect the cooling of the stripped absorbent in a superior manner preparatory to recycling the absorbent to the absorption step. Another object is to eifect stripping of the rich absorbent in an improved manner. Further objects and advantages of my invention will become apparent to one skilled in the art, from the accompanying disclosure and discussion. p
The accompanying drawing portrays diagrammatically in vertical longitudinal section one arrangement of equipment which is highly preferred for carrying out the present invention.
In one process aspect the presentinvention accomplishes separation of a gaseous mixture into two fractions by suspending a finely divided solid absorbent in the mixture to be resolved under conditions such as to effect absorption of the desired fraction of the mixture by the absorbent, separating the resulting absorbent from the unabsorbed fraction, or tail gas, suspending the rich absorbent in a heated recycle stream-of stripped product gas under conditions such as to effect desorption of the absorbed fraction from the absorbent as a result of the heat derived from the hot recycle product gas, separating the resulting stripped absorbent from the stripping and. desorbed product gas, suspending the resulting stripped absorbent in a cooled recycle stream of the unabsorbed or tail gas under conditions such as to effect cooling of the absorbent to a temperature suitable for its reintroduction to the absorbing step, separating the resulting cooledabsorbent from the resulting tail gas, and recycling the cooled absorbent to the first-named suspending step. i a
My invention is based not only on the discovery that markedly improved results can be obtained by suspending a finely divided solid absorbent in the feed gas, the stripping gas and the cooling gas-in the absorbing, stripping and cooling zones, respectively, but also on the discovery that much improvedresults can be obtained by heating a portion of. the absorbed or product gas and employing this'for stripping and by cooling a'pQle tion of the unabsorbed or tail gas and using the thuscooled tail gas for cooling the absorbent to remove the heat imparted thereto in the stripping operation.
One feature of the present process is that the finelydivided solid absorbent is suspended in the feed gas under conditions such as to eifectthe desired absorption, and the resultingrich absorb! ent, after separation from the unabsorbed-gas in any suitable manner, is desorbed by suspending it in a heatedrecycle stream of stripped product gas. This feature of myinvention is highly advantageous because contamination of theabsorbent or of the desorbed product with the heated stripping medium is completelyavoided sincethe heated stripping medium is itself a portion of the desorbed product gas. In addition heat transfer is nearly perfect as compared to the poor heat transfer obtained when indirect means of heating the solidabsorbent, such as coils located'in the bed of absorbent, are employed in. accordance with prior practice.
As another feature of the present process the finely divided solid absorbent is suspended in the feed gas under conditions effecting absorption of the desired fraction of the feed gas by-th absorbent'followed by stripping of the separated absorbent and the hot stripped absorbent is cooled by suspending it in a cooled recycle stream of .tail gas, thereby effecting cooling of'the absorbent to a temperature suitable for recycle to the absorption step. This feature also is highly advantageous over the customary methods of cooling the hot stripped absorbent befor re-introducing the same to the absorption step, One advantage is that the tail gas is readily available being made continuously by the process. Furthermor the absorbent is not contaminated by an extraneous gaseous medium as would be the case were such an extraneous medium employed instead of tail gas for direct contact cooling of the absorbent. Cooling the tail gas before suspension of the hot finely divided'absorbent therein and passage of the resulting suspension into the cooling zone is advantageous, among other rea 'ons, beca se erosion of the cooler or heat exchanger is eliminated, whereas if the absorbent were suspended in the stream of recycled tail gas and the resulting suspension passed through a heat exchanger or cooler, erosion would be a serious problem. Furthermore heat transfer between the cooled gas and the finely divided solid absorbent suspended therein is very good as compared with the poor heat transfer obtained when cooling coils or other indirect coolin means are employed.
The process of my invention is preferably carried out in the following manner. The finely divided solid absorbent is suspended in a stream of the gaseous mixture employed as feed and the resulting suspension is introduced upwardly into the absorbing zone. Conditions in the absorbing zone are maintained such as to efiect absorption of the desired component or components of the feed by the absorbent. The rich absorbent is allowed to settle to the bottom of the absorbing zone and is Withdrawn therefrom in th form of a relatively compact mass. Tail gas free from absorbent is withdrawn from the upper portion of the zone. The withdrawn rich absorbent is suspended in a heated recycle stream of stripped product gas and the resulting suspension is introduced upwardly into the stripping zone where conditions are maintained suchas to effect desorption of the absorbed fraction and allow the resulting stripped absorbent to settle to the bottom of the zone. The resultin gas is withdrawn in a condition free from absorbent from the upper portion of the stripping zone. This gas has a composition identical with the absorbed fraction and is made up of the absorbed fraction and the recycled product gas employed for stripping. 'The gas withdrawn from th top of the stripping zone is split, into two streams'one of which is a product stream withdrawn from the system at a rate equal to that at which the product is entering the system in the form of feed gas and the second of which is a recycle stream which is heated and employed as the stripping medium in the stripping zone.
Stripped absorbent is withdrawn from the bottom of the stripping zone as a relatively compact mass and is suspended in a cooled recycle stream of tail gas. Tail gas withdrawn from the absorption zone is split into two streams, namely, a stream which is withdrawn from the system at a rate equal to that at which the tail gas fraction enters in the feed, and a recycle stream which is cooled and used to eficct cooling of the hot stripped absorbent. The resulting suspension of stripped absorbent in cooled recycle tail gas is introduced upwardly into the cooling zone, where conditions are maintained such as to effect cooling of the absorbent to the temperature at which it is desired to reintroduce it into the absorbing zone. The resulting cooled absorbent is caused to settle to the bottom of the cooling zone and is down to 20 microns in diameter.
withdrawn as a relatively compact mass from said zone. The thus cooled absorbent is recycled to the absorbing step. The recycle gas is withdrawn from the upper portion of the cooling zone and this stream of tail gas-so withdrawn, may conveniently be merged with the aforesaid stream of tail gas withdrawn from the system.
As will presently appear more fully, I prefer to maintain a light gaseous phase containing a relatively low proportion of absorbent in the upper portion of each of the three zones, and a dense phase containing a relatively high proportion of absorbent below the light phase in each zone, and to effect what is known as hindered settling in the dense phase in each zone. These results are preferably effected by correlating the velocity upwardly through each zone and the weight and size of the absorbent particles.
My preferred absorbent is cuprous chloride, but any cuprous halide, mixtures of cuprous halides, or other unsaturated hydrocarbon complex-forming metal salt of the heavy metals of groups 1 and 11 of the periodic system will work. The absorbent must have the property of forming an unsaturated hydrocarbon complex with the metal salt absorbent so as to make it possible to selectively absorb the unsaturated hydrocarbon. The absorbent may be used alone in finely divided solid form or it may be deposited on an inert support such as bauxite, asbestos, fullers earth, silica gel, pumice, charcoahor the like. Schulze and Morris in Patent No. 2,386,358 disclose methods of preparing supported absorbents which would be suitable to prepare absorbents to use in my process. For example, a 2G to 60 mesh bauxite in a closed kettle is sprayed with a hot water solution of cupric chloride containing about 8 pounds of cupric chloride per gallon. The bauxite is stirred constantly while the cupric chloride solution is being added. The cupric chloride solution is added until the bauxite is thoroughly moistened; at which time the reagent mixture will be about 55 per cent cupric chloride. The cupric chloride deposited on the bauxite is then reduced to cuprous chloride by passing sulfur dioxide gas or ethyl mercaptan gas through the wet agitated bauxite. The absorbent comprising cuprous chloride deposited on bauxite is dried and kept out of contact with oxidizing materials such as 02 or One skilled in the art will have no trouble preparing the absorbent to be used or operating in the absence of air and other oxidizing materials. The equipment used in the process may be swept clear of air as by passing methane or other inert gas through the system. I prefer to use an absorbent of particle size to 300 mesh, but the particle size may vary from 10 mesh In carrying out my process the gas velocity and particle size are correlated to give hindered settling in each of the absorbing, stripping and cooling zones.
The process of my invention has many applications. It may be used generally to separate unsaturated hydrocarbons from gaseous mixtures containing more saturated hydrocarbons. Typical separations are those wherein olefins are separated from gaseous mixtures containing close boiling paraffins and where diolefins are separated from gaseous mixtures containing close boiling olefins and paraiiins. My process is particularly useful in separating the conjugated diolefin butadiene-1,3 from gaseous mixtures containing more saturated close boiling hydrocarbons, or in separating isoprene from gaseous mixtures containing more saturated close boiling hydrocarbons. It is advisable in practicing my invention to remove any cyclopentadiene or acetylene from the feed stock, since these compounds are difiicult to desorb from the absorbent and operational difficulties arise. My invention can most economically be used where boiling points of the various components are so close together that ordinary fractional distillation is very costly and impractical. It is preferable to limit the separation to mixtures containing hydrocarbons having no more than five carbon atoms. Low temperatures aid the formation of the complex and the temperature in the absorb' ing zone should be just sufficient to keep all com ponents in the feed in the gaseous state.
The process of my invention is completely continuous, each step of the process being carried out continuously and without interruption. This is highly advantageous over batch or intermittent processes which have been proposed heretofore.
Each of the three zones, namely the absorption zone, the stripping zone and the cooling zone, may take the form of a vertically disposed elongated substantially cylindrical vessel closed at its opposite ends. The bottom may conveniently be of conical shape to facilitate removal of absorbent settling to the bottom of the vessel. Suitable equipment for separating absorbent particles from the gaseous or light phase above the lower or dense phase, and discharging the separated gas, substantially or completely free from absorbent particles, from each zone may conveniently be provided within the upper part of each vessel. Such separating equipment preferably takes the form of a cyclone separator of known type located wholly within each zone in the top thereof and arranged to withdraw the gaseous phase in the upper portion of the zone continuously, to separate the absorbent therfrom, to discharge the resulting gas through a conduit leading outside the zone, and to return the separated absorbent through a dip leg, or standpipe, depending from the cyclone to a point well below the level of dense phase in order to form thenecessary seal and prevent gas phase from blowing back up the legs, which would nullify the action of the cyclone.
The suspensions of absorbent in the feed gas, recycle product gas used for stripping, and the recycle tail gas used for cooling are introduced upwardly into the lower portions of the absorber,
stripper and cooler respectively under conditionsv regulated to effect the desired result in each of said zones. Typically the rates of absorbent introduction and withdrawal from each of the three zones are substantially equal during normal operation of the process. However a concentration of absorbent particles considerably greater than that prevailing in the incoming suspensions is maintained in the fluid-like absorbent beds (i. e. in the dense phase) inside the three zones. This result is brought about by correlating the linear velocity of the fluid mixture upwardly through the bed, and the average weight and size of the absorbent particles, to give hindered settlingof the absorbent particles in the fluid bed due tothe lifting action of the upwardly moving fluid stream working oppositely to the force of gravity on the absorbent particles. Hindered settling is reduced or substantially eliminated in the upper portion of each of the three zones. If desired, this may be accentuated by providing an enlarged upper portion. There is a relatively sharp line of demarcation between the fluid bed proper, in which there is pronounced hindered settling, and a high sorbent concentration is greatly reduced. The
lower or dense phase resembles a boiling liquid; The level of the dense phase, i. e. the interface between the dense phase and the light phase, is
very pronounced and resembles the interface between a liquid and a supernatant gas or vapor.
It is highly desirable to introduce the suspensions of absorbent in gas into each of the three zones through a distributing cone located in the bottom section of the zones. Such a'distributing cone is preferably substantially smaller in diameter than the zone and spaced above the bottom thereof (which is preferably conical) in order to allow settling of absorbent downwardly through the annular space, between the distributing cone and the walls of the zone into the space below the distributing cone, whence it may be withdrawn continuously as a relatively compact stream of absorbent. Such distributing cones-aid greatly in'the uniform distribution of the suspension over the entire area of the zones. The distributing cones may be provided across their top with foraminous means, such as perforated grids, for distributing the incoming suspension.
In each zone the degree of hindered settling, or backfiow of absorbent particles, should be such as to result in thorough mixing and sufficient turbulence in the lower, or dense :phase portion, of the zone to give a substantially uniform temperature distribution throughout the zone.
If desired the upper portions of the three zones, that is the absorbing, stripping and cooling zones, may be enlarged relative to the lower portion thereof in order to aid in the maintenance of hindered settling dense phase conditions in the lower portion, and to reduce greatly the amount of absorbent entrained in the light gaseous phase prevailing in the upper portions of the zones.
It will be understood that suitable provision will be made for the addition of make-up absorbent as required to compensate for system losses. Generally such make-up absorbent will be introduced in fresh condition directly to the first suspending step, wherein the suspension in the feed gas is prepared for introduction to the absorbing zone. It will also be understood that, if desired, suitable provision may be made for withdrawing a stream of the stripped absorbent continuously to a suitable regeneration unit, wherein the absorbent is treated in suitable manner to remove any contamination thereof.
ess described above, other types of fluidizedcon tacting may be employed within the broad concept of my invention. However such other types of fluidized contacting are much less preferably :5 because they involve too great a capital outlay for original equipment, and are undesirable in other respects, among which is the unnecessary com lexity and the difliculties encountered in operation. v V
The temperatures at'which absorption, desorpa V Thethus regener-' -ated absorbent will be recycled to the system.
tion-and cooling arecarried 'out in the practice of my invention can be readily established by one; skilled in the'art in the light of the present discl-osureaand discussion. Generally speaking, I prefer to can? out the absorption at a temperature just su fi ient to keep all hydrocarbons in the gaseous state. Generally the desorption is carried out at a considerablyelevated temperature. The stripped absorbent is cooled in the Cooling step to a temperatureat which it is suitable for reintroduction to the absorption step. Since the absorption involves the liberation of heat, may be desirable to cool the absorbent in the cooling step to a temperature below that of the incoming feed in order to compensate for such heat of absorption and consequent temperature rise. Alternatively oradditionally the feed gas may be cooled prior to the suspension of the cooled absorbent therein.
For the separation of butadiene-l,3 from a gaseous mixture containing more saturated close boiling hydrocarbons the following operating conditions are recommended and preferred.
Pressures-Low superatmospheric in the absonption zone.
Atmospheric or low subatmospheric in the desorption zone.
The absorption of butadiene-l,3 is aided by pressure and the desorption is hindered by pressure.
Temperatures Absorption znc.-Between 35 F. and 50 F. Mixtures of hydrocarbons containing butadiene- 1,3, other more saturated C4 hydrocarbons, and minor amounts of other more saturated hydrocarbons would boil in the range from 25 F. to 30 F., hence for vapor phase absorption of the butadiene-1,3 at one atmosphere pressure or slightly higher the temperature must be above 30 F. The complex formation ZCuCl is favored by low temperature.
Desorption eone.-i3etween 175 F. and 250 F. Temperatures in this range reverse the complex formation reaction.- Since product butadiene is used as the heating medium, it is desirable to desoro at high temperatures in order to reduce the amount of butadiene lost via the desorbed. absorbent.
Cooling coma-Cooled tail gas should be at a temperature required to cool the hot absorbent to the temperature desired in the absorption zone. Feed gases will have little eiiect on this temperature since they are introduced at about the temperature desired in the absorption zone.
In the accompanying drawing the absorber, stripper and cooler are shown as combined into a single unit, the absorber I being at the top, the stripper 2 being immediately therebelow and the cooler 3 being at the bottom. A single cylindrical shell, which is elongated vertically, may be used to form all three zones, this single shell being divided into the three zones by partitions 4 and 5 extending thereacross. The feed enters via line 5 and at point I is admixed in any suitable manner with cooled stripped absorbent flowing to conduit 8 to give a suspension which is conveyed by conduit 9 into absorber l. The means for suspending the absorbent in the stream of feed gas at point I may take any form known to the art. The resulting suspension is introduced upwardly in absorber l by distributing cone 10, forming the hindered settling dense phase in the lower portion of zone I. The upper level of the dense phase is indicated by line H. The absorbent which settles out passes around the distributing cone is and falls to the bottom of the absorbing zone, being collected as a relatively compact mass above collecting cone i2 and being withdrawn via line l3. Cyclone separator I4 is provided in the top of absorber i, and withdraws light gaseous phase continuously through inlet 1-5, separates the absorbent therefrom, and discharges the resulting tail gas via line [6. The separated solid absorbent is collected in leg or standpipe 57, which depends from separator M to a point well below the level it of the dense or hindered-settling zone.
The rich solid absorbent is conveyed by a conduit 13 to a point .13 where it is suspended by any suitable means, and in any suitable manner, in a'stream of heated recycle product gases entering via line Iii. The resulting suspension is conveyed by a conduit 28 upwardly through distributor cone 2| located in stripping zone 2. Hinder/ed settling conditions prevail in the lower portion of zone 2, the level of the dense phase being indicated by numeral 22. The rich absorbent is heldin zone 2 for a suflicient period of time and under conditions such that the absorbed fraction is substantially completely stripped therefrom by the heat imparted thereto by the heated recycle product gas. The stripped absorbent collects as a relatively compact mass above collecting cone 23, located in the bottom of zone 2, whence it is withdrawn continuously via means 24. The light gaseous phase in the upper portion of zone 2 is continually sucked into cyclone 25 which separates the product gas substantially free of entrained absorbent and discharges same via line 26. The separated absorbent collects in the depending leg of cyclone 25 and is continuously returned thereby to a point below the dense phase level 22.
The product gas stream is split at point 21 into two streams one of which is withdrawn from the system via line 28 and the other of which is passed via line 29 through heater 3%, the heated stream being employed to suspend rich absorbent prior to entry into zone 2. The recycle gas product stream may be heated in any suitable manner. I prefer however to heat it by indirect heat exchange with any suitable heating medium, such as steam.
The stripped hot absorbent is passed via means 24 and 3| to a point 32, where it is suspended in a stream of cooled recycle tail gas flowing in line 33. The resulting suspension is passed by means 34 upwardly into cooling zone 3, being distributed therein by distributing cone 35. Hindered settling conditions prevail in cooling zone 3, the level of the dense phase being indicated by numeral 36. The cooled absorbent collects in the bottom of zone 3 in collecting cone 3'! and is withdrawn continuously by means 8 which conveys it to the point i where it is suspended in the incoming feed entering via line 6.
The light gaseous phase prevailing in the upper portion of cooling zone 3 is continuously suckedinto cyclone 38 which separates the solid absorbent therefrom, discharging the resulting tail gas via line 39 and returning the solid absorbent to a point below the level 3'6 of the dense phase.
The tail gas discharged via line it from the top of absorbing zone I is split into two streams at point 40, one of the streams being withdrawn from the system via lines 4! and 52 and the other sagas stream being recycled via line 43 containing cool- "er' 44 for use in suspending the'hot' absorbent and for-cooling same in cooling zone 3. Cooler '44 is preferably an indirect cooler; the recycle tail-gas being cooled in any suitable manner as by indirect heat exchange with cooling water.
sorbent and of suspensions of absorbent in gas streams. "It will be understood by those skilled in the art that the drawing is schematic only and that details of conveying means compressors, pumps, heaters, coolers, piping, Ts, valves, check valves, gas seals, suspending means, etc. have been omitted from the drawing in the intereset of simplicity and more ready understanding of the invention. Such'details may readily be supplied, by those skilled in the art, for any specific application of my invention.
For starting up operations, a line 29A is provided 'for introducing a gas stream into the product recycle line 29 during the starting up period when the amount of product gas from stripping zone 2 is zero or very small in amount. As soon as steady state operation has been instituted, the flow of such extraneous gas through line 29A may be terminated. The'gas supplied during this starting up period may be either (a) an inert gas (1)) product gas from an outside source or (c) tail gas from line l6. The introduction of this gas would be discontinued as soon as the product stream reaches the volume required to supply the heat needed 'for desorption. However, I do not wish to ex- 'clude the possibility that inert gases may be used along with the recycle product gas for effecting stripping in zone 2, if desired, during the normal process period as Well as at the start of operations.
The extraneous gas supplied via line 29A during starting up and/or during normal operation should be onethat may be readily separated from the desired product, leaving via line 28, by conventional means within the skill of the art.
It is preferred that the feed gas be free from constituents which would gradually foul up the absorbent. Accordingly if the feed gas which i is .availablecontains such contaminants, it is treated before entering the system in order to remove such objectionable components.
In case absorbent contaminants get in the system, fouling up the absorbent, a take ofi line 24A has been provided, so that contaminated absorbent coming from the desorption zone 2 can be withdrawn. Fresh uncontaminated absorbent can be added to the system either through an inlet line 3IA, entering absorbent conduit line 3|, or through an inlet line 8A, entering absorbent conduit 8.
From the foregoing many advantages of my invention will be obvious to those skilled in the art. The principal advantage is that a greatly improved method of separating a gaseous mixture into two fractions is provided. Another advantage is that the equipment requirements are simple and adapted to long life. Another advantage is that the fluidized conditions employed allow enormous surface contact between the finely divided absorbent and the gases at vapors. My invention utilizes the. absorbent much more completely because the available absorptive area of a given weight of finely divided absorbent is enormous compared to that of .the
same absorbent in the'form of coarse particles. Another advantage is that my invention provides for the stripping of the rich absorbent by means of product gas itself so that no contamination whatsoever of the stripped material orof the absorbent is encountered. The heating of the richabsorben't by means of heated product gas is further advantageous since heat transfer is much improved over heating by indirect means such as steam coils. Still another advantage of my invention is that the stripped hot absorbent 'is cooled by 'a stream of cooled tail 'gas itself whereby excellent heat transfer is attained in the cooling zone and contaminationof the cooled absorbent with the cooling agent is avoided because the cooling agent is either not absorbed to any appreciable extent or if it is absorbed'it does not objectionably, contaminate the absorbent,
It should be pointed out however, that, in some cases at least, the gas which is not absorbed in zone I (i. e. the tail gas), because of the preferential absorption of the product gas, would be absorbed to some extent'in zone B'Where the concentration of product gas is very low. If this occurs, the absorbedtailgas would then be replaced by the more readily absorbed product gas when the absorbent reaches zone I so the net result is the same as if the tail gas were not absorbed in the cooling step, viz. the absorbent is not contaminated by an extraneous gaseous medium which might be used instead of tail gas for direct cooling of the absorbent.
Another advantage is that my invention provides a unitary process for the separation of gaseous mixtures into two fractions, each step cooperating with the rest of the process. Numerous other advantages of my invention will be apparent to those skilled in the art.
When separating an unsaturated-hydrocarbon having no. more than five carbon atoms from a mixture containing more saturated close boiling 4 hydrocarbons a contact time of 10. to30v seconds in the absorbing zone is satisfactory to give a high percentage of absorption of the desired product. The contact time in the desorption and cooling zonescanvary over a wide range, the
necessary heating and cooling being regulated by the. temperature and amount of the product strippinggas and cooling recycled tail gas respectively. 1 H .lAdv'antages of thi invention are illustrated by the following example. The reactants, andtheir proportions, and other specific ingredients are presented as being typical and should not be cone strued to limit the invention unduly.
Example {i hydrocarbon mixture produced by the catalytic dehydrogenation of butenes and having the composition (in parts by volume) is passed into an absorption zone in contact with a solid 200 mesh cuprou-s chloride absorbent.
11 The'flow of feed and absorbent are adjusted so as to provide a contact time of about 20 seconds at 40 F. The cuprous chloride-butadiene-l,3 complex is continuously withdrawn from the absorption zone and passed to a desorption zone in contact with a heated stream of product butadiene at a temperature of 200 F. Described butadiene having a purity of 99.5% is withdrawn from the top of this desorption zone, while cuprous chloride substantially free from the diolefin complex is withdrawn from the bottom thereof and passed to a cooling zone. There it is contacted with a stream of the unabsorbed tail gas from the absorption zone at a temperature of about 40 F.
As will be evident to those skilled in the art, various modifications of this invention can be made, or followed, in the light of the foregoing disclosure and discussion, without departing from the spirit or scope of the disclosure or from the scope of the claims.
I claim:
1. An absorption process for eiiccting the separation of an unsaturated hydrocarbon containing not more than five carbon atoms from a gaseous mixture containing the sametogether with close boiling more saturated hydrocarbons said mixture being free of cyclopentadiene and acetylenes, which comprises the following steps: suspending in said mixture in an absorbing zone at least one finely divided, solid cuprous halide absorbent under conditions such as to effect absorption of unsaturated hydrocarbon from said mixture by said absorbent; separating the resulting rich solid absorbent from unabsorbed tail gas; suspending said rich absorbent in a heated stream of stripped product gas in a separate stripping zone under conditions such as to eiTect desorption of absorbed material from said rich absorbent and merger of desorbed material with said stripped product gas; separating resulting stripped absorbent from resulting product gas; cooling said stripped absorbent by suspending same in a cooled recycle stream of said unabsorbed tail gas under conditions such as to effect cooling of said absorbent; separating resulting cooled absorbent and recycling same to said absorbing zone; and withdrawing product gas.
2. The process of claim 1 wherein the absorbent is at least one finely divided solid cuprous halide supported on an inert material.
3. A chemical absorption process for effecting the separation of a diolefin containing not more than five carbon atoms from a gaseous mixture containing the same together with close boiling more saturated hydrocarbons said mixture being solid grains of an absorbent, of size between 10 mesh down to 20 microns in diameter comprising at least one cuprous halide supported on an inert material, in said mixture in an absorbing zone under conditions such as to effect absorption of said diolefins from said mixture by said absorbent; separating resulting rich absorbent from unabsorbed tail gas; suspending said rich absorbent in a heated stream of stripped product gas in a separate stripping zone under conditions such as to effect desorption of absorbed material from the rich absorbent and merger of desorbed material with said stripped product gas; separating resulting stripped absorbent from resulting product gas; cooling said stripped absorbent by suspending same in a cooled recycle stream of said unabsorbed tail gas under conditions such as to effect cooling of said absorbent; separating resulting cooled absorbent and recycling same to said first-named step; withdrawing unabsorbed tail gas from the system; and withdrawing said resulting product gas from the system.
4. The process of claim 3 wherein the diolefin separated is butadiene-1,3 and wherein the absorbent is cuprous chloride supported on an inert material.
5. The process of claim 3 wherein the absorbent is cuprous chloride supported on an inert material.
6. The process of claim 3 wherein the diolefin separated is isoprene and the absorbent is cuprous chloride supported on an inert material.
7. The process of claim 3 wherein the diolefin to be separated is butadiene-1,3 and wherein the absorbent is cuprous bromide supported on an inert material.
8. The process of claim 3 wherein the diolefin to be separated is butadiene-l,3 and the absorbent is cuprous chloride supported on bauxite.
9. The process of claim 3 wherein the diolefin to be separated is a conjugated diolefin containing not more than 5 carbon atoms and wherein the absorbent is cuprous chloride supported on bauxite.
REFERENCES CITED The following references are of record in the file of this patent:
UNITED STATES PATENTS Number Name Date 2,386,200 Drennan Oct. 9, 1945 2,386,379 Wolk Oct. 9, 1945 2,386,734 Wolk Oct. 9, 1945 2,446,076 Campbell et al. July 2'7, 1948
|Cited Patent
|Filing date
|Publication date
|Aug 19, 1940
|Oct 9, 1945
|Phillips Petroleum Co
|Recovery of diolefins
|Jan 28, 1943
|Oct 9, 1945
|Phillips Petroleum Co
|Diolefin recovery
|Mar 8, 1943
|Oct 9, 1945
|Phillips Petroleum Co
|Method for recovery of diolefins
|Mar 1, 1941
|Jul 27, 1948
|Standard Oil Dev Co
|Separation and purification of gases
|Citing Patent
|Filing date
|Publication date
|Aug 6, 1965
|Aug 23, 1966
|Exxon Research Engineering Co
|Recovering allene by solid cuprous halide
|Mar 8, 1984
|Oct 8, 1985
|Hidefumi Hirai
|Solid adsorbent for unsaturated hydrocarbon and process for separation of unsaturated hydrocarbon from gas mixture
|Jan 21, 1987
|May 31, 1988
|Hidefumi Hirai
|Solid absorbent for unsaturated hydrocarbon and process for separation of unsaturated hydrocarbon from gas mixture
|Sep 4, 1987
|Sep 5, 1989
|Hidefumi Hirai
|Process for separation of unsaturated hydrocarbon from gas mixture
|Aug 7, 2000
|Jun 28, 2005
|The Regents Of The University Of Michigan
|Sulfur resistant adsorbents
|Sep 28, 2010
|Apr 15, 2014
|Research Triangle Institute
|Process and system for removing impurities from a gas
|Sep 28, 2010
|Aug 2, 2012
|Gunnar Henningsen
|Process and system for removing impurities from a gas
|Jun 7, 1961
|Aug 5, 1965
|Hoechst Ag
|Verfahren zur Entfernung geringer Mengen von Acetylen aus Gasgemischen
|Apr 17, 1984
|Feb 13, 1985
|Hidefumi Hirai
|Method of preparing solid adsorbent for unsaturated hydrocarbon and process for separation of unsaturated hydrocarbon from gas mixture
|Jul 23, 2001
|Feb 14, 2002
|The Regents Of The University Of Michigan
|Sulfur resistant adsorbents
|U.S. Classification
|585/800, 585/849, 585/829, 95/108, 95/144
|International Classification
|Cooperative Classification
|European Classification


text:
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text:
Shrimp from the Devil Priest
This delicious dinner recipe is courtesy of Mario Batali and can be found in his "Molto Italiano" cookbook.
- Yield: Serves 4
Source: The Martha Stewart Show, July Summer 2007
- 1/2 cup extra-virgin olive oil
- 6 cloves garlic, thinly sliced
- 4 jalapenos, seeded and thinly sliced
- 1 tablespoon crushed red pepper flakes
- 2 cups Mario Batali's Basic Tomato Sauce
- 1 cup dry white wine
- 20 large shrimp, heads on, split down the back, and deveined
- 4 slices rustic peasant bread, each 1 inch thick
- 2 tablespoons fresh marjoram leaves
- 1/4 cup toasted bread crumbs
Preheat the broiler. In a 12-inch skillet, heat 1/4 cup oil over medium heat. Add garlic and jalapenos and cook until softened, about 1 minute. Add shrimp, red pepper flakes, tomato sauce, and wine and bring to a boil. Lower the heat and simmer until shrimp is just cooked through, 4 to 6 minutes.
Meanwhile, toast bread on baking sheet under the broiler, turning once. Place 1 slice toasted bread in the center of each of 4 plates. Drizzle bread with 1/8 cup oil.
Place 5 shrimp on each piece of toast, and spoon the sauce over them. Sprinkle with marjoram leaves and bread crumbs, drizzle with remaining 1/8 cup oil, and serve.