text:
|Publication number
|Publication type
|Publication date
|Dec 16, 1975
|Filing date
|Mar 13, 1974
|Priority date
|Mar 13, 1974
|Also published as
|Publication number
|James R Gross, Russell T Mcfadden
|Original Assignee
|Dow Chemical Co
|Export Citation
|BiBTeX, EndNote, RefMan
|Patent Citations (5), Referenced by (96), Classifications (31)
|External Links: USPTO, USPTO Assignment, Espacenet
United States Patent 11 1 Gross et a1.
1 Dec. 16, 1975 [73] Assignee: The Dow'Chemical Company,
Midland, Mich.
22 Filed: -Mar. 13,1974
21 Appl. No.: 450,650
[52] US. Cl ..260/29.6 E; 260/296 TA, 260/78.5 R; 260/89.5 S, 260/296 SO [51] Int. Cl. C08L 31/02; CO8L 33/02 [58] Field of Search 260/785 R, 29.6 TA, 29.6 H, 260/296 E, 89.5 S, 29.6 SQ
[ 56] References Cited UNITED STATES PATENTS 2,649,439 8/1953 Brown 260/895 S 3,245,933 4/1966 Muskrat 60/296 N 3,514,419 5/1970 Darlow et all. 260/296 H 3,669,103 6/1972 Harper et a1 128/156 3,810,468 5/1974 Harper et a1 128/156 Primary Examiner.l0seph L. Schofer Assistant E.\'aminerPeter F. Kulkosky Attorney, Agent, or Firm-Benjamin G. Colley- [57] ABSTRACT Water swellable polyacrylate articles are made from a solution of the polyacrylate having an effective amount of a soluble crosslinking agent therein by heating and/or drying the solution. The polyacrylate solution is made from a polyacrylate by saponification and the cross-linking agent is then added.
9 Claims, No Drawings METHOD FOR MAKING A CROSSLINKABLE AQUEOUS SOLUTION WHICH IS USEFUL TO FORM SOFT, WATER-SWELLABLE POLYACRYLATE ARTICLES BACKGROUND OF THE INVENTION This invention relates to soft, water-swellable articles made from crosslinked polyacrylates, methods for their preparation, and to an aqueous solution of polyacrylates which is useful to make absorbent articles.
It is known from US. Pat. Nos. 3,669,103 and 3,670,731 that polymeric sorbents that are crosslinked during polymerization can be used to make disposable diapers, dressings and the like.
It is further known from Ser. No. 371,909, filed June 20, 1973, that water swellable articles can be made from post-polymerization crosslinked polyelectrolytes. However, these articles are generally stiff and brittle and generally require a plasticizer to make a film or casting soft enough to be useful in most applications, expecially in diapers. A disadvantage of using a plasticizer is that the most effective plasticizers are also humectants and make the polyelectrolyte article very sensitive to high humidity.
For example, if polyacrylates are converted through alkaline ester hydrolysis to the corresponding copolymer of the acrylate and acrylic acid salt, as in Ser. No. 371,909, approximately 80 percent or more of the acrylate mers must be so converted before the polymer becomes water soluble. This is attributed to alkaline attack on the polymer particle from the outside in, whereby the polymer molecules on the outside become much more altered by ester hydrolysis than those on the inside of the particle. At the high degrees of hydrolysis then necessary to solubliize all the polymer, the resulting polymer is more akin to a salt of polyacrylic acid than to a polyacrylate. The softness of the original polyacrylate has been replaced by the glassy brittleness of a salt. This brittleness is highly undesirable in water swellable (absorbent) articles.
SUMMARY OF THE INVENTION It has been discovered that the use of plasticizers can be eliminated in the known post-polymerization crosslinked polyacrylates by providing for the partial saponification of the alkyl acrylate mers in the polymer chains. Thus, when about 30 to about 70 weight percent of the alkyl acrylate mers are left intact in the polymer, the resulting crosslinked article formed from a solution of the partially saponified polyacrylate is soft and flexible without the necessity of adding a special water-soluble plasticizer such as glycerine.
The invention comprises methods of making crosslinkable aqueous solutions, methods of making soft, water-swellable crosslinked polyacrylate films and fibers as well as methods of making an absorbent article coated with a dry water-swellable soft polyacrylate and the products produced by the above methods.
Before the final products can be prepared, it is essential to'prepare a solution of the polyacrylate wherein an alkyl acrylate, or a mixture thereof with an alkyl methacrylate, is partially saponified with an alkali metal hydroxide solution. In general, the method of making this solution comprises A. forming a polyacrylate solution having about 30 to about 70 weight percent alkali metal carboxylates by dissolving in an aqueous alkali metal hydroxide solution a polyacrylate comprising 1. about 30 to about 92 percent by weight of an alkyl acrylate wherein the alkyl group has 1-10 carbon atoms, an alkyl methacrylate wherein the alkyl group has 4-10 carbon atoms, or mixtures thereoof; 2. about 8 to about percent by weight of an olefinically unsaturated carboxylic acid, and 3. about 0 to about 15 percent by weight of an omega hydroxy-alkyl acrylate having 14 carbon atoms in the hydroxy alkyl group; I B. heating the solution until saponification is complete,
and C. adding to said solution about 0.1 to about 10 weight percent based on the dissolved polymer of a watersoluble crosslinking agent which is reactive with carboxylate salt groups.
The final products of this invention are made by coating a substrate with the above solution or extruding the solution into non-solvents to form fibers both followed by heating and crosslinking the polyacrylates.
The final products of this invention are water-swellable and are useful wherever aqueous solutions need to be absorbed. The present invention is particularly useful to make disposable absorbent articles as an additive to increase absorbency while decreasing the articles bulk. Examples of the diverse utilities are surgical sponges, tampons, diapers, meat trays, litter mats for household animals and the like.
DETAILED DESCRIPTION The alkali-soluble polyacrylates useful to form the crosslinkable solutions of this invention can be made by known techniques such as emulsion, suspension, bulk, or solution polymerization techniques, so long as they consist of about 50 to 92 percent by weight of an alkyl acrylate with 1-10 carbon atoms in the alkyl moiety or an alkyl methacrylate with 410 carbon atoms in the alkyl moiety, about 8 to about 50 perccent by weight of an olefinically unsaturated carboxylic acid and about 0 to about -15 percent by weight of an omega hydroxy alkyl acrylate having 1-4 carbons in the alkyl moiety.
It is preferred to use alkali-soluble latices having about 15 to about 60 weight percent of non-volatile polymer solids as is set forth below.
Examples of useful alkyl acrylates are methyl acrylate, ethyl acrylate, propyl acrylate, hexyl acrylate and the like. Examples of useful alkyl methacrylates are butyl methacrylates, hexyl methacrylates, octyl methacrylate, decyl methacrylate and the like.
Examples of useful omega hydroxy alkyl acrylates are 2-hydroxyethyl acrylate, hydroxymethyl acrylate, 3- hydroxy-propyl acrylate and 4-hydroxybutyl acrylate.
The foregoing polyacrylates are then dissolved in an aqueous alkali metal hydroxide solution. Generally the equivalents of hydroxide solution used are from about 30 to about 70 percent based on the molar concentration of polymerized monomer and the preferred amount is from about 40 to about 55 percent. In any event, the amount of hydroxide solution added is sufficient to convert or saponify some of the acrylate esters to alkali metal carboxylates and to neutralize the carboxylic groups of the polyacrylate used into alkali metal carboxylates so that the converted polyacrylate has about 30 to about 70 weight percent of alkali metal carboxylates.
This solution is then rendered crosslinkable by adding about 0.1 to about weight percent based on the dissolved polymer of a water soluble crosslinking agent which is reactive or crosslinkable with carboxylate salt groups.
The foregoing aqueous solution can be used per se to prepare the final products of this invention. However, it is sometimes advantageous to add various amounts of volatile monohydric alcohols and/or ketones td control the viscosity of the aqueous solutions and increase the rate of drying. Examples of useful monohydric alcohols are lower alkanols such as methyl alcohol, ethyl alcohol and propyl alcohol. Examples of useful ketones are acetone, and methyl ethyl ketone.
Illustrative examples of the soluble crosslinking agents useful in this invention are polyhaloalkanols such as 1,3-dichloroisopropanol, 1,3-dibromoisopropanol; sulfonium zwitte rions such as the tetrahydrothiophene adduct of novolac resins; haloepoxyalkanes such as epichlorohydrin, epibromohydrin, 2-methyl epichlorohydrin and epiiodohydrin; polyglycidyl ethers such as glycerine diglycidyl ether, ethylene glycol diglycidyl ether, propylene glycol diglycidyl ether, diethylene glycol diglycidyl ether; and the mixtures of the foregoing.
The olefinically unsaturated carboxylic acids used in this invention can be mono or poly carboxylic acids.
Examples of the mono-olefinic monocarboxylic acids are acrylic, methacrylic, crotonic, isocrotonic, angelic, tiglic, senecioic or mixtures thereof.
Examples of the mono-olefinic polycarboxylic acids are maleic, fumaric, itaconic, aconitic, teraconic, citraconic, mesaconic, glutaconic.
Compounds containing two or more of the functional groups of the foregoing crosslinking agents would also be useful, as well as precursors which would form these functional groups under the conditions encountered in heating or drying the polyelectrolyte solutions.
Sulfonium zwitterions are known from U.S. Pat. No. 3,660,431, dated May 2, 1972; Ser. Nos. 205,754 and 205,755 both filed on Dec. 7, 1971. The disclosures of this patent and patent applications are incorporated herein by reference.
The crosslinking technique used in this invention to transform water-soluble polyacrylates into insoluble but water-swellable polymers is known as nucleophilic displacement on saturated carbon.
The carboxylate ion on the polyacrylate acts as the nucleophile while the cross-linking agent is the substrate for the nucleophilic attack. Typical leaving groups and their corresponding substrates are listed in Table I. Any combination of two or more of these leaving groups on the same substrate could act as a crosslinking agent for the polyacrylates of this invention.
Table II lists several illustrative compounds used as cross-linking agents in this invention and the operable limits to obtain insoluble but highly swellable polyacrylates according to this invention. Once insolubility is reached, higher levels of cross-linker give polymers which swell in aqueous media to produce firmer, less slippery gels but of lower actual absorbency.
TABLE I Leaving Groups in Nucleophilic Displacement (R alkyl or aryl) TABLE I-continued Leaving Groups in Nucleophilic Displacement R ulkyl or aryl) TABLE II Cross-linking Agents for Polycarboxylates Crosslinker Wt. of Polyelectrolyte l.3-dichloroisopropanol 04-10% epibromohydrin 05-10% epichlorohydrin l-l0% glycerine diglycidyl ether 0.10-457r novolac sulfonium ion l-l0% The rate of nucleophilic displacement is concentation dependent and is a factor in this invention. In solution, when the concentration of the cross-linker is very low, the rate of reaction is quite slow (pot life 10-48 hours before gelation). Once the solution is applied to a substrate Surface and evaporation of solvent begins, the rate of cross-linking accelerates. Applying heat at this time increases the reaction rate even more.
If the cross-linking reaction is allowed to proceed in the original solution as by heating, aging, or excessive amounts of cross-linker, the absorbent articles of this invention cannot be fabricated. The solution will become progressively more viscous and stringy until it forms a continuous gel which could not be spread,
sprayed or spun.
In the method of making water-swellable films by the present invention the above solution of the polyacrylates is spread on a flat plate or roller of metal, plastic, or other impervious substrate and heated to a temperature greater than 30C. to crosslink the polyacrylate and drive off the excess water and/or alcohol. The film is then peeled off the plate or roller by a scraper to recover the intact film for subsequent storage or use.
Similarly, when an absorbent article is prepared, the article which is to be the substrate is coated with the solution of the polyacrylate and then the coating is cross-linked. It is to be understood that for the purposes of this invention the coating step implies a complete coating or a discontinuous coating, thus when a fibrous substrate such as cellulose batting, paper, woven or non-woven cloth, and the like are usedas the substrate, the solution can be applied in a discontinuous manner, i.e. in a pattern of large dots, squares, or grid lines to retain the inherent flexibility of the fiberous substrate and at the same time vastly improve its water absorbency. Wood pulp can be coated by slurrying it in the polyacrylate solution followed by a fluffing operation.
If desired. the water swellable film prepared as above can be used per se as the inner absorbentlaye'r in baby diapers. It is sometimes advantageous that the film be disintegrated into flakes, stripso'r powders. This is accomplished by crushing or comminut'ing the film in a hammer mill, blenders, or the likejlf long flat strips are desired, the film can be sliced widthwise with appropriate slicers. I
In some instances, water-swellable fibers are desired. These can be prepared by extruding the above solution of the polyacrylates into a bath comprising lower alkyl ketones such as acetone, methyl ethyl ketone, diethyl ketone and the like. Alcoholic solutions may be extruded into a non-aqueous coagulant such as chlorinated hydrocarbons, i.e. methylene chloride, perchloroethylene and the like. The soft extruded fibers are then removed from the bath by any convenient means such as a three or five roll cluster and carried through a heated chamber at a temperature greater than about 30C. and preferably in the range from about 70 to about 150C. to dry and to crosslink the polyacrylate fibers.
The absorbency of the crosslinked polyacrylates (grams of solution gelled per gram of pol-yacirylate) is determined in the following manner using synthetic urine (0.27 N sodium chloride solution).
'A 0.5 gram sample of a crosslinked polyacrylate is weighed into a 250 ml. beaker, a 0.27 N sodium chloride solution (150 ml.) is poured into the beaker and allowed to soak for 2 hours at room temperature, with occasional'sti'rring. The swelled polyacrylate is then collected by filtration and the gel capacity is reported as grams of solution gelled per gram of polymer salt.
Thefollowing examples are presented solely to illustrate but-'not limit the invention.
EXAMPLE 1 Three mixtures were made up having the following compositions.
' Part B 2.1 g. Sodium 28 g. Methacrylic Persulfate Acid 8.4 g. Acrylic Cld 3. l g. t-Dodecyl Merca ptan "dioctylsodiurn sulfosuccinate (Triton GR-S) Part A was charged to a 2 liter reactor and brought to 40C. while under vigorous nitrogen purge. Eighteen milliliters of Part B was added to the reactor followed by all of Part C. The remainder of Part B was added over the next 2.5 hours while the temperature was held at 39-41C. The latex was then digested at 40 for 1.5 hours, cooled to 30 and bottled. The latex contained 39.5 percent non-volatiles.
Four hundred grams of latex prepared above was mixed with g. of sodium hydroxide dissolved in 120 g. of deionized water at 75C. to give a %-solution of polymer which was 31.4 percent by weight sodium acrylate and methacrylate. Ten grams of the above solution was mixed with 30 mg. of glycerine diglycidyl ether 1.0 percent curing agent by weight of polymer).
. 'A sheet was cast on mirror-finish chrome plate using a 25 mil draw bar, air dried, and oven cured for 15.5 hours at and 0.5 hour at This polymer sheet imbibed 23 times its own weight of synthetic urine (0.27 N NaCl solution) in the above absorbency test.
EXAMPLES 2-7 The procedure of Example 1 was repeated with varying amounts of sodium hydroxide and curing agent. The results are shown in Table 111 along with Example E. A. Ethyl acrylate Hydroxyethyl acrylate is present in the amount of 8 mole 'r; in all examples.
*Glycerinc diglycidyl ether 1 In g. 0.27 N NaCl per g. polymer These examples showthat softness and absorbency have an inverse relationship. The best all around product of these examples is one containing approximately 50 mole residual acrylic esters and cross-linked by approximately 0.15 weight glycerine diglycidyl ether.
EXAMPLE 8 Example 1 was repeated using the following monomer mix, and less initiator and no mercaptan chain stopper in order to raise the molecular weight.
The polymerization was carried out at 60C. and produced a latex of 40.6 percent non-volatiles.
1125 g. of the above latex was added in a-small stream over a period of 25 minutes to a slowly stirred solution of 187.16 g. 50% NaOH in 547.9 g. deionized water. After the polymer had all dissolved, the viscous solution was heated at 50C. for 22 hours to complete the saponification. The resulting solution (25.4 percent solids) had a Brookfield viscosity of 16,200 cps. at 25C. (No. 5 spindle, 10 rpm). The polymer is 50% ethylacrylate by moles with the remainder being sodium acrylate and methacrylate.
32 g. of the above solution was blended with 16 mg. (0.2 wt.%) of glycerine diglycidyl ether and cast on polished chromium plate with a 25 mil draw bar. After air drying, the film was lifted from the plate and placed in a oven. The absorbency (gel capacity) of the film in 0.27 N NaCl was 64 g. solution per gram polymer after a 20 minute cure. The film was strong and flexible right out of the oven and required creasing in order to tear it.
EXAMPLES. 9-12 Eight grams of the saponified solution prepared in Example 8 was mixed with various amounts of 1,3- dichloroisopropanol and films were cast and cured from these mixtures in the manner of Example 8. The gel capacities of the films are set forth in Table IV.
TABLE IV Wt.7( Mg. of D.C.|.P. Example D.C.I.P. Crosslinker Ahsorhenc v* D.(.l.P. 1.3-dichloruisopropanol gms 0.27 N NziCl per gm of polymer These examples show the optimum level of crosslinker using D.C.l.P. is near 0.5 percent by weight of polymer to be cured.
EXAMPLES l320 TABLE V Mole Wt.7( Example 71 E. A. G.D.E. Absorbency Softness 13 55 0.2 44.4 soft 14 52 0.2 48.8 soft 15 50 0.2 49.6 somewhat soft 16 40 0.2 57.2 brittle 17 55 0.175 52.4 soft 18 52 0.175 58.8 soft 19 50 0 175 58.4 somewhat soft 20 40 0.17 5 60.0 brittle E. A. ethyl acrylate G.D.E. glycerine diglycidyl ether These examples show that the unconverted ethyl acrylate portion of the copolymer can be increased to 52 mole without significant loss in absorbency and a desirably soft product is obtained.
EXAMPLE 21 Three mixtures were made up having the following compositions:
Part A 230 gms deionized water 0.3 gms Triton GR-5 1.0 gms Na S O (sodium persulfate) 10.0 gms itaconic acid Part B 20 gms methacrylic acid 170 gms ethyl acrylate Fart 70 s deionized water -.Part A was chargedto a 2 liter reactor and brought to 60C. while under a vigorous nitrogen purge. Then 20 ml. of Part B was addedfollowed by all of Part C. The remainder of Part B was added continuously over a period of one hour at 60C. Thelatex was digested for one hour at this temperature to obtain a final latex having 40.6 percent non-volatiles.
Then, gms of the above latex was mixed with 16.9 gms of a 50'percent aqueous sodium hydroxide solution and 49.1 gms of deionized water and heated at 55C. for about 10 hours to give a 25 percent solution of polyelectrolyte containing 52 molar percent ethyl acrylate. This polyelectrolyte also was calculated to have 51% by weight ethyl acrylate 30% by weight sodium acrylate 12.3% by weight sodium methacrylate 6.5% by weight disodium itaconate.
Twenty grams of the above polyelectrolyte was blended with 45 grams water and 7.5 mg. (0.15%) glycerine diglycidyl ether. A film was cast on a mirror finished chrome plate using a 25 mil drawbar and this film was air dried 6.5 hours at room temperature and then oven cured at C. for 16.5 hours. The absorbency of the final cured film was 41 gms/gms of polymer in the above absorbency test with synthetic urine.
Example 21 illustrates that the polymerization recipe and process can be significantly altered but still allow the preparation of highly absorbent polymer.
We claim:
1. A method for making a crosslinkable aqueous solution which is useful to form soft water-swellable polyacrylate articles which comprises A. forming-a polyacrylate solution having about 30 to about 70 weight percent alkali metal carboxylates by dissolving in an aqueous alkali metal hydroxide solution containing sufficient alkali metal hydroxide to saponify some of the acrylate esters and to neutralize the carboxylic acid groups a polyacrylate comprising I. about 30 to about 92 percent by weight of an alkyl acrylate wherein the alkyl group has l-10 carbon atoms, an alkyl methacrylate wherein the alkyl group has 4-10 carbon atoms, or mixtures thereof,
2. about 8 to about 50 percent by weight of an olefinically unsaturated carboxylic acid, and
3. about 0 to about 15 percent by weight of an omega hydroxy-alkyl acrylate having 1-4 carbon atoms in the hydroxy alkyl group B. heating the solution until saponification is complete, and
C. adding to said solution about 0.1 to about 10 weight percent, based on the dissolved polymer, of a water soluble crosslinking agent which is reactive with carboxylate salt groups.
2. The method as set forth in claim 1 wherein the unsaturated carboxylic acid is a poly carboxylic acid.
3. The method asset forth in claim 2 wherein the polycarboxylic acid is selected from maleic, fumaric, itaconic, aconitic, teraconic, citraconic, mesaconic, glutaconic or mixtures thereof.
4. The methodv as set forth in claim 1 wherein said unsaturated carboxylic acid is a monocarboxylic acid.
5. The method as set forth in claim 4 wherein the monocarboxylic acid is selected from acrylic. methacrylic, crotonic, isocrotonic, angelic, tiglic, senecioic, or mixtures thereof.
acrylic acid.
8. The method as set forth in claim 6 wherein the water soluble crosslinking agent is a polyglycidyl ether. 9. The method as set forth in claim 8 wherein the 5 polyglycidyl ether is glycerine diglycidyl ether.
1 UNITED STATES PATENT AND TRADEMARK OFFICE CERTIFICATE OF CORRECTION PATENT N0. 3,926,891 DATED December 16, 1975 INVENT0R(5) James R. Gross et a1.
It is certified that error appears in the aboveidentified patent and that said Letters Patent is hereby corrected as shown below:
Q Column 2, line 38, "50 to 92" should read 30 b0 92 Column 8, line +6, 8 to about 50" should read 8 to about '70 Signed and Scaled this Eleventh Day of December I979 [SEALE Arrest:
I SIDNEY A. DIAMOND Attesting Oflicer Commissioner of Patents and Trademarks
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|May 15, 2003
|Dec 4, 2003
|Murali Rajagopalan
|Highly neutralized polymer golf ball compositions including oxa acids and methods of making same
|May 18, 2004
|Oct 28, 2004
|Gartner Herbert A.
|High internal phase polyelectrolyte emulsions for the manufacture of superabsorbent polymers and superabsorbent polymers made therefrom
|Sep 19, 2005
|Feb 2, 2006
|Nippon Shokubai Co., Ltd.
|Absorbent resin composition
|Apr 30, 2004
|Aug 2, 2007
|De La Mettrie Roland
|Process for treating keratin fibres by applying heat
|Jul 13, 2006
|Aug 21, 2008
|Dow Global Technologies, Inc
|Microcavity-Containing Resilient, Thermoplastic Foam; Composite of Such Foam and Particles; Methods of Preparing and Articles Prepared From Same
|Mar 6, 2009
|Dec 10, 2009
|Mircea Dan Bucevschi
|Biocompatible, Biodegradable, Water-Absorbent Hybrid Material
|Sep 15, 2009
|Jan 14, 2010
|L'oreal S.A.
|Process for treating keratin fibres by applying heat
|Jul 17, 2009
|Jun 9, 2011
|Basf Se
|Method for the enzyme-catalysed hydrolysis of polyacrylic acid esters, and esterases used therefor
|Mar 24, 1980
|Feb 5, 1985
|The Dow Chemical Company
|Absorbent films and laminates
|Jun 10, 1987
|Apr 19, 1988
|The Procter & Gamble Company
|Hydrogel-forming polymer compositions for use in absorbent structures
|Oct 25, 1982
|May 5, 1983
|Arakawa Chem Ind
|Verfahren zur herstellung eines festen, trockenen und wasserabsorbierenden harzes
|Dec 14, 1982
|Jul 6, 1983
|Seitetsu Kagaku Co., Ltd.
|Water-absorbent resin having improved water-absorbency and improved water-dispersibility and process for producing same
|Dec 14, 1982
|May 30, 1984
|Seitetsu Kagaku Co., Ltd.
|Water-absorbent resin having improved water-absorbency and improved water-dispersibility and process for producing same
|Jun 20, 1986
|Jan 21, 1987
|Taiyo Fishery Co., Ltd.
|An aqueous composition, method of producing a water absorbent polymer, water absorbent polymer-coated article and method of producing the same
|Oct 17, 1995
|Apr 24, 1996
|Air Products And Chemicals, Inc.
|Self-crosslinking, aqueous absorbent polymer compositions
|Feb 25, 1991
|Apr 2, 1997
|Kimberly-Clark Corporation
|Absorbent structure
|Jul 18, 2008
|Jan 20, 2010
|Basf Se
|Method for enzyme-catalysed hydrolysis of polyacrylic acid esters and esterases to be used
|Nov 6, 2001
|May 25, 2011
|Sorbent Therapeutics, Inc.
|In vivo use of water absorbent polymers
|Sep 21, 2007
|Jun 27, 2012
|Dow Global Technologies LLC
|Fibrillated polyolefin foam
|Apr 15, 1985
|Oct 23, 1986
|The Dow Chemical Company
|A process for absorbing water having a ph less than four
|Aug 9, 1985
|Feb 12, 1987
|The Dow Chemical Company
|Material for absorbing aqueous fluids
|Apr 2, 1986
|Oct 8, 1987
|The Dow Chemical Company
|Process for preparing improved weak acid resins and porous weak acid resins
|Jul 7, 1992
|Jan 21, 1993
|Chevron Research And Technology Company
|Ethylene-alkyl acrylate copolymer saponification process
|Dec 17, 1999
|Jun 22, 2000
|The Dow Chemical Company
|Preparation of a low polydisperse water-soluble polymeric composition
|Jul 17, 2009
|Jan 21, 2010
|Basf Se
|Method for the enzyme-catalysed hydrolysis of polyacrylic acid esters, and esterases used therefor
|Sep 29, 2010
|Apr 7, 2011
|Wilcox Heather J
|Male urinary incontinence device
|Aug 20, 2013
|Feb 27, 2014
|Ardelyx, Inc.
|Compounds and methods for inhibiting nhe-mediated antiport in the treatment of disorders associated with fluid retention or salt overload and gastrointestinal tract disorders
|Feb 19, 2016
|Aug 25, 2016
|Osmotica Kereskedelmi Es Szolgaltato Kft
|Method of improving gaba-b receptor agonist therapy
|Feb 19, 2016
|Aug 25, 2016
|Osmotica Kereskedelmi Es Szolgaltato Kft
|Method of administering r-baclofen in an extended release dosage form
|Feb 19, 2016
|Aug 25, 2016
|Osmotica Kereskedelmi Es Szolgaltato Kft
|Controlled release oral dosage form of gaba receptor agonist
|Feb 19, 2016
|Aug 25, 2016
|Osmotica Kereskedelmi Es Szolgaltato Kft
|Controlled release oral dosage form of gaba receptor agonist with enhanced pharmacokinetics
|May 13, 2016
|Nov 17, 2016
|Mcknight Gary David
|Non-aqueous organo liquid delivery systems containing dispersed poly (organic acids) that improve availability of macro & micro-nutrients to plants
|U.S. Classification
|523/412, 525/330.6, 523/111, 525/385, 525/134, 525/329.6, 525/355
|International Classification
|Cooperative Classification
|European Classification


text:
missing translation for 'onlineSavingsMsg'
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Promega™ Dual-Luciferase™ Reporter (DLR™) Assay Systems
Combine the speed and sensitivity of two luciferase reporter enzymes into an integrated single-tube dual reporter assay
Manufacturer: Promega™ E1910
Specifications Description & Specifications
|100 Assays
|Luciferase Assay Buffer II; Luciferase Assay Substrate (lyophilized); Stop & Glo Buffer; Passive Lysis 5X Buffer
|Dual-Luciferase Reporter Assay System
Get Up to $1,000 in Complimentary Promega ProductsPurchase up to $1,000 in any combination of Promega™ reagents and receive an equivalent amount of complimentary Promega products of your choice. This is an NLSU exclusive offer. You must apply and qualify for the program to be eligible.
: 06/30/18

subset: commoncrawl


text:
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Hello, I'm called, Sis. I was born in Dyersburg, Dyer County, Tennessee, to L.D. and Helen June Williams Singleton. I was raised in Chicago, Illinois, mostly. In 1980, I moved to Gary, Indiana. I love Genealogy, tracking the path that led to my Family & me. I was always, told as a small child, that my paternal grandfather came from Ireland and that my maternal Gr' grandmother, was full blooded Cherokee Indian. I found out it wasn't my grandfather that came from Ireland, but, his father. Well, at least that what it say's on a 1920 census report.
I would like to Thank Everyone, who has left Cards & Tokens on my Memorials. I truly appreciate it.
If you find any mistakes I have made, please let me know and I will correct ASAP.
God Bless YOU and OUR COUNTRY.
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nora barton-carver
Find A Grave Memorial# 32432100
i believe this memorial is incorrectly linked to the wrong mother, the ollie ashley who died in 1907 in morgan, tn was the daughter of robert williams and appears to only have had one child by harry ashley b. 1905 and raised by his maternal grandparents, that was ernest ashley. not sure which memorial manager to contact for this correction. thanks!
Added by
nora barton-carver
on Jul 04, 2017 12:21 AM
Kathy Galpin Biggs
Fleda and Thomas Jones Biggs
Hi Sis -
I found the headstones for Fleda and Thomas - they don't have all the great information you have shared though. Thought you might want to contact the creator of these:
Thomas: 123469403
Fleda: 123469635
Thank you.
Added by
Kathy Galpin Biggs
on May 10, 2017 7:01 PM
Bonnie Brasure-Mauzy
Hiram Myles Jones buried Tiptonville, Tennessee
You have parents wrong here. His father was John Green Francis Jones and Maudie Marie Dunn-Jordan. Both his parents are buried in these family plots in the Tiptonville Cemetery.
Added by
Bonnie Brasure-Mauzy
on Apr 18, 2017 1:09 PM
Dennis Lauzon
REG : Memorial# 28207651
Hello Sis,
Were you able to attain the first name of Virginia Dales husband? I have been trying to track that down with no luck.
Thanks so much for your work and support!
Added by
Dennis Lauzon
on Mar 26, 2017 3:02 PM
Dennis Lauzon
REG : Memorial# 28207651
Hello Sis,
We you able to attain the first name of Virginia Dales husband? I have been trying to track that down with no luck.
Thanks so much for your work and support!
Added by
Dennis Lauzon
on Mar 26, 2017 2:58 PM
Beth Hall (mom of Hayes)
27969134 Harry Jones
I emailed awhile ago for a transfer and also asked for a edit on my step fathers but I haven't heard anything and the edit was never done. Just checking to see if you got it. My contr. # is 46528452
Added by
Beth Hall (mom of Hayes)
on Feb 13, 2017 7:35 PM
Jerry Samuel Lee Sr
Find A Grave Memorial# 34503290 Jerry Samuel Lee Sr I have his obit and U.S. Social Security Death Index, just edit his birthday and death date.
Added by
on Feb 11, 2017 9:09 PM
Terry A. Zier
Andrew Jackson Williams #23269518
I'm sort of confused. Do you know if Andrew Jackson Williams was married to just Emerline Booth or was he married also to Elleanor Evaline Bowers?
Added by
Terry A. Zier
on Feb 06, 2017 4:54 PM
William R. Ward
David Jonathan Hall #26985948
Hey Sis,
Please connect my great uncle, David Jonathan Hall, to his mother, Elizabeth Ann (Youree) Hall #123977500 or transfer maintenance to me. He is shown as a half-brother because he is not connected.
Thank You, Bill Ward
Added by
William R. Ward
on Dec 08, 2016 10:10 AM
Greg Roach
Charles Hawks
Hello, I was researching Benjamin Hawks son to Charles and Anna and using Ancestry an Findagrave I found your work. I posted a death certificate for Charles that shows burial location. His memorial# is 167727741 I posted same info there also some edits. I am trying to link family members to Benjamin and Hattie. Does this help any?
Thanks for all of your hard work; Greg
Added by
Greg Roach
on Nov 05, 2016 3:22 PM
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|"Michael A. Smith" <...@apache.org>
|Re: [VOTE] (re-vote) XxxUtils constructors
|Thu, 22 Aug 2002 20:54:58 GMT
On Thu, 22 Aug 2002, Geir Magnusson Jr. wrote: > That would be fine in a 2.0 release. You might not want to do that with an > incremental release if it's already been release. > > I realize that's more 'listen to your customers'... Commons Collections has already had a release with some Utils in it, so absolutely it would require a major revision number change in order to implement such a change. I have no problem with that and would have argued the same thing. > Commentary : sounds like a fine solution as long as you make it on a major > release as to NOT BREAK PEOPLE ALREADY USING IT. I have no issue with that... regards, michael -- To unsubscribe, e-mail: <mailto:firstname.lastname@example.com> For additional commands, e-mail: <mailto:email@example.com>
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Hey there, time traveller!
This article was published 8/12/2013 (1320 days ago), so information in it may no longer be current.
The province's youth organizations will be $100,000 richer next year.
The money is coming from a new community investment program created by MTS called "Future First".
Starting in 2014 the telecommunications company will be offering youth-serving organizations grant opportunities totalling $100,000.
The funding will be going to organizations that specifically focus on "youth advancement" and positive social change.
"Manitoba's youth face many challenges," including poverty and lack of access to education and work, said Pierre Blouin, MTS Allstream CEO during the launch event. "But there are many organizations in the community working to improve these barriers.
"It's our intention with Future First to provide support to these organizations and help provide the means to create new initiatives," said Blouin.
The Future First strategy also incorporates post-secondary scholarships, sponsorships, employee volunteerism, and a corporate United Way campaign.
Recipients of the Future First grants will be presented with the $10,000 on Manitoba Day, May 12.
MTS will be releasing more details about how to apply for Future First grants and the selection process in early 2014.
Blouin said MTS provides up to a million dollars in community investment each year.


text:
As Labor Day approaches, beach days get fewer and further between. But summer isn't officially over until Sept. 23, so families are rushing out to make the most of it with dolphin watches aboard local cruise ships.
The Cape May Whale Watcher runs two-hour dolphin watches from Schellenger's Marina, daily through the middle of October, when the dolphins head south.
Capt. Jeff Stewart Jr., whose father started the company in 1993, says while dolphins are the main event, it's something different every time.
"Sometimes we'll see a lot of bird life," says Stewart, who's been working on the boat since he was 8. "Just the other day we had a sea turtle and a shark."
The boat has seating on two levels. There is an indoor area with tables and a view of the ocean. There are restrooms and a snack bar on board, and strollers are allowed on the first deck.
The watch is a hit among young kids. That's why Jodi and Craig Chasse brought their daughter Ciarra. The Chasses, from Connecticut, had seen dolphins from the shore the day before and decided to try a dolphin watch.
"We'd been planning on going on a dolphin watch for a while," said Craig Chasse, "just to check out the dolphins and see what's going on."
He takes photos of wildlife, sometimes aided by the eyes of his 9-year-old daughter.
"Take a picture of the parasailor, Dad!" says Ciarra who, not surprisingly, is most looking forward to seeing the dolphins.
While most of the tour will be spent watching dolphins, the cruise through the bay is more than just a commute. Over the loud speaker, Stewart points out natural and manmade landmarks. It feels like a 3-D nature documentary as he rhythmically narrates the shore, which rolls by on both sides. The salt marshes, osprey stands, World War II era structures and swing railroads keep the kids entertained right up to the moment of the main event.
"If you look into the trees to the left you'll see a bald eagle resting in the canopy about 25 feet up," Stewart says over the loud speaker. Everyone on the boat stares into the trees. Stewart appears to be making it up, but as the boat pulls closer to the shore, to avoid the Cape May-Lewes Ferry, it becomes easily spottable. All of the sudden it spreads its wings and, as if it's been paid off by the Cape May Whale Watchers, flies directly over the boat.
Joanne Anderson is sitting inside with her 9-month-old son, Dylan.
"We came primarily for the kids," she says smiling at Dylan. "I'm here with my sister and her kids." Her daughter, Hallie, comes running in.
"I saw the bald eagle," says the excited 8-year-old. Joanne Anderson asks her about it, but Hallie's already pointing to something else. "Look, a big boat!"
The tour never loses sight of land. It's like touring Cape May from a whole new point of view. As we get farther from land, though, and Delaware is off on the horizon, someone spots a dolphin well off in the distance. The captain doesn't bother to point it out, which seems strange, but soon we learn why. For more than half an hour, the boat is completely surrounded by dolphins. They come right up to the side, sometimes even jumping. Stewart educates the crowd on everything from how they communicate (by slapping their tails on the water, a real crowd pleaser) to the difference between a dolphin and a porpoise.
It turns out the location of these dolphin tours is no accident. Stewart explains that Cape May is the northern-most calving ground for these creatures, so mothers and children are looking over the deck at more than 40 mother dolphins and their calves.
The Chasses, who initially spotted the dolphins, walk around the deck, checking out the dolphins from a variety of angles. Some people leave their seats upstairs and head downstairs for a different view. The snack bar, which stocks cookies, juice, ice cream, coffee and more, gets a lot of business, especially from the little ones. Binoculars can be rented from the snack area as well. As the boat continues around the island, away from the dolphins, the crowd returns to their seats to enjoy the sun and sea breeze. It's a perfect, late-summer day, something Stewart explains is not a requisite.
"It's a great rainy day activity," Stewart says. "A lot of people think, 'what happens to the dolphins when it rains?' Guys, the dolphins are already wet."
But what happens to the humans when it rains? They have that one covered, too. On top of the permanent indoor seating, the boats have expandable roofs that will keep passengers dry even right up against the railing.
As the watch winds down, Laurie Newton, of Egg Harbor Township, explains this is their typical end-of-summer activity.
"We come every year," says the mother of two. "I grew up in Wildwood Crest. You have to do the end of the summer, before school starts stuff."
Her daughter, Emily, is glad it's a tradition.
"I love doing this every summer," says the 12-year-old. "My favorite is always the dolphins. They're always out."
Back on the top deck Ciarra Chasse is satisfied with the tour. And her favorite part? You guessed it: dolphins.
"And now she's got like 400 pictures of dolphins," laughs her mother.
Dolphin-watching tours
Cape May Whale Watcher
1218 Wilson Drive, Cape May
609-884-5445, capemaywhalewatcher.com
Cost: $28 adults, $18 children ages 7 to 12, free children 6 and younger
When: 10 a.m. to 6 p.m. daily through mid-October; two-hour tours
JCC Boats
6200 Park Blvd., Wildwood Crest
609-729-7776, jjcboats.com
Cost: $28 adults, $20 children ages 6 to 12, free children younger than 6
When: 9:30 a.m. daily; two-hour tours
Atlantic City Cruises
Historic Gardner's Basin, N. New Hampshire Ave., Atlantic City
609-347-7600, atlanticcitycruises.com
Cost: $34 adults, $29 seniors, $18 children ages 5 to 15, free children younger than 4
When: 1 p.m. daily through Sept. 19; Wednesdays, Saturdays and Sundays from Sept. 22 to Oct. 9; two-hour tours
Silver Bullet Tours
Wildwood Marina at Rio Grande and Susquehanna avenues, next to the Boat House and Urie's Restaurant
609-522-6060, silverbullettours.com
Cost: $28 adults, $15 children ages 2 to 11
When: 9:30 a.m, 12 p.m. and 2:30 p.m. daily; 90-minute tours


text:
Who We Are
In 1994, the California Primary Care Association (CPCA) was created to provide a unified voice for community health centers (CHCs) throughout California.
Our Mission
To lead and position community clinics, health centers, and networks through advocacy, education and services as key players in the health care delivery system to improve the health status of their communities.
Whom Our Members Serve
California is home to more thank 1,100 CHC sites, including Federally Qualified Health Centers (FQHC), FQHC Look-Alikes, and Rural Health Centers. Combined, these CHCs serve more than 5.6 million patients annually through over 17 million patient encounters. More than 50% of these patients are Hispanic and 43% speak a primary language other than English. Nearly 65% fall under 100% of Federal Poverty Level, with 35% eligible for Medi-Cal subsidies and 30% uninsured.
How We Support Our Members
Why work with the California Primary Care Association?
Since 1994, CPCA has been the statewide leader and recognized voice for California's 1150+ community health centers (CHCs).
With the advent of federal health care reform legislation, CHCs will play a key role in meeting the primary care needs of the millions of newly patients in California. Given CPCA's prominent role in assisting our members during this historic time of growth, there has never been a better time for your business to have visibility as being part of the movement to help ensure "healthcare access for all."
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The Annual Sponsorship Program ensures a year-round presence with CPCA's membership so that you can build more meaningful relationship with key health care decision-makers through increased recognition and trust of your brand. This program also provides a meaningful discount for your sponsors who wish to have a presence at all of CPCA's conferences and event s throughout the year. The Annual Sponsorship Program's tiered structure provides flexibility and opportunity for organizations of all types, sizes and marketing budgets. This program opens January 1st of each calendar year and will be on a first come, first served basis.
Each year, CPCA hosts a number of events intended to provide opportunities for members, community partners, clinic leadership, key decision makers, and health care stakeholders to learn from each other. Participants share best practices, discuss challenges and opportunities, and celebrate those who have been instrumental in supporting the essential work of CHCs. In addition to our regular meetings, trainings, and advocacy opportunities, CPCA hosts six major events, each with attendance of anywhere from 100 to over 900 attendees.
How to Get Involved
CPCA looks forward to partnering and finding creative ways to support the mission of community clinics and health centers in California. We would be happy to schedule a meeting with our Sponsorship Team to discuss your organization's specific needs.
Become part of the movement that represents over 1,150 community health centers and over 5 million patients helping to ensure "healthcare access for all!"
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PerformanceRetail Forms Alliance with Cybera
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AUSTIN, Texas -- PerformanceRetail, provider of Web-based merchandising and store-operations software for the retail industry, and Cybera Inc., which delivers fully managed broadband networks for retail, have entered into a co-marketing alliance to provide dedicated networks and applications to the retail industry. This alliance will enable retailers to more quickly drive improved profitability and efficiencies in key store processes as they implement broadband connectivity and Web-based merchandising and store-operations solutions.
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The three branches of the government under the Constitution are like a school
The teachers/ pathways administrator and are like the executive branch (president) because..
the teachers try to make the students follow their rules just like the executive branch makes the people obey the laws
The principal is like the checks and balances because..
the principal determines which actions of the students is wrong justlike checks and balances
The school's superintendent is like the separation of powers because..
like the separation of powers determines how each branch gets its own power, the superintendent does the same for the school board
The code of conduct is like the Constitution because..
like the constitution is the base of the government, the code of conduct is the base of the school system
The assistant principal is like the judicial branch (supreme court) because..
the judicial branch interprets the laws just like the assistant principal interprets the rules of the school
The school board is like the legislative branch (Congress) because..
the school board makes the rules just like the legislative branch makes laws
The students are like the people because...
the students have to obey the rules just as the people obey the laws
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The three branches of government are like a football team
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Dominique Dowlingon 16 December 2013
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The SUF-660P Universal Flat Wall Mount (37-65") is extremely thin only 0.33" (8mm) from the wall, This near-invisible mount is ideal for ultra-thin flat panels and supports the weight of standard screens. Its all-steel, universal design is the ultimate solution in delivering space-saving, ultra-sleek look that brings the screen closer to the wall.
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Let us know when your receive great advice so we can thank our lawyers and point others with similar questions in the right direction.Got it!
Already on probation for possession of meth. era
The person could potentially be looking at a couple things. One, the person would be charged with a new felony for the new possession charge. Additionally, the department of parole and probation will most likely want to try to revoke the persons probation (if they are on probation out of district court). If the person gets picked up and taken into custody because of the alleged violation (new arrest) then the person would not be able to bail out before a probation revocation hearing is held (which could take a few weeks).Ask a similar question
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Fans of vintage tube overdrive are most likely already familiar with the Vox name. Of course, if you're just starting out, it only makes sense to begin with something simple, and the Valvetronix VT20+ 20W 1x8 Guitar Combo Amp is a terrific choice. Loaded with 99 presets and tons of FX, this stunning combo amp delivers a wide range of sought-after sounds that cover every style. Boasting a 12AX7 preamp tube and unique Power Level control, the Valvetronix VT20+ is a versatile amp that's perfect for both recording and practicing at home.
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With so many iconic musical artists attached to the Vox name, you know exactly what you're getting into when you go with one of the amplifiers and effects from this section. In the world of popular music, Vox will forever remain in a class of their own, and if you still don't know why, it's time you gave them a try.


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How do I remember my password to log into this site?
I should really stop doing trolling. I had an actual question about a month ago that NSU probably could have helped with. Must have solved it because I can't remember what it was.
In any case, anyone use Tasker on Android? Anyone? Anyone? Bueller? Bueller?
I hate Tasker. I do a couple things on the command line that run at boot and have something else for shell stuff through widgets. It annoys me that I can't see what's being passed to the system from most apps.
So, actual question... writing a power saving thing for Galaxy S II, persistant script with almost zero battery footprint. On my phone I can't just toggle 3g to 2g. I have to turn off mobile data, then go into settings and toggle, then turn data back on. I can turn data on and off but don't know how to toggle between radio states. Its a specific annoyance for my model. Anyone have the answer; swich the radio in use at the command line? Anyone? Bueller? Bueller?


text: Friday a family member was going to cook a big meal and took some sausage out of the freezer and put it out to thaw (NOT in the fridge, fully out). They seen they had to much and put a pack of pork sausage back in the fridge for me to use. I didn't get a chance to cook it that day and ended up cooking it around midnight of Saturday/Sunday. Now I'm wondering if it really is still safe. The package was opened and a small chunk taken out, mid Fri. afternoon.


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Aylward Game Solicitors
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Aylward Game Solicitors Brisbane are a modern and dynamic firm of Brisbane Solicitors and Brisbane Family Lawyers who are strongly committed to traditional professional values of the legal practice in Australia.
Aylward Game Solicitors Brisbane were established in 1998 and are based in modern and attractive offices in Brisbane's CBD, providing high quality legal advice and representation to clients throughout Queensland and more widely around Australia.
Our main areas of practice are Commercial and Business Law, Commercial Litigation, Property Law and Conveyancing, Vendor Finance, Family Law, Wills, Estates, Enduring Powers of Attorney, Collaborative Law and Town Agent Services.
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American Gun Cabinet Collection
Showcase your cherished keepsakes and heirloom items in this stunning Amish handcrafted Curio Cabinet. This curio cabinet is built to fit in a corner and take advantage of this unused space in your home. Choose to order in oak, cherry or brown maple wood with a variety of finish selections.
© Copyrights 2003 - 2017 DutchCrafters All rights reserved.


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Oldsmobile automobile owners have come to expect a certain level of reliability when driving their Cutlass Supreme around town. The vehicle in your driveway is head and shoulders above the rest compared to all the other cars, trucks, and SUVs in today's marketplace. When your Oldsmobile Cutlass Supreme was born, it was destined for a driver who wants long-lasting quality in their automobile. Car aficionados know that good looks is built into each Oldsmobile, and understand that only top quality replacement Cutlass Supreme parts will suffice when your car or truck needs fixing.
On every car today, there are pieces of optional equipment and there are pieces of standard equipment. Your Oldsmobile Cutlass Supreme door lock solenoid actuators are the reason you can electronically lock and unlock your doors. Because power door locks are now equipped on almost all vehicles, door lock solenoids will be found in virtually all doors on all cars and trucks. Restore your Oldsmobile Cutlass Supreme to its original level of convenience and fix or replace your broken door lock solenoid actuator right away.
Given all the trouble that can be involved with performing maintenance on your car or truck, let www.carpartsdiscount.com be the number one store you go to make buying it easy. When your Oldsmobile needs a top quality replacement Door Lock Solenoid Actuator, there's no need to trust any store other than the authority, Car Parts Discount. Don't let a broken Door Lock Solenoid Actuator spell the end of your car, truck, or SUV, and don't risk lowering its resale value by using anything but the best replacement parts. When it comes to Oldsmobile Cutlass Supreme Door Lock Solenoid Actuator parts, you can find them for 1997, 1996, 1995, 1994, 1993, 1992, 1991, 1990, 1989, 1988, 1987, 1986, 1985, 1984, 1983, 1982, 1981, 1980, 1979, 1978, 1977 models by clicking the appropriate year below.


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Moderator: Community Team
JBlombier wrote:I've always liked this one.
JBlombier wrote:I suggest you click on the image
Lil_SlimShady wrote:JBlombier wrote:I suggest you click on the image
Yeah, I take that back.
Symmetry wrote: it's a 2dimes post! He's not going to post things that are in anyway wrongheaded or thoughtless. Everything he posts is gold.
Return to Sixteen shots of rum. No girl.
Users browsing this forum: Bernie Sanders


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SBI 2200 Probationary Officers (PO) Recruitment 2016 Latest Notification – Download Past Papers:-state bank of india has declare a new notification of SBI PO Recruitment 2016 with vast number of vacancies. state bank of india released the Probationary Officer posts in state wise vacancy and backlog vacancies..interested candidate can apply to go to the official website or Log on to official website sbi.co.in.its a good news of all the seekers who are trying to do job in a banks sector.its a government jobs .there are Total no of 2200 Vacancies for Probationary Officer posts has been published by SBI authorities.there are large no of vacancies .
SBI PO Recruitment selection process is in 4 stages.
Phase-I : Preliminary Examination (Objective Type).
Phase-II: Main Examination (Objective & Descriptive Test).
Phase-III: Group Discussion and Phase-IV: Personal Interview.
In this article we have given complete information on SBI PO eligibility criteria, important dates, how to apply online application form, recruitment selection procedure, pay scale, age limit, schedule below.
SBI 2200 Probationary Officers (PO) Recruitment 2016 Latest Notification
State Bank of India is the most reputed Bank in India and is the largest banking and Financial Company.there are different head quaters across india .the services of state bank of india is so fast and its is available almost of any town or any state of india. sbi every year release a recruitment process for the post of clerk, Probationary Officer(po),Specialist Officer and Manager, senior manager, counsellors and certain other vacancies. sbi select only the talented person for smooth processing of organisation.State Bank of India headquarters in Mumbai, Maharashtra.
Important dates:
Online registration: 04-05-2016 to 24-05-2016
Application Fees Dates: 04-05-2016 to 27.05.2016
Download of call letters for Online Preliminary Examination 14-06-2016 onwards
Online Examination – Preliminary 2nd, 3rd, 9th & 10 July 2016
Result of Online Exam – Preliminary 18-07-2016
Download of Call Letter for Online Main Exam 21-07-2016 onwards
Conduct of Online Examination – Main 31st July 2016
Declaration of Result – Main 16th August 2016
Download Call Letter for Interview 22nd August 2016
Conduct of Group Discussion & Interview 1st September 2016
Declaration of Final Result 30th September 2016
SBI PO Selection Process 2016:-
Phase-I: Preliminary Examination (Objective Type)
Phase-II: Main Examination (Objective & Descriptive Test)
Phase-III: Group Discussion
Phase-IV: Personal Interview
Pay scale of SBI PO is Rs. 14500/- to Rs. 25700/-. Aspirants need to pay application fee and intimation charges Rs. 100/- for SC/ST/PWD. General & OBC pay rs Rs. 600/-. Candidates have to make Online Payment through Credit / Debit or Net Banking, and there is No Challan. Candidates are requested to check all the important dates, exam schedule dates and guideline before applying.
How to Apply for SBI Recruitment 2016
- Visit official website sbi.co.in
- Click on career
- Click on SBI Probationary Officer Recruitment 2016-17
- Carefully read the notification
- Check eligibility qualifications
- Go through that link
- Click on New Registration
- Provide the asked details i.e. Candidates name, Father's Name, Mobile Number, Email-ID)
- Upload Scanned Photo & Signature
- Provide education details & examination details
- Do online fee payment and click on submit
- If candidates are not sure about the details they can apply through Candidate Login ID & password
- Direct link to apply online for SBI PO recruitment and notice pdf is mentioned below
- For Prelims, Main exam and GD & Interview jaggy.in team will update the exam dates and SBI PO admit card.
download past papers:-
you can download the previous papers will help you to clear all the examination without facing any difficulties..
you can log on to the official website of sbi.co.in..


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London Has Fallen 2016 HD-TS x264 MP3-CPG
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Video....: 720x368, 29.97 fps�
Genre: Action | Crime | Thriller
IMDB info
Provider: Lori.Yagami
PLOT: In London for the Prime Minister's funeral, Mike Banning discovers a plot to assassinate all the attending world leaders.
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How to Wear The Outlier Shade in Your Eyeshadow Palette
The 9 Red Lipsticks Dita Von Teese Won't Leave Home Without
There's an outlier in every great eyeshadow compact—a black-sheep pigment that remains untouched as the shades around it disappear with overuse. Maybe it's burnt orange or brick red—bright, beautiful...intimidating. Here, makeup artist Miguel Lledo shows us how to work with the outlier from three of our favorite shadow palettes. The trick, he says, is applying it in tandem with all the other colors in the set.More
With a small eyeshadow brush, sweep the light peach shade across the lid up to the crease and into the inner corner. The neutral shade will anchor bolder layers, Lledo says.
Warning: These Sweaty, Glowy Photos of Celebs Post-Workout Will Inspire You to Exercise


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By Simon Montlake, Special for USA TODAY
PATTANI, Thailand A Muslim insurgency in southern Thailand has grown more violent in the six months since Thai military officers seized power in a coup and promised to end the conflict.
Muslim separatists' attacks on Buddhists in the south have increased in recent months, testing the new government's decision to try a less forceful approach there.
Thai security forces on Wednesday detained seven Muslims suspected of beheading an elderly Buddhist and killing three police officers. Gen. Sonthi Boonyaratglin, the army chief who led the Sept. 19 coup that overthrew Thailand's elected civilian government, said last week that the insurgency had intensified. "Insurgent groups have turned their focus on killing randomly, ending the lives of innocent people," he said.
Then-prime minister Thaksin Shinawatra's failure to pacify the south was among the justifications Sonthi and other coup leaders cited for their decision to take power.
Buddhists make up roughly 95% of the 64 million Thais. In three southern provinces, however, there are 1.7 million Muslims and 300,000 Buddhists. The isolated rural area is populated largely by ethnic-Malays and is a rural backwater.
Since 2004, more than 2,100 people have been killed in political violence in the south.
Zachary Abuza, who studies militant Islam in Asia and tracks the violence in Thailand as a professor at Simmons College in Boston, says the daily death toll has risen to an average of nearly four a day, up from 1.6 in 2006.
The March 15 execution-style slaying of nine Buddhist bus passengers — their Muslim driver was spared by the gunmen after he knelt to pray — sparked national outrage. Now, Buddhists want weapons to defend themselves against militants, raising the risk of sectarian fighting, says Panitan Wattanyagorn, government security adviser and member of a prominent southern Buddhist family.
Beheadings and the burning of victims' corpses — including Buddhist monks and teachers — have brought fear. "I grew up there in the 1960s and I've never seen brutality like this," Panitan says.
The surge in violence in the south comes as the military government is trying to set conditions for restoration of civilian rule and focus security efforts on maintaining stability in Bangkok, the capital.
Since pushing Thaksin from office, the military government has been more cautious in the south — slower to arrest Muslim suspects, quicker to release those arrested without sufficient evidence.
Prime Minister Surayud Chulanont, a former army commander, has apologized for past abuses.
Army officers say separatist groups are attacking more to undermine the conciliatory approach. "They want to destroy stability so that people can't count on the government because there's no justice or security in their lives," says Col. Acra Tiproch, a spokesman for the Army's southern command.
Srisompob Jitpiromsri, a political scientist at Prince of Songkhla University in Pattani, says the insurgents "don't accept a soft or peaceful approach from the government. Their message is that this policy is a failure."
At least three insurgent groups are coordinating daily shootings and bombings of security personnel, government officials, and Muslim and Buddhist civilians.
Thailand has held talks in neighboring Malaysia with exiled Thai Muslims who claim to speak for the rebels, without much success.
Army officers say foreign extremists don't appear to be involved, though Thai insurgents have trained elsewhere in Southeast Asia. Acra says intelligence suggests only 1% of Muslims aid the insurgency and about 2,000 are involved in violence.
Abuza and other analysts say the insurgency is fed by historical, ethnic and religious grievances among ethnic Malay-Muslims, who have kinship ties across the border with Malaysia.
Thaksin stirred resentment in 2004 when he ordered the suppression of a Muslim protest in Tak Bai, a coastal town. Nearly 80 Muslim men later died in army custody. None of the officers involved has been disciplined.
Moderate Muslims say they don't know who is behind the killings and can't trust the government to investigate impartially.
"Muslim people want to cooperate with the government. But their trust has been destroyed," says Ahmad Somboon Bualuang, former member of a government peace panel.
Conversation guidelines: USA TODAY welcomes your thoughts, stories and information related to this article. Please stay on topic and be respectful of others. Keep the conversation appropriate for interested readers across the map.


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A blanket of dense fog shrouding much of the region this morning has reduced the visibility in places to near zero.
The National Weather Service has issued a dense fog advisory until 10 a.m., warning motorists that the fog will remain through the morning commute and visibility in places will be one quarter of a mile or less.
When the fog lifts, skies are predicted to be cloudy, with temperatures in the low 80s. There is a 30 percent chance of showers and thunderstorms this afternoon.


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On this Episode of Simply Geek, we have a special interview with Carl Callewaert from Fund3D games. Tech65's Justin met Carl Callewaert (Game Instructor/Director of Animation/Owner Fundi3D) and had a great chat with him about 3D Gaming industry, developing 3D Games and the technology behind 3D (not the geeky glasses type, but the stuff that's used to make things like WoW such games). They talk about the current status of 3D Gaming and where things might go in the future.
-Justin and Carl Callewaert.


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TOLEDO, OH – Lucas County Commissioners Pete Gerken, Carol Contrada, Tina Skeldon Wozniak were joined by Paul Toth, President and CEO of the Toledo-Lucas County Port Authority to announce a request for proposals regarding the development of the Hotel Seagate site in downtown Toledo, as a hotel to support the Seagate Convention Centre. This is an important step in the redevelopment of a critical downtown corner.
Recognizing that a vital downtown Toledo is crucial to development efforts throughout Lucas County, on November 18, 2014, the Board of Lucas County Commissioners authorized the purchase of the former Hotel Seagate at 127 & 141 North Summit Street, Toledo, Ohio 43604 (Resolution #14-1037).
The building was built in 1970 and is located across the street from Promenade Park, a prime location in downtown Toledo. This once-thriving property steadily deteriorated throughout the years. Since the November 2014 purchase, the former hotel has been cleared of all asbestos and stands ready for the next phase of its redevelopment.
"This is an exciting time for Lucas County, Downtown Toledo in particular, we are building upon the success of multiple development projects in the heart of the city," said Commissioner Tina Skeldon Wozniak.
"Tourism is a billion dollar industry in Lucas County. The commissioners are committed to doing everything we can to build on our strengths in Lucas County and a redeveloped Hotel Seagate is integral to this effort," said Commissioner Carol Contrada.
"Today's announcement is the result of the lasting bonds we have built with the business community. Throughout this process we have sought opinions from a wide-range of stakeholders to ensure that this property is redeveloped as a result of private-public partnerships," said Commissioner Pete Gerken.
Redevelopment of the former Hotel Seagate presents a transformative opportunity for our community because the property is strategically located adjacent to the Huntington Center, the SeaGate Convention Center, and considerable investments that have led to a resurgence of business activity, entertainment, and housing. For example, the Hensville entertainment district, which opened Spring 2016, redeveloped several buildings adjacent to 5/3 Field into a vibrant new entertainment district. ProMedica is also scheduled to relocate its corporate headquarters to Downtown Toledo, bringing several hundred professional staff downtown every day.
The former Hotel Seagate redevelopment's is integral to downtown revitalization efforts. The Board of Lucas County Commissioners is therefore seeking written proposals from qualified developer/operator teams for the planning, design, construction, financing, ownership, commissioning and operation of a limited service, midscale to upper midscale hotel the site of the former Hotel Seagate.
The County envisions that the construction of a new hotel facility or the rehabilitation of the existing building should create and support new demand for the SeaGate Convention Center and Huntington Center facilities, promote larger events in surrounding areas of the City, and possibly spur additional development in the downtown area. The hotel should function in harmony with, and support the activities and events of, the SeaGate Convention Center. The hotel should also exemplify environmentally sustainable technology related to design, construction, and efficient operation, and the eventual development and design of the hotel should allow for maximum flexibility in order to respond to changes in community and market needs over coming decades.
Applicant firms should have development experience and be able to demonstrate financial capacity to undertake the project. Firms interested in submitting a proposal for this project can find the complete Request for Proposals and contract documents at www.co.lucas.oh/Bids.aspx. Bidders must be registered as a vendor via the Lucas County website/PlanetBids. Vendor registration can be completed at http://planetbids.com/portal/portal.cfm?CompanyID=24980. A set of these documents will also be available for viewing at the office of the Lucas County Department of Planning and Development, One Government Center, Suite 800 43604. The deadline for submission is Friday, October 14, 2016 at 12:00 PM. # # #


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"Xbox One X will not do well," says analyst
Jul 20, 2017 | 8 Comments
This is for the players who wants to play with team. You can't progress the game if your a loner. I love the card graphics, card's skill especially when you are using the fusion by adding skills or increase the power of your cards. Its really fun when all of your guildmates join in attacking DarkLord.
You cant trade cards with other players. No PvPs.
Need updates for new features. I hope they will add trading system and PvP.


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I have been dealing with this company for approximately 8 years and they have always been so very kind and willing to work with my families needs. We have all of our insurances through Affordable insurance and we couldn't be happier!
Liars and thieves... I'd tell anyone from personal experience to RUN in the opposite direction of this company!! This place is a RIP OFF, period!! They change things in your policy without proper signatures and will assign undeclared drivers to vehicles on your policy so they can charge you more money. They give you extra coverage you don't need on home owners, which means you end up paying more money for coverage that you don't even need. They quote you one rate in person and then deduct a higher rate from your automatic withdrawal. Your insurance company is suppose to help you get cost effective coverage while protecting your assets; not bleed you for extra money while giving you ineffectual coverage and NOT informing you about it. If your with this company?? Get another quote else where; I did and saved a bundle. These people should be shut down!! When you think of Affordable Insurance in Caldwell, Id. Remember theses words - Theft and Deception
I did not want to but had to give them at least one star to post this review. Hopefully it will save someone else from getting ripped off by this agency.
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Did you know ?
Swapping your high heels for a pair of driving shoes can help you qualify for cheap car insurance by avoiding accidents and getting "safer driver" discounts.
Safety Tip
It is easier to get cheap car insurance with a car that has high safety rating than one without one.
Savings Tip
When you are looking for cheap car insurance, ask if the insurance company offers a policy where they forgive the first accident.


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Hal Gausman
Ph: 360-805-6729
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Ph: 360-805-6726
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Ph: 360-805-6726
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Superintendent Coordinator Assistant
Ph: 360-805-6700, ext. 5707
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Ph: 360-805-6727
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