text:
Mirror mirror on the wall... is this the best fairy tale adaptation of all? The stunning new trailer for Snow White and the Huntsman promises a visual masterpiece
The first teaser trailer for Snow White and the Huntsman has been released, and has already set tongues wagging about the hotly anticipated adaption of the classic fairy tale.
The grown-up version of the children's story boasts Twilight's Kristen Stewart in the title role, with Chris Hemsworth as the huntsman and Charlize Theron as a malevolent evil queen.
Capitalising on the Breaking Dawn buzz, the trailer will surely whet the appetites of K-Stew fans dreading the gap between the next two Twilight installments.
Scroll down to watch the trailer...
Who's the fairest of them all? Kristen Stewart is pale as snow in the new trailer for Snow White and the Huntsman
Steals the show? Charlize Theron's malevolent evil queen is the star of the trailer at least
The trailer opens with a chilling speech from Charlize, who utters in a (convincing) English accent: 'Do you hear that? It's the sound of battles fought, and lives lost. It once pained me to know that I am the cause of such despair. But now their cries give me strength.'
'Beauty is my power,' she adds, before the scene cuts to her 'sucking' the life from a hapless girl before throwing her mercilessly to the ground.
The magic mirror morphs into a cloaked human shape to answer his mistress's question: 'Mirror mirror on the wall, who is fairest of them all?'
The price of beauty: The evil queen sucks the life out of one of her subjects to maintain her youthful looks
Forever young: The queen is prepared to stop at nothing to remain the fairest of all
To no-one's surprise but the queen, he replies: 'You are the fairest, but there is another destined to surpass you. Consume her heart, and you shall live forever,'
Outraged, the queen orders her minions: 'Find me someone who doesn't fear the dark forest to hunt her down.'
The huntsman, played by Chris Hemsworth of Thor fame, is threatened with death unless he captures and kills Snow White.
Break from tradition: Chris Hemsworth, plays the Huntsman, who ends up falling in love with Snow White in this adaption
Though his mission is to bring the evil queen her rival's heart, he ends up becoming her protector and mentor in a quest to vanquish the Evil Queen.
The film also stars Ian McShane, Eddie Izzard, Bob Hoskins, Toby Jones and Ray Winstone among the dwarves.
Produced by Alice In Wonderland's Joe Roth, it is clearly a visual feast, with no expenses spared on sweeping landscapes and stunning effects.
Full interaction: The magic mirror morphs into a human-like form to pass judgement on his mistress's reflection
Surprises in store: It's no wonder that few are brave enough to venture into the dark forest
Though the trailer has already been praised for its design and the beautiful shots, there has been concern that Kristen's portrayal of Snow White would be too similar to that of the role she is most famous for, Bella Swan.
Stewart recently revealed however that she was not initially attracted to the role of Snow White, but became interested after realising the new version was a very different take on the classic character.
She truly does not let her heart cloud her mind,' the Twilight actress told Entertainment Weekly earlier this summer. 'Also I get to have a sword and stuff, and really cool weapons.
Highly anticipated: The official trailer for the film was released today, and has already caused a stir with its stunning visuals
Sweet dreams: The trailer shows the queen stabbing someone in their sleep
'This girl has the amazing ability to channel fear, things that people are typically afraid to do, into this really focused, really charged, driving energy,' she added.
The 21-year-old star looked pale and exhausted as she was spotted filming scenes for her upcoming film, Snow White And The Huntsman, in Surrey this afternoon.
The U.S. actress is currently promoting the latest installment to the Twilight Saga as well as playing the fairytale character in the 2012 movie.
Fury: Charlize plays the villain with admirable gusto
Wearing a brown medieval dress with grubby jeans and boots, Kristen looked worlds away from the Disney character that many people will associate the storyline with, but it was her complexion that looked more downcast.
The actress looked tired and fed up as she hung around on the outdoor set in between takes.
She was still wearing a bandage on her right hand after she injured herself filming horse riding scenes in Wales last week.
Is that the prince? The hero isn't quite who you'd expect in this version
Perhaps Kristen was in pain with the injury as well as feeling a little jet lagged from her trip to Los Angeles.
At one point the brunette was seen holding her hand on her hip and as she waited around for the crew members to prepare the location for her next scene.
But she wasn't alone as she had her hunky co-star, Chris Hemsworth, to keep her company.
Familiar? There is some concern that Kristen's role will be too similar to that of Bella Swan in the Twilight saga
... but the actress has insisted that she chose the role because it promised a daring break from tradition
The Australian actor plays the Huntsman in the highly-anticipated film and certainly looked the part in grubby shirt and trousers, chunky knee-high boots and his scruffy hair pulled back into a ponytail.
The pair were joined by a young actress, who was also dressed in medieval attire.
Kristen was later spotted filming a scene with the girl by the lakeside.
No doubt the Twilight star has jetted back to the UK for the vampire film's London premiere next week.
Calling in the cavalry: The film promises some epic battle scenes
She joined her on/off screen lover Robert Pattinson in Los Angeles last week at a hand and foot print ceremony at Graumans Theatre and also appeared on The Tonight Show With Jay Leno.
The actress is probably looking forward to when the Twilight promotional tour ends and she can concentrate more on filming the fairytale adaptation - her co-star certainly is.
Robert has said it's 'time to move on' from his blood-sucking role and is looking forward to laying low for a little while.
Feeling the strain: The 21-year-old actress has been jetting back and forth from Los Angeles as she promotes the latest Twilight film
Injured: Kristen was still wearing a bandage on her right hand after she hurt herself filming a horse riding scene in Wales last week
Speaking to Marie Claire UK, the British actor said: 'If you're just an empty shell with your face stuck on everything, then there's only so long the hysteria can last.
'I don't like people taking my photo — ever,' he added. 'If there's anything that stresses me out it's people following me around.
'Most actors encourage the attention because they think it will make them have a more lasting career. I don't think that's the case. The more you reveal yourself, the less interesting people find you. Mystery lasts a lot longer, so you just hide.'
Looking the part: Kristen and her co-star Chris Hemsworth were joined by a young female actress who also wore medieval attire
Fairytale adaptation: The actress plays the lead role in the highly-anticipated 2012 film
But Kristen won't be doing a lot of hiding, especially as the first promotional picture for Snow White And The Huntsman was released by Universal Pictures yesterday.
The banner for the upcoming film
centers on Kristen Stewart, and the dark and distorted take on the
Disney classic is clearly evident in the artwork.
Stewart is seen standing in woods, armed with a large dagger.
She is clad in a leather dress and knee-high boots, and turns provocatively to her side.
Racy: Kristen was spotted flashing some flesh on the Wales set of the film back in September
Alongside her in the three-way banner, is Charlize Theron's villainous Evil Snow Queen, also armed with a hefty blade.
Wearing a high-collared cape, ravens ominously circle around her.
Meanwhile, The Huntsman emerges from the tree branches wood wielding an axe, edging dangerously close to Stewart.
Riding high: Kristen was also seen going for a beach ride with co-star Chris Hemsworth at her side
The banner for Snow White and the Huntsman was unveiled by Universal
Pictures today, and centers on Kristen
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12/2/12 - 9:45am
- philosophizingphilosoraptor
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Fellow Monkeys,
Morgan Stanley has been taking quite a beating in this forum, as well as many others. Revenues are down, its compensation, already lacking, is also down, and everyone seems to be pretty downbeat on them.
What is your opinion on Morgan Stanley? Still the #2 IBD? Overtaken by JPM? How does it compare to Goldman? And, above all, is it still a desriable place to work for, especially given its future outlook?
Comments (4)
12/2/12 - 11:11am
- Dreamgazing
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Three Stooges: Curly ClassicsDirector: Archie Gottler, Del Lord, Edward Bernds
Cast: Archie Gottler, Curly Howard, Del Lord, Edward Bernds
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Product Details
- Release Date:
- 02/02/1999
- 0043396028562
- Rating:
- Source:
- Sony Pictures
- Region Code:
- 1
- Presentation:
- Sound:
- [Dolby Digital, stereo]
- Time:
- 1:48:00
- Sales rank:
- 40,392
Special Features
Cast & Crew
|Curly Howard
|Actor,Curly,Dr. Curly Howard
|Marjorie White
|Moe Howard
|Actor,Dr. Moe Howard
|Larry Fine
|Actor,Dr. Larry Fine
|Christine McIntyre
|Dell Henderson
|Dr. Graves
|Dorothy Granger
|Lucille Ball
|Daisy Simms
|Monte Collins
|Arthur Houseman
|Fight Timekeeper
|Bud Jamison
|Gertie Green
|Lulu Banks
|Gino Corrado
|Jeanie Roberts
|Hiccupping Nurse
|Monty Collins
|Mr. Zero
|Vernon Dent
Technical Credits
|Archie Gottler
|Del Lord
|Edward Bernds
|Jules White
|Lou Breslow
|Ray McCarey
Scene Index
0. Episodes
1. A Plumbing We Will Go
2. Men In Black
3. Micro-Phonies
4. Punch Drunks
5. Three Little Pigskins
6. Woman Haters
Customer Reviews
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Panasonic UK was established in 1972.
Since then the company has grown substantially and become a leading supplier of consumer and business related electronics products. Its headquarters is located in Bracknell, Berkshire and this is supported by a national Logistics Centre in Northampton.
There are also separate companies... Show more
Panasonic UK was established in 1972.
Since then the company has grown substantially and become a leading supplier of consumer and business related electronics products. Its headquarters is located in Bracknell, Berkshire and this is supported by a national Logistics Centre in Northampton.
There are also separate companies within the UK responsible for the sales of industrial products such as components and computer peripherals (Panasonic Industrial) and professional video and broadcast products (Panasonic Broadcast).
- Panasonic UK News
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AMD Rolls Out Processors For Mobile Markets
Intel isn't the only chip manufacturer making waves.
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text:
|Publication number
|Publication type
|Application number
|Publication date
|Dec 14, 1993
|Filing date
|Sep 15, 1992
|Priority date
|Sep 18, 1991
|Fee status
|Publication number
|Tadahiko Kubota
|Original Assignee
|Fuji Photo Film Co., Ltd.
|Export Citation
|BiBTeX, EndNote, RefMan
|Patent Citations (4), Non-Patent Citations (2), Referenced by (28), Classifications (15), Legal Events (7)
|External Links: USPTO, USPTO Assignment, Espacenet
The present invention relates to a secondary battery.
As separators for secondary batteries including lithium secondary batteries, porous polymer films have been used hitherto which have excellent permeability to electrolyte solutions. However, due to the porous nature of such a porous polymer film separator, use thereof as the separator in a secondary battery has inevitably had a practical problem that as the battery is repeatedly charged and discharged, dendrites grow and penetrate through pores of the porous film to cause a short-circuit or the dendrites fall from the electrode to cause a decrease in capacity.
JP-A-53-84134 discloses a separator for secondary batteries, such as lithium secondary batteries, which is obtained by grafting an electrolyte solution-permeable polymer onto a porous substrate thereby to fill the pores of the substrate with the polymer. (The term "JP-A" as used herein means an "unexamined published Japanese patent application".) However, this separator film is not suited for practical use because it swells too much. Although a measure for controlling the swelling of the film is disclosed in JP-B-62-17822, this technique has failed to provide a substantial solution to the swelling problem. (The term "JP-B", as used herein, means an "examined Japanese patent publication".)
JP-A-2-82457 discloses a method of producing a separator which comprises impregnating a porous resin film with a monomer and then irradiating the resulting film with ultraviolet rays to polymerize the monomer, thereby to fill the pores of the film with the polymer. However, this method has a drawback that the adhesion between the porous resin and the polymer is so poor that the separator develops voids at the interface between the porous resin and the polymer. Thus, this method has been unable to solve the problem of dendritic growth.
Further, JP-A-3-41107 discloses a separator modification utilizing plasma-initiated polymerization. In general, plasma-initiated polymerization is a technique of polymerizing a gaseous-phase or liquid-phase monomer by irradiating the monomer with a plasma (as described in "Plasma Polymerization" written by Yoshihito Osada et al., published by Tokyo Kagaku Dohjin, Japan). This method, however, has also failed to improve the adhesion between the polymer substrate and the polymer formed by plasma polymerization to a desired level. In addition, even in the case where the polymerization of a monomer was conducted by irradiating a substrate with a plasma to graft-polymerize the monomer onto the substrate, the thus-obtained separator was unable to sufficiently inhibit dendritic growth.
A first object of the present invention is to prevent dendritic growth.
A second object of the present invention is to provide a secondary battery which, when charged and discharged repeatedly, suffers only a slight decrease in capacity.
A third object of the present invention is to provide a secondary battery using a battery separator having excellent dimensional stability.
A fourth object of the present invention is to provide a secondary battery using a battery separator which comprises a porous substrate and a polymer which virtually fills all the pores of the substrate, and in which the adhesion of the polymer to the substrate is excellent.
The above and other objects of the present invention are accomplished with a secondary battery comprising a positive-electrode active material enabling the battery to discharge and to be charged, an electrolyte solution, a separator, and a negative-electrode active material enabling the battery to discharge and to be charged, wherein the separator is obtained by subjecting a porous polymer substrate to plasma treatment and polymerizing a monomer in the presence of the plasma-treated substrate thereby to graft-polymerize the monomer onto the substrate.
FIG. 1 is a sectional view illustrating the construction of the coin-type batteries fabricated in Examples 1 to 10 and Comparative Examples 1 to 4.
The porous substrate to be irradiated with plasma in order to produce the separator employed in the battery of the present invention may be made of a polymer such as a polyolefin, poly(vinyl halide), polyester, polyamide, polysulfone, cellulose, polyurethane, or the like. Preferred examples of the substrate polymer include polyethylene, polypropylene, polybutene, polyisobutylene, ethylene-propylene copolymers, poly(vinyl chloride), poly(1,1-dichloroethylene), poly(chlorotrifluoroethylene), poly(1,1-dichloro-2-fluoroethylene), poly(1,2-dichloro-1,2-difluoroethylene), poly(1,1-difluoroethylene), poly-(1,2-difluoroethylene), polytetrafluoroethylene, poly[(pentafluoroethyl)ethylene], polyhexafluoropropylene, poly(3,3,3-trifluoropropylene), poly(vinyl fluoride), poly(ethylene terephthalate), poly(butylene terephthalate), poly(ethylene adipate), poly(oxy-2,2,3,3,4,4-hexafluoropentamethyleneoxyadipoyl), poly(oxytetraphthaloyloxy-1,4-phenyleneisopropylidene-1,4-phenylene), poly(oxytetramethyleneoxyterephthaloyl), nylon 3, nylon 6,6, nylon 4,6, nylon 5,6, nylon 6, nylon 6,2, nylon 11, poly(oxy-1,4-phenylenesulfonyl-1,4-phenylene), poly(oxy-1,4-phenylenesulfonyl-1,4-phenyleneoxy-1,4-phenylenemethylene 1,4-phenylene), carboxymethyl cellulose, hydroxyethyl cellulose, triacetoxy cellulose, diacetoxy cellulose, and poly(oxytetramethyleneoxycarbonyliminohexaethyleneiminocarbonyl). Of these, polyethylene, polypropylene, ethylene-propylene copolymers, and polytetrafluoroethylene are particularly preferred.
For use in producing the separator to be employed in the battery of the present invention, it is preferable if the porous polymer substrate has a porosity of from 30 to 90%, with the more preferred range of the porosity thereof being from 40 to 90%.
Further, the maximum pore diameter of the porous polymer substrate is preferably from 0.01 to 50 μm, more preferably from 0.01 to 20 μm, and most preferably from 0.01 to 5 μm.
As the monomer for use in producing the separator to be employed in the battery of the present invention, any vinyl compound may be used as long as the compound is polymerizable. It is, however, preferred that the monomer contain a group capable of dissolving in the electrolyte solution to be employed in the battery of the present invention. The group capable of dissolving in the electrolyte solution may be anionic, nonionic, or cationic. Preferred examples of such a group include ethylene oxide groups, propylene oxide groups, ester groups, carbonyl groups, amide groups, amino groups, nitrile groups, alkyl groups, phenyl groups, sulfonic acid groups, phosphoric acid groups, and carboxylic acid groups.
Preferred examples of the monomer to be used for producing the separator include compounds represented by general formulae (1), (2), and (3), alone or in combination thereof, described below. ##STR1##
In general formula (1), R1 represents a hydrogen atom or an alkyl group having from 1 to 3 carbon atoms, and preferably is a hydrogen atom or a methyl group. R2 represents --C(O)--X1 --(CH2 CH2 O)n --R3, --C(O)--Y--(CH2)x --C6 H5, or --CN, in which X1 and Y represent an oxygen atom or --N(R4)--, in which R4 represents a hydrogen atom or an alkyl group having from 1 to 3 carbon atoms. X1 preferably is an oxygen atom, --N(CH3)--, or --N(C2 H5)--. n is an integer preferably from 0 to 50, more preferably from 0 to 23, and most preferably from 0 to 9. R3 represents a hydrogen atom, an alkyl group having from 1 to 3 carbon atoms, an aralkyl group, or an aryl group having from 6 to 14 carbon atoms, preferably, a hydrogen atom, an alkyl group having 1 or 2 carbon atoms, an aralkyl group having from 7 to 10 carbon atoms, or --C6 H5, and more preferably, a hydrogen atom, a methyl group, or C6 H5 group. x is an integer preferably from 1 to 5, and more preferably, from 1 to 3.
Examples of R2 include --C(O)O(CH2 CH2 O)n CH3, --C(O)O(CH2 CH2 O)n --C6 H5, --C(O)OCH2 C6 H5, --C(O)OC6 H5, --C(O)CH3, --C(O)OC2 H5, --C(O)OC3 H7, --C(O)NH2, --C(O)N(CH3)2, and --CN. ##STR2##
In general formula (2), R5 represents a hydrogen atom or an alkyl group having from 1 to 3 carbon atoms, and preferably is a hydrogen atom or a methyl group. X2 represents --C(O)--X3 --C(O)--, in which X3 represents --O--X4 --O--or --O--(CH2 CH2 O)m --. X4 is an alkylene group, preferably one having from 1 to 20 carbon atoms, more preferably, one having from 1 to 10 carbon atoms, and most preferably, one having from 1 to 6 carbon atoms.
m is an integer of 1 or more, preferably from 1 to 50, more preferably from 1 to 20, and most preferably from 1 to 10.
Examples of X2 include --C(O)--O--(CH2 CH2 O)m --C(O)--, --C(O)--O--(CH2)6 --O--C(O)--, --C(O)O--CH(CH3)--CH2 CH2 OC(O)--, and --C(O)O--CH2 C(CH3)2 CH2 OC(O)--. ##STR3##
In general formula (3), R6 represents a hydrogen atom or an alkyl group having from 1 to 3 carbon atoms, and preferably is a hydrogen atom or a methyl group. R7 represents an alkyl group or a group having the formula --CH2 O--R8, in which R8 represents a hydrogen atom or an alkyl group having from 1 to 10, preferably 1 to 5, more preferably 1 to 3 carbon atoms. Preferred examples of R7 include alkyl groups having from 1 to 10 carbon atoms, --CH2 OH, --CH2 OCH3, and --CH2 OCH2 CH3. More preferred examples of R7 are alkyl groups having from 1 to 3 carbon atoms, --CH2 OH, --CH2 OCH3, and --CH2 OCH2 CH3.
Specific examples of compounds of general formula (1) are given below, but the compound is not, of course, limited to these examples. ##STR4##
Specific examples of compounds of general formula (2) are given below, but the compounds are not, of course, limited to these examples. ##STR5##
Specific examples of compounds of general formula (3) are given below, but compounds are not, of course, limited to these examples. ##STR6##
In conducting polymerization, any one of the compounds of general formulae (1), (2), and (3) may be polymerized alone, or two or more of these compounds may be polymerized in combination with one another in an arbitrary proportion.
Water or an organic solvent, preferably water, may be used as a reaction medium for the polymerization.
In the case where water is used as a reaction medium to polymerize a hydrophobic monomer, it is preferred to use a surfactant so that the polymerization is conducted while the monomer is kept in a dispersed or emulsified state.
The process for the plasma treatment and polymerization for producing a separator is explained below. The polymerization of the monomer is conducted while a porous polymer substrate, which has undergone plasma surface treatment, is immersed in a solution or dispersion of the monomer. Although the product of the polymerization of the monomer may contain a non-graft-portion in the polymer substrate, it is preferable for the polymerization product to contain a grafted polymer.
Each step of the process is explained below.
The plasma surface treatment for activating the surfaces of the porous polymer substrate may be conducted by using ordinary discharge treatment. Details of the discharge plasma treatment are given, for example, in J. R. Hollahan and A. T. Bell, Techniques and Applications of Plasma Chemistry, Wiley, New York, 1974 and in other books and publications.
Reactions of high-energy active particles, such as radicals and ions, generated in a discharge plasma take place within an extremely thin surface layer of the polymer substrate and, as a result, C--C bonds or C--H bonds in the molecules of the polymer are cleaved and polymeric radicals are formed. These reactions are followed by reactions between radicals and elimination reactions, thereby to form crosslinks and unsaturated bonds. In some cases, polar groups are newly introduced through reactions with an active gas such as oxygen.
On the other hand, polymeric radicals which have not undergone the above reactions, which are secondary reactions, can take part in graft polymerization when brought into contact with the monomer. In other words, the polymeric radicals can be utilized as graft polymerization-initiating sites.
In producing a discharge plasma, audio-frequency waves having a frequency on the order of from several kilohertz (kHz) to several tens of kHz, radio-frequency waves having a frequency of 13.56 MHz, or microwaves having a frequency on the order of GHz may be utilized.
For producing a separator to be employed in the present invention, high-voltage discharge for the plasma treatment is generally conducted under a reduced pressure, preferably at any of various gas pressures higher than 0.001 Torr and lower than 20 Torr. For example, it is more preferred to conduct the plasma surface treatment by irradiating the polymer substrate with a plasma for a period of from 5 seconds to 10 minutes under conditions of a gas pressure of from 0.01 to 1.0 Torr and an output of from 5 to 500 W.
As a plasma gas source, use may be made of a gas which does not deteriorate the substrate polymer, such as a noble gas (e.g., helium or argon), nitrogen, or a residual inorganic gas.
The step of grafting a monomer onto the plasma-treated polymer substrate is now explained. This graft polymerization can be carried out in various ways, which are generally divided into two methods: (1) a method in which the polymer substrate already activated with plasma is directly treated with a degassed monomer solution to allow the polymer to react with the monomer; and, (2) a method in which the activated polymer substrate is first brought into contact with air or oxygen gas to form peroxides, the peroxides are subsequently pyrolyzed to oxy-radicals, and the resulting polymer substrate is then treated with a degassed monomer solution to allow the polymer to react with the monomer. Both of these two methods are usable for producing a separator to be employed in the battery of the present invention.
It is generally desirable for the graft polymerization reaction to be carried out in vacuo (e.g., under a high vacuum). However, it is possible to conduct the polymerization at a higher pressure (e.g., ordinary pressure) in the absence of air or oxygen, for example, in a nitrogen or argon gas atmosphere.
The temperature for the graft polymerization varies depending on the polymerization activity of the monomer employed. In general, however, the graft polymerization may be conducted at a temperature of from 0� to 100� C., preferably, from room temperature to 90� C.
The reaction time for the graft polymerization is not particularly limited, but a practically preferred range thereof is from 10 minutes to 10 hours.
When the film thus obtained by the above-described process is used as the separator for the battery in this invention, the thus-obtained separator may be impregnated with an electrolyte solution containing a supporting electrolyte dissolved therein.
As the supporting electrolyte, a salt of a Group Ia or IIa element of the periodic table is used. Examples of these salts include LiBF4, LiClO4, LiCF3 SO3, LiPF6, lithium toluenesulfonate, NaClO4, NaBF4, NaCl, LiCl, LiOH, and NaOH. These may be used alone or in combination of two or more thereof.
The solvent for the supporting electrolyte is not particularly limited as long as it dissolves the electrolyte therein. Examples of the solvent include propylene carbonate, butylene carbonate, ethylene carbonate, γ-butyrolactone, dimethoxyethane, tetrahydrofuran, methyltetrahydrofuran, acetonitrile, 1,3-dioxolane, nitromethane, dimethylformamide, dimethyl sulfoxide, and water. These may be used alone or in combination of two or more thereof.
There is no particular limitation on the concentration of the supporting electrolyte in the solution in which the separator is impregnated. However, the electrolyte solution generally has a supporting electrolyte concentration such that the separator film after impregnation has an ionic conductance of preferably 10-9 S/cm or higher, more preferably 10-6 S/cm or higher, most preferably 10-4 S/cm or higher.
Examples of the positive-electrode active material for use with the separator in the battery of the present invention include oxides, sulfides, and selenides of manganese, molybdenum, vanadium, titanium, chromium, niobium, cobalt, and nickel, active carbon (described in JP-A-60-167280), carbon fibers (described in JP-A-61-10882), polyaniline, polymers of amino group-substituted aromatic compounds, polymers of heterocyclic compounds, polyacene, and polyyne compounds. Particularly useful are active carbon, γ-MnO2 (described in JP-A-62-108455 and JP-A-62-108457), a mixture of γ-β-MnO2 and Li2 MnO3 (U.S. Pat. No. 4,758,484), amorphous V2 O5 (JP-A-61-200667), V6 O13, Lix Niy CO.sub.(1-y) O2 (0.05≦x≦1.10, 0≦y≦1) (JP-A-1-294372), MoS2 (JP-A-61-64083), TiS2 (JP-A-62-222578), polyaniline (JP-A-60-65031, JP-A-60-149628, JP-A-61-281128, JP-A-61-258831, JP-A-62-90878, JP-A-62-93868, JP-A-62-119231, JP-A-62-181334, and JP-A-63-46223), polyacetylene (JP-A-57-121168, JP-A-57-123659, JP-A-58-40781, JP-A-60-124370, JP-A-60-127669, and JP-A-61-285678), and polyphenylene.
In the electrode active materials, an electrically conductive material such as carbon, silver (JP-A-63-148554), or a poly(phenylene derivative) (JP-A-59-20971) and a binder such as Teflon may generally be incorporated.
Examples of the negative-electrode active material for use in the battery of the present invention include lithium metal, polyacene, polyacetylene, polyphenylene, carbon (JP-A-1-204361), calcium metal, sodium metal, aluminum, magnesium, zinc, niobium, and alloys of these metals, particularly lithium alloys. Examples of such lithium alloys include aluminum or magnesium alloys (JP-A-57-65670 and JP-A-57-98977), mercury alloys (JP-A-58-111265), Pt alloys (JP-A 60-79670), Sn-Ni alloys (JP-A-60-86759), Wood's metal alloys (JP-A-60-167279), electrically conductive polymer alloys (JP-A-60-262351), Pd-Cd-Bi alloys (JP-A-61-29069), Ga-In alloys (JP-A-61-66368), Pb-Mg alloys (JP-A-61-66370), Zn alloys (JP-A-61-68864), Al-Ag alloys (JP-A-61-74258), Cd-Sn alloys (JP-A-61-91864), Al-Ni alloys (JP-A-62-119865 and JP-A-62-119866), and Al-Mn alloys (U.S. Pat. No. 4,820,599). Of these, lithium metal, its alloys with Al, and carbon are useful.
In the separator employed in the battery of the present invention, the amount of the polymer grafted onto the polymer substrate is preferably 0.001 to 20 mg/cm2, more preferably 0.01 to 10 mg/cm2, and most preferably 0.1 to 5 mg/cm2.
As described above, in producing the separator to be employed in the battery of the present invention, a polymer layer can be efficiently formed on the surfaces of a polymer substrate. The separator thus formed has advantages in that the polymer layer formed on the substrate never peels-off the substrate or dissolves away over a prolonged time period (or even when the separator is subjected to various treatments), and the separator retains its initial performance over a prolonged time period. Moreover, in producing the separator, the thickness of the polymer layer to be formed on a substrate can be controlled freely, from an extremely small to a large thickness, by suitably selecting polymerization conditions (temperature, time, monomer temperature, surfactant amount, etc.). A further advantage of the separator is that in the polymer layer-forming step, the substrate is less damaged as compared to the case of polymer film formation utilizing electron beams or the like and, hence, the properties originally possessed by the substrate are not substantially impaired.
Therefore, due to the use of the separator, the secondary battery of the present invention can show excellent charge-discharge cycle characteristics and is substantially free from internal short-circuiting and dendritic growth.
The present invention will be explained below in more detail with reference to the following examples, but the invention is not to be construed as being limited thereto. Unless otherwise indicated, all parts, percents, ratios and the like are by weight.
Plasma irradiation was conducted using plasma irradiator Model BP-1 manufactured by Samco International Kenkyusho as follows.
A porous polypropylene film (trade name, Julagard 2500; manufactured by Polyplastics Co., Ltd., Japan) having dimensions of 6 cm by 6 cm was placed on an electrode plate, and the pressure in the plasma irradiator was reduced to 0.675 Torr while nitrogen gas was continuously introduced therein at a rate of 30 ml/min. The polypropylene film was then irradiated with a plasma at an output of 50 W for 60 seconds. Subsequently, the pressure inside the irradiator was raised to ordinary pressure by introducing nitrogen gas, and the polypropylene film was then taken out from the irradiator. This plasma-treated polypropylene film was immersed in 200 g of an aqueous monomer solution which contained, as a monomer, 30 g of compound 1-2 as specified hereinabove and had been heated beforehand to 65� C. The monomer was then allowed to react at 65� C. for 3 hours. The polypropylene film was then taken out from the resulting monomer solution, subsequently washed with 1 liter of water for one day to remove the monomer which has been unreacted, and then dried. It was ascertained that a graft polymer had been formed on the resulting film in an amount of 2.2 mg per cm2 of the film. Further, examination with an electron microscope revealed that the pores of the porous polypropylene film had been clogged.
This film was then immersed in a 1-mol/liter LiBF4 solution in propylene carbonate/dimethoxyethane=1 (by volume). As a result, although the film swelled in the direction of thickness (dry film thickness 31 μm, after-immersion film thickness 58 μm), no swelling was observed in either of the length and width directions. The film after immersion had an ionic conductance of 1�10-3 S/cm.
Using this film as a separator, 100 batteries having a construction as illustrated in FIG. 1 were fabricated. In FIG. 1, numeral 1 denotes a positive-electrode active material, numeral 2 denotes a nonwoven fabric impregnated with an electrolyte solution, numeral 3 denotes a negative-electrode active material (lithium), numeral 4 denotes a stainless-steel case, numeral 5 denotes an insulating synthetic rubber, and numeral 6 denotes the separator. These batteries were subjected to a charge-discharge test in which charge and discharge were conducted between 1.5 V and 3.5 V at a constant current of 2 mA. No internal short-circuiting was observed.
Further, some of the batteries that had undergone 100 cycles of charge and discharge were charged and then disassembled, and the lithium surfaces were examined with an electron microscope. As a result, no dendritic growth was observed.
The positive electrode employed in each of the above-fabricated batteries had been prepared by mixing 90 parts by weight of V6 O13 as a positive-electrode active material, 5 parts by Weight of Teflon as a binder, and 5 parts by weight of carbon black as an electrically conductive material to prepare a positive-electrode active material mixture, and then pressing the mixture into a pellet having a diameter of 1.3 cm. As the negative electrode, a lithium metal disk having a diameter of 1.3 cm was used which had been obtained by die-cutting.
Polymer-grafted films were prepared in the same manner as in Example 1 except that the monomer, the output and time for plasma irradiation, and the temperature for polymerization were changed as shown in Table 1, and in the case of using a hydrophobic monomer, the following surfactant A was used for dispersing the monomer in an amount shown in Table 1. ##STR7##
The grafted polymer amount and ionic conductance for each polymer-grafted film are shown in Table 1. In the same manner as in Example 1, batteries were fabricated using each of the films and were subjected to a charge-discharge test. No dendritic growth was observed in any of the batteries.
TABLE 1__________________________________________________________________________ Plasma Polymeri- GraftedMonomer irradiation zation polymer IonicExamplecompound No. Water Surfactant* Output time temperature amount conductanceNo. (amount (g)) (g) (wt %) (W) (sec) (�C.) (mg/cm2) (S/cm)__________________________________________________________________________1 1-2(30) 170 -- 50 60 65 2.2 1.0 � 10-32 1-2(30) 170 -- 40 60 65 2.5 1.1 � 10-33 1-6(25) 175 -- 40 60 65 3.1 1.2 � 10-34 1-9(30) 170 8 50 90 65 2.7 0.9 � 10-35 1-11(30) 170 10 40 60 65 2.6 1.0 � 10-36 1-2(36), 2-3(4) 160 10 50 90 60 2.1 1.0 � 10-37 1-2(36), 2-7(4) 160 10 50 60 65 2.0 1.0 � 10-38 1-9(36), 2-8(4) 160 10 50 60 65 2.3 0.9 � 10-39 1-11(36), 2-6(4) 160 10 50 60 65 3.0 1.0 � 10-310 1-2(36), 2-3(2), 160 10 50 60 65 2.7 1.0 � 10-33-1(2)__________________________________________________________________________ *Based on the amount of monomer
One hundred batteries were fabricated in the same manner as in Example 1 except that untreated Julagard 2500 was used in place of the polymer-grafted film.
The batteries thus obtained were subjected to the same charge-discharge test as that in Example 1. As a result, two of the batteries suffered internal short-circuiting.
Further, some of the batteries that had undergone 100 cycles of charge and discharge were charged and then disassembled, and the lithium surfaces were examined with an electron microscope. Dendritic growth was observed.
A porous polypropylene film (Julagard 2500) having dimensions of 6 cm by 6 cm was irradiated with electron beams at a dose of 20 Mrad. This film was immersed in the same monomer solution as that used in Example 1, and polymerization and washing were then conducted in the same manner as in Example 1. As a result, a film onto which a polymer had been grafted in an amount of 5 mg/cm2 was obtained. After being dried, this film was immersed in the same electrolyte solution as that used in Example 1. As a result, the film not only swelled in the direction of thickness (dry film thickness 32 μm, swelled film thickness 61 μm), but also swelled in the length and width directions by 10%.
30 parts by weight of compound 1-7 as specified hereinabove was mixed with 70 parts by weight of a 1-mol/liter LiBF4 solution in propylene carbonate/di-methoxyethane=1/1 (by volume). Thereto was added 2,2-methoxy-2-phenylacetophenone as a photosehsitizer in an amount of 0.2% by weight based on the amount of the monomer. A polypropylene nonwoven fabric was immersed in the thus-prepared solution and then irradiated with ultraviolet rays for 10 minutes using a 200-W UV lamp, thereby polymerizing the monomer. Batteries were fabricated using the resulting film and subjected to a charge-discharge test in the same manner as in Example 1. The batteries that had undergone 100 cycles of charge and discharge were charged and then disassembled in an argon atmosphere, and the lithium surfaces were examined with an electron microscope. Dendritic growth was observed.
Graft polymerization was conducted in the same manner as in Example 1 except that 200 g of an aqueous solution containing 30 g of compound B (specified below) and 29 g of surfactant A used above was used as an aqueous monomer solution. ##STR8##
As a result, a film onto which a polymer had been grafted in an amount of 1.8 mg/cm2 was obtained. This film had an ionic conductance of 3.0�10-5 S/cm. Batteries were fabricated using this film and subjected to a charge-discharge test in the same manner as in Example 1 except that a constant current of 0.1 mA was used. After the test, the lithium surfaces were examined and, as a result, dendritic growth was observed.
While the invention has been described in detail and with reference to specific embodiments thereof, it will be apparent to one skilled in the art that various changes and modifications can be made therein without departing from the spirit and scope thereof.
|Cited Patent
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|Sep 18, 1979
|Compagnie Generale D'electricite
|Poly (2-hydroxyethylmethacrylate) membranes for electrochemical use and the manufacture thereof
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|May 28, 1993
|Oct 10, 1995
|The University Of Tennessee Research Corporation
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|Apr 19, 2004
|Oct 23, 2007
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Utah Jazz: Kyrylo Fesenko hopes he'll play bigger in Game 2
PLAYA VISTA, Calif. — With all of the height hype and hoopla about the Los Angeles Lakers' length advantage, one not-so-small thing has seemingly managed to go unnoticed.
Between the two teams, the Utah Jazz have the tallest player.
Kyrylo Fesenko, Utah's 7-foot-1 starting center, just didn't play like it in Game 1.
And — after grabbing only one rebound, scoring all of two points and blocking nary a Laker shot in 13 minutes — he knows it.
"I'm bigger than they are, so it's not about the size or the weight," said the 300-pound Fesenko at practice Monday.
It is, he added, about being "more aggressive" and establishing himself as a big force early on. Kinda like he did for periods while being recognized for his beefy and big presence and solid play during the Denver series rather than for his one-liners and goofy antics. You know, when he even got Carmelo Anthony to repeat his name in frustration.
"I want to get back on track," Fesenko said, "play my game, get much more physical, play better defensively and just do my job."
For Fesenko, that includes: "Definitely more rebounds, more blocks, more fouls — I have a long way to go, and I'm not happy with my (Sunday) game."
Jazz coach Jerry Sloan acknowledged that his third-year center has plenty of room to improve, but for now, he's sticking with this Plan B in the injured Mehmet Okur's absence.
"We haven't cut him. It sounds like we just cut the guy with everybody's questions," Sloan quipped. "No, he'll start (Tuesday) and hopefully play much better."
Fesenko admitted that he struggles when matched up with the quicker Pau Gasol, one of the Lakers' 7-footers. Gasol had 25 points, 12 rebounds and five blocks in Game 1.
Then again, who doesn't struggle against Gasol?
But Fes likes his matchup with Andrew Bynum, the other 7-foot Laker. He plans on trying to body the banged-up L.A. big more before he gets the ball while keeping him away from the post, where he's tougher to handle.
Sloan called Fesenko's Game 1 flop "the hard knocks of the NBA," but the coach says the key to bouncing back is simply to realize what the Jazz are trying to do and then to do it.
"We want him to succeed," Sloan said. "... But he has to do the work."
The 23-year-old Fesenko isn't the only inexperienced guy Sloan has had to reteach and remind what the team has tried to run over the years.
"If he knows what we're doing, he has to do it," Sloan said. "And that's all younger players, that's not just him. You run into that with a lot of young players, and some guys are faster picking it up than others, but that's the way your patience gets tested in working with him."
And Fesenko, Mr. Patience-Tester himself, understands he's capable of contributing more than he did Sunday.
"I need to play better," he said. "I know I can."
The Nuggets do, too. Now the Jazz just need the Lakers to realize it as well.
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In collaboration with Spanish performance artist Alicia Framis, United Nude has come up with a shoe for the "Moon Life" project, based on the premise that humans will one day live in outer-space. The carbon-fiber shoe comes flat, packed with assembly instructions and interchangeable uppers that you can switch out for a custom look. Apparently, these heels are actually meant to be worn, although they look like a broken ankle waiting to happen. If this is the future, pass us the key to a bomb shelter. We're quite happy to avoid the upcoming leaps ahead in shoe technology, and content to wear our non-assembly shoes of the past in peace. (Ecouterre)
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Walters Newswire
Comprehensive Real-Time News Feed for Walters, OK.
Results 1 - 15 of 15 in Walters, OK
WALTERS, OK The Cotton Electric Charitable Foundation will distribute more than $25,000 to various organizations with money raised by co-op members. The program, Operation Round Up, rounds up electric bills to the nearest dollar. Comment?
Oklahoma declares state of emergency in 9 southern counties w/Photo
... winds. Initial reports show damage in numerous communities including Apache, Cyril, Lawton, Maysville and Walters. Further damage assessments are ongoing. The executive order allows state agencies to make emergency purchases related to disaster ... Comment?
Emergency declared in 9 Oklahoma counties after storms w/Photo
... winds to the state. Lamb said in a news release that damage is reported in Apache, Cyril, Lawton, Maysville and Walters and that damage assessments are ongoing. The order allows state agencies to make emergency purchases related to disaster relief ... Comment?
Flash flooding strands motorists, closes park in southern Oklahoma w/Photo
... at Apache and Pauls Valley recorded more than 5 inches of rain since midnight, while sites at Ketchum Ranch and Walters caught about 4 inches, according to the Mesonet. There is a 20 to 40 percent chance of storms Monday, with a marginal risk of ... Comment?
OSF performs at Magnolia Festival w/Photo
From left, Matt Rizzo, Allyson Thomas, Jace Caldwell, Rebecca Ford, Cortney Baker, Deborah Clements, Bella Walters, and Jarrett Self rehearse using their light sabers for "A Tribute to the Force Awakens." The Oklahoma Shakespearean Festival partnered with the Magnolia theatre to kick of the summer during Durant's very own Magnolia Festival. Comment?
Woman Hospitalized After Driving Through Pasture In Cotton County w/Photo
Misti Lane, 37, of Wichita Falls, Texas, was driving through a field a little more than a mile east of Walters when she lost visibility due to high weeds. Walters drove down an embankment and into a dry creek bed. Comment?
Geneseo State men's hockey team honors fallen teammate w/Photo
(Keith Walters via AP). In this photo taken Nov. 8, 2014, and provided by Keith Walters, Geneseo's Matthew Hutchinson skates with the puck during an NCAA college hockey game against SUNY Plattsburgh in Geneseo, N.Y. When the Geneseo State Knights ... Comment?
2 teens injured in rollover wreck near Walters w/Photo
ABC, 24/7, Telemundo - Oklahoma Highway Patrol says a 17-year-old driver and his 16-year-old passenger were southbound on County Road N2610, a gravel road just north of Walters, when the vehicle went into a broad slide and started to roll. The 2004 Mazda the two teens were in rolled one and three-quarter times, it hit a fence and a tree while rolling. Comment?
Bulldogs advance after 7-6 win over Geronimo. w/Photo
... to the second round in the Cache Tournament. They will face Del City today at 4 p.m. after Del City defeated Walters in yesterday's first round. If the Bulldogs win that game, they will play at 8 p.m., weather permitting. A loss today against Del ... Comment?
Prosecutors say man accused in 1997 cold case has history of sexual assaults w/Photo
... motive." In the first incident, Palma is accused of illicitly touching an 8-year-old girl in either 1979 or 1980 in Walters. He allegedly entered the victim's home through a bedroom window during the night. Records show he was never charged with a ... Comment?
Emergency services expand in Cotton County w/Photo
... spread the equipment around the county, so it can be accessible to their main population areas. Fire departments in Walters, Temple, Devol and Randlett will each receive three portable generators, a permanently mounted generator and a light pole so ... Comment?
Phillip Wayne Spence Phillip Wayne Spence, 78, of Grapevine, died Thursday, Dec. 3, 2015, at a Grapevine hospital from complications due to pulmonary fibrosis.Wayne was born Nov. 15, 1937, in Walters, Okla. Comment?
Kingston wins playoff game over walters w/Photo
The Kingston Redskins, , used their big play passing game and some timely running plays to overpower the Walters Blue Devils 56-26 Friday night at Kingston in the first round of the 2A playoffs. "I am so pleased with the win, the team played with such great effort," said Kingston Head Football Coach John Caraway. Comment?
SE downs OK Baptist, 40-27 w/Photo
... took a 13-0 lead. Akinwande got a rushing touchdown with 1:39 to go in the quarter to stretch the advantage to 20-0. Walters made his first field goal of 25 yards in the second quarter for a 23-0 lead. OBU would finally find an answer with a rushing ... Comment?
Richard Moore - Dick' Lawrence w/Photo
... Lawrence, 91, passed away Wednesday, Aug. 26, 2015, at the Teague Nursing Home. He was born Sept. 6, 1923, in Walters, Okla., to Richard W. and Eunice Pearl Moore Lawrence. The Lawrence family moved to Teague in 1939 where Dick graduated from Teague ... Comment?
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Snype nodded. "Yeah it's something along those lines. Don't worry, the person we're supposed to be helping volunteered. It's a class after all... ah, I guess you'll need a ride over the swamp. Wouldn't want you to get any muck on your figure." Snype said. Hilda eventually moved on through the swamp with the rest of the class. They didn't have to jump into the water yet thankfully.
Len sighed. "Yeah. I probably will... I'm sure it's nice to be with someone like that... I'm not worried about it though. I don't usually think about that kind of thing very much." Len said, looking at Alexis for a moment as she patted his arm. He was lost in thought for a split moment. He snapped back into reality when he saw the class moving further into the swamp. Len decided to surprise Alexis a bit this time. Len picked Alexis up and proceeded to place her on his back so that she could get a good grip on him.
"Well if your willing to give this ride another go, Let's head to the swamp!" Len said happily.
Mark had never heard of the name Zekrom before... it sounded like a pretty powerful name to him though. He was a firm believer of legendary Pokemon himself, even though he had never seen one before.
"Well, whatever it was, it sure is powerful. Maybe there are other pokemon that can do that kind of thing. You never know... still though, let's head on into the swamp." Mark said as he started to follow the class. He noticed Snype and Thyme together.
"Hey Thyme, You can rest on my shoulder if you want. I doubt Bri would have fun washing you if ya got dirty huh?" Mark said.


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My navigation screen is black and the radio buttons won't work. I can still use my radio through the steering controls but not the CD player and the radio has noise spikes randomly, if it is up high the noise drops down, if the radio is turned down, it spikes way up. The navigation screen gets a little brighter when the radio spikes up... I loved my Yukon until recently when the speedometer gauge had to be replaced last year and the sunroof has fallen apart...Time to trade it in, but I owe twice as much as it books!
navigation/radio on 2005 GMC Yukon Denali
1 answer
ANSWER by Visitor,
February 06, 2011
I have had the same problem. Advised to simply replace it with an after market because of all the problems he has seen with these.
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text:
Busy junction outside Victoria Terminus (Chhatrapati Shivaji Terminus), UNESCO World Heritage Site, Mumbai (Bombay), Maharashtra, India, Asia
Credit: Stuart Black / robertharding
Creative #: 158318945
License type: Rights-managedRights-managed products are licensed with restrictions on usage, such as limitations on size, placement, duration of use and geographic distribution. You will be asked to submit information concerning your intended use of the product, which will determine the scope of usage rights granted.
Collection: robertharding
Max file size: 5,120 x 3,427 px (17.07 x 11.42 in) - 300 dpi - 5.17 MB
Release info: Not releasedNot released: This imagery has no model or property release. Any commercial use requires additional clearance from third parties.
- 19th Century Style,
- Architecture,
- Building Exterior,
- City,
- Color Image,
- Day,
- Famous Place,
- Horizontal,
- Incidental People,
- India,
- Maharashtra,
- Moped,
- Mumbai,
- On The Move,
- Outdoors,
- Photography,
- Railroad Car,
- Railroad Station,
- Road,
- Taxi,
- Tourism,
- Traffic,
- Transportation,
- Travel,
- Travel Destinations,
- UNESCO World Heritage Site,
- Victoria Station - Mumbai,
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Busy Junction Outside Victoria Terminus Maharashtra India Asia Stock Photo19th Century Style,Architecture,Building Exterior,City,Color Image,Day,Famous Place,Horizontal,Incidental People,India,Maharashtra,Moped,Mumbai,On The Move,Outdoors,Photography,Railroad Car,Railroad Station,Road,Taxi,Tourism,Traffic,Transportation,Travel,Travel Destinations,UNESCO World Heritage Site,Victoria Station - MumbaiPhotographer Stuart Black / roberthardingCollection: robertharding


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