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The Hamilton Spectator has nabbed a National Newspaper Award.
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I guess you could call it a mid-life crisis.
I'd never heard of the mystery of the missing land registry book until I appeared as guest speaker at the Stoney Creek Historical Society's February meeting, to talk about the history of The Hamilton Spectator.
I was so impressed at the zeal of this group, at its healthy and rapidly growing membership. They behave as though they've been entrusted with the commission of some great purpose, and they're happily picking up crusaders along the way.
A great purpose indeed. Greg Armstrong puts it directly, with a hint of manifesto, in his Message From Our President on the society's website: "We exist to capture and preserve the history of Stoney Creek for current and future generations."
That's a noble charge, but as with any such spirited group, part of the hold is a legendary challenge, a recovery quest, a sense of something lost that must be found.
And that something? The aforementioned land registry ledger. It's missing, as I found out at the meeting. By now, it's society lore.
It's been missing for 10 years, and the society would dearly love to get it back.
When you visit the SCHS's offices at the old Stoney Creek Alliance Church building on Highway 8, what strikes you immediately is the dynamic collection of materials.
Under glass are Billy Green's drum and his leather pants; on the walls are many framed documents and photos; in the big rollout compartments of the shelving units at the back are these sheaves of buff paper, yellowing with time, bound into larger books or ledgers, tied in a bow, beautifully preserved. On the paper are ink entries in a very neat hand, with dates, names and locations.
These are Stoney Creek land records — registration of deeds, titles, plot surveys, subdivisions. They date back to the very beginning.
The society has all the Saltfleet and Stoney Creek records, detailing all land transactions in the township from the late 1700s to1955.
Before 2012, when it moved in to its current space, the society had no permanent home and stored its material in the boardroom of a friendly local business, says Armstrong.
"We didn't do check-in, check-out on the materials," he says. "They weren't there to be borrowed." But people could come in and consult the documents; visits worked on an honour system.
SCHS members are not thinking the worst. Perhaps someone wasn't aware of the policy and removed the missing land records in ignorance, meaning to return them but then forgetting.
Whatever the case, they're gone. They have not been seen since 2005.
"We interviewed people," says Greg, "but nothing came up."
The book that is missing is a critical one. It details the land development and changes of ownership for downtown Village of Stoney Creek, as that area was taking shape, 1905 to 1950s.
These records cover such pivotal areas as Lake Avenue, the Gage property, the Jones house, and the period was one of growth spurt in the village centre.
"The grant is right from Concession 1, 2, 3 and 4 and lots 23, 24, and 25," says Greg. The one square mile heart of town.
It's a little like a Superman museum missing Action Comics 1.
Judy Green of the SCHS (married to Doug Green, descendant of Billy Green) staffs the society's space now — it's open from 1 to 4 p.m. Tuesdays and Thursdays — and says that whoever has the land records right now might not realize they have it.
"They would be loose sheets maybe still covered in brown craft paper," she says.
What might have happened, says member Kathy Wakeman, is that someone had the records and left them to someone else who now has no idea what they have.
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The society has put out calls before, with no luck. We'll keep our fingers crossed.
firstname.lastname@example.com 905-526-3306
Location, ST | website.com
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|By John Cowan
Article Rating:
|January 1, 2013 02:00 PM EST
Another year, another dollar… or something like that. It's time for an update on the 6 things I think I think for Infrastructure-as-a-Service (IaaS) in the coming year!
1. Hybrid Cloud Computing
2012 Perspective: Hybridization WAS key in 2011 and I'm doubling down in 2012. If you've paid attention to the consolidation in the industry, you'd best do the same. The big boys are snapping up anything that smells like bridging the enterprise to the multi-tenant host. Look for this trend to intensify.
2013 Perspective: VMware buys DynamicOps. Red Hat buys ManageIQ. Cisco buys Cloupia. Consider the consolidation trend intensified. The big question for 2013 is what the big boys have in mind for the cool technologies they've acquired in 2012. Whatever they might have in mind, the signal from the customer is clear. Hybrid cloud computing is considered critically important to wide-scale adoption of cloud computing in general. As I highlighted earlier this year, as big as the cloud computing market is becoming it still pales in comparison to private IT operations. Hybrid cloud computing is correctly viewed as a technology tap to this underlying market.
2. Cloud Federation & Interoperability
2012 Perspective: I've spoken with some pretty big names in the business and scale is an issue with their regional plays in the market. The challenge in 2011 for cloud federation was the degree of difficulty associated with interoperability. There was much progress on this front in 2011 but I think before broad based federation goes from concept to reality there needs to be more plumbing. 2012 will be the year real interoperability tracks are laid as a foundation for scalable cloud federation.
2013 Perspective: We as an industry had the opportunity to lay down tracks for real cloud federation and interoperability at this time last year. What happened was rather disappointing. Basically, industry titans from OpenStack, Amazon, Citrix, and others all postured. I remember sitting in the crowd at GigaOm Structure when the first official shots were fired on the subject of API standardization. What could have been a wonderful opportunity to seize the moment and end vendor lock-in before it ever started in cloud computing, big vendors did what they do best. They opened up their respective Kimonos and bragged about the size of their case studies. What a (albeit entertaining) waste of time and opportunity.
Because we all anticipate the cloud market, particularly IaaS, growing at a serious CAGR in 2013 there will be growing customer pressure to allow the movement and billing transfer of workloads between independent cloud operators. The opportunity for a new or existing company to emerge with a solution to this problem will become significant in the coming year.
3. Cloud Ecosystem Enablement
2012 Perspective: VMware unveiled its plans to stitch together Vcloud operators at its big VMworld shindig, but this wasn't the only giant making big bets on the cloud ecosystem concept. Equinix, one of the world's largest data center operators, hatched is master plan for a 'Marketplace' of Platform Equinix Partners and Synnex, one of the most powerful IT Distributors in North America took a huge step with its Cloudsolv application and services portal. Watch what these three companies do in 2012 to drive ecosystem growth.
2013 Perspective: Dell, HP, Cisco, Arrow, Avnet, Telefonica, Singtel…just to name a few. Billions in unstructured cloud business potential spanning distribution, hardware and telecoms just waiting to be harnessed. The lure of these types of captive markets will push the envelope on cloud ecosystem enablement despite a big challenge encountered in 2012. That big challenge was the relative learning curve incurred when you cross-pollinate large singularly focused business units.
4. Emerging Cloud Communities
2012 Update: By the middle of the 2nd quarter I was beginning to worry about this prediction. Was I going a bit too far out on a limb? Then, bang! VMware announces the big deal with the NYSE. Wow. Talk about going big or going home. The NYSE community cloud has a lot of eyes on it. A large number of other vertical deals are hanging in the balance, hoping to learn what not to do when details of the NYSE project become more public. I think this VMware play will be a big success and in 2012, you will see many other big players follow suit.
2013 Perspective: Do you hear that sound? No? I didn't think so. There's no sound in a vacuum that is the lack of follow up from the big NYSE deal in 2011. No big pharma cloud. No big banking cloud. No big offshore financial cloud.
How come?
Would-be community cloud enablers in 2012 figured out what they needed to figure out, which they are hoping to do in 2013. What they need to figure out has nothing to do with the technology and everything to do with operational and contractual concerns. The commonality of vertical market integration resolves certain compliance risks, but it doesn't mean private IT operators are ready, suited or even capable of offering a legitimate outbound customer service. Ask any CFO or CEO of a publically traded company about the idea of taking on the liability risk created by a new service that, oh by the way, has nothing to do with existing strategy. At a minimum in 2013 look for new corporate structures to emerge in order to facilitate offering community clouds as a service.
5. Channelization
2012 Perspective: I am still a firm believer in the channel and I'm still banking my company's future on it. However, the Channel failed to capitalize on the cloud opportunity in 2011 the way I thought it would. Don't get me wrong, the needle definitely moved. But the cloud operators and the broader channel are still separated by an expertise gulf that is limiting how much cloud money flows via the intermediary. The investment from the IaaS providers continues to be there. Find me one IaaS services or software provider that doesn't showcase a channel program today. 2012 will see the gulf shrink and the channel heat up because Distribution will hit its stride and carry with it more evidence of the gold rush I saw last year.
2013 Perspective: The channel didn't emerge as the boon of cloud computing adoption in 2012, but it continued to make significant progress. Cloud Sherpas recently raised $40M on a bet that it had figured out the model to integrate cloud into the enterprise. That's not a small bet on the channel intermediary concept. There were other big wins in the market too.
In 2013 you will see vendors get very serious about forcing channel intermediaries to declare their allegiance. Programs are maturing and dollars are flowing inbound to support the intermediary to the customer. This is a sure sign that we are on the cusp of growing the cloud wave in a big way.
6. IaaS Futures Market
2012 Perspective: Spot market concepts made progress in 2011 but as expected were not able to truly capture the imagination of the market. However, the groundswell around commodity compute resource trading is gaining momentum. And in 2012 look for general progress in this area with a few players coming out of the woodwork to surprise some.
2013 Perspective: Fact – trading compute contracts is going to happen. If you trust nothing else I write, trust me on this.
As predicted, a few players came out of the woodwork on this. Specifically, the Eurex and Zimory (via TSystems) in Europe announced that they had formed a partnership to build a trading platform in 2013.
What is unclear is exactly how this is going to happen. How will the market be organized? Look for clarity to emerge in 2013 on this subject.
Since last year's 6.1 bonus prediction was such a hit (um, cloud brokerage, anyone?) I will keep with the new tradition. Here's my scoop: Keep an eye on the fall of old empires. The world economy is definitely not what it was two years ago, but neither are some of these tech titans of yesterday:
Cloud Computing – the agent of change – can mean rebirth or extinction for some of the biggest companies to dominate the tech landscape in the last 30 years. Look for significant strategic moves by some of the giants as they posture for survival in the new era.
Have a great 2013!
The post 6 things I think I think for IaaS in 2013 appeared first on 6fusion.
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text:
Lou Smit's Reasons
Posted in the JonBenet Ramsey Forum
#1 Feb 22, 2014
I have read a ton of stuff on JonBenet but can someone tell me what Lou Smit's reasons were for suspecting an intruder? I mean, where can I read a discussion of reasons? Not someone yelling at me.
#2 Feb 22, 2014
Can't help with a link. I do know however that Lou was as self-described a Christian. After interviewing John Ramsey, his initial conclusion was that John was being upfront and not lying about the crime. So, it was my impression that he more or less went with his instinct and fit the crime to his belief in the innocence of John and the family's profession in their belief in Christ as their Savior. I do believe Kolar addressed that in his book, Foreign Faction.
Since: Mar 08
Location hidden
#3 Feb 22, 2014
Smit from Steve Thomas's perspective: "Three days later at a detective briefing, Smit made his first appearance, greeting us all and taking a seat along the west wall. We went around the table to update our findings. Finally it was his turn. He had been around only about seventy-two hours, not anywhere near long enough to devour the case material, but we hoped he might have some initial insights. He did.
Lou shifted the toothpick to a corner of his mouth, and his eyes twinkled with the excitement of a good bird dog on point. He said,'I don't think it was the Ramseys.'
He never budged from that position."
From there it would just be a matter of Smit's marshalling factoids to confirm his initial bias. And I think he said that he thought Patsy was a loving mother and wouldn't have committed a crime like that.
Since: Mar 08
Location hidden
#4 Feb 22, 2014
Georgina, I'd recommend that you read _JonBenet_ by Steve Thomas. Thomas both respects and disagrees with Lou Smit so it's not a bad introduction to Smit's thinking.
#5 Feb 22, 2014
yeah, smit asked John "did you do it?" and John said "no" and smit said "swear to God?" and there's your uncle Bob! What an interrogation! Every police dept. can learn from Smit's 'expertise' LOL swear to God and you're home free;)
Since: Mar 08
Location hidden
#7 Mar 10, 2014
Google "standing in her shoes" "Todd Hartman" Read the version that pops up associated with Rocky Mountain News. It has Smit's arguments and rebuttals to them.
Brisbane, Australia
#8 Apr 4, 2016
Hi Georgina there is a documentary by Lou smit that really opened my eyes about the intruder theory even more , he shows in video evidence and his reasoning behind his thoughts on why it was an intruder responsible and not the ramseys
#12 Apr 4, 2016
Thanks for the link!
United States
#13 Apr 4, 2016
#14 Apr 5, 2016
Kirk Mitchell wrote in the Denver post:
"A thorough investigation did not uncover allegations of past abuse. An autopsy determined that there was no evidence of long-term sexual abuse, Smit said.
There was not one instance of physical or sexual abuse, he said.You just dont turn into something overnight. Usually you have some inkling. John would call his kids when he was on the road. His ex-wife said he was a good father.""
...the evidence on her body indicates JonBenét was tortured by a sexual sadist while she was struggling and still alive. There was a mark on her finger indicating she was struggling with the binding while she was still alive.
It must have been terrifying. You dont get a mark like that if it was staging after death, Smit said.All her injuries were while she was alive.
The last injury JonBenét received was the blow to her head, he said. A baseball bat was found. Ramseys said it wasnt their bat.
That was a very heavy blow, Smit said.
That contradicted the staging theory.
Smit said there was a recent shoe print left in the dust of the room with a concrete floor where JonBenét was found that hasnt been matched to anyone else.
Smit said he believes the killer or killers entered the Ramsey home, wrote the ransom note with the intention of taking JonBenét out of the house and when efforts to get the girl out of the house failed, abandoned the plan and fled the home.
He is definitely a stone cold psychotic killer, he said.
#15 Apr 5, 2016
Thanks for proving what a fool he was. And that you are, for going along with him!
I forget who it was (sorry, whoever you are), but someone here recently said that you can't have it both ways: you couldn't believe Smit had been a great investigator previously and think he was a fool on this case. That's not an exact quote, but to that effect. Hey, I'm cool with that idea! If his conduct on this case was typical, Clouseau would be offended!
#16 Apr 6, 2016
"Blue Lou"
Just read Lou Smit's blue line theory of a stun gun. A Blue line was visible on the nape of the victim's neck.
Since: Dec 14
Location hidden
#17 Apr 6, 2016
It was her blood vein.
Since: May 13
Location hidden
#18 Apr 6, 2016
From 'The Daily Camera'(May 2, 2001):
Air Taser representative Stephen Tuttle said he was contacted by an investigator early on in the case and provided Smit with the same model to conduct his experiments.
"I am bewildered. I don't know what to think about the theory," Tuttle said. "It defies the logic of what the weapon does."
Tuttle conceded that two marks are close to the width of the contacts of an Air Taser, but said that's where the similarities end.
"We have never seen those types of marks when you touch somebody with a stun gun," he said. "We are talking hundreds of people that have been touched with these devices. I can't replicate those marks."
Tuttle said it is uncommon for the stun gun to leave only two marks on the skin. The body moves away from the stun gun, causing multiple, erratic marks.
"How you can keep this thing perfectly still, not once, but twice on a squirming child? It doesn't make any sense," he said. "I hope that doesn't throw water on somebody's investigation."
He also said the Air Taser does not render people unconscious.
Nebraska Dr. Robert Stratbucker, who has conducted several experiments on stun guns and is considered a courtroom expert, said he takes "considerable issue" with Smit's stun gun theory.
***Stratbucker said it is "pure nonsense" that the stun gun would leave a blue mark in between red marks on the skin as Smit claimed.***
***"I have not seen ever, ever any blue marks, and I don't know what the cause of any blue mark could be," he said.***
United States
#22 Apr 7, 2016
Blue marks vs red marks
United States
#23 Apr 7, 2016
1. Do the marks vary in color with pigmentation?
2. Does the redness of the marks deepen over time (i.e. bluish)
3. Do the marks turn blue postmortem?
4. Have stun gun marks been evaluated on subjects that are deceased or during the stages of rigor mortis?
#blue #red
Since: Dec 14
Location hidden
#24 Apr 7, 2016
MarkBeckner[S] 20 points 2 days ago
Stun gun - no. The coroner and others who looked at the abrasion did not believe it came from a stun gun. The distance between the two marks did not match the probes of any stun gun we found. Stun guns are loud and hurt like crazy - which would have probably elicited some screaming. That probably would have woke someone up.
DA involvement in this case was inappropriate. They interfered in the investigation by being roadblocks to getting things done. They did not want to do a grand jury until forced too. We never allowed the DA to get that involved in a case again. Today, the new DA is great to work with and the police and DA's office work as a team.
from Mark Beckner's AMA on Reddit
Since: Dec 14
Location hidden
#26 Apr 7, 2016
Additionally, Lou Smit claimed on the show that the blue vein showing between the marks on JonBenét was a product of the blue arc produced by the stun gun when discharged. Apparently Mr. Smit failed his high school electronics class, or he would have known that the color of an electrical arc has nothing to do with the burn you get from it. The arc from an Air Taser stun gun could no more leave a blue line than a lightening bolt could turn a person blue if they were struck by it. Welders who expose their skin to the intense blue arc produced by arc welding get a typical red sunburn, they don't turn into blue smurfs--nor would their finger turn blue if they were stupid enough to touch the arc.(And where are the blue lines on your pig tests, Lou? Didn't the fact that they weren't reproduced on the pig tell you anything?) UPDATE 7/18/03 - On the MSNBC Dan Abrams Show last night, Michael Kane (the special prosecutor brought in to handle the Ramsey case) commented for the first time in public about the stun gun myth: KANE: The thing about the stun gun that everybody keeps coming back to. There was one person who was qualified who actually looked at that little girls body on the autopsy table and that was Dr. Meyer, whos a forensic pathologist. He looked at those very marks and said that they were abrasions. It is a quantum leap-you can take a stun gun and put it up against somebodys body...and its going to leave a burn. It dosen't leave an abrasion. So all these other opinions that have come out that said that this was a stun gun, there is absolutely no way they would ever get into evidence because there is no evidence that these were burns. ABRAMS: But,... there were other experts like Mr. Doberson and others and Lou Smit who have said they absolutely believe that there was a stun gun used. KANE: But theyre basing that based on photographs of marks on her body. When the uncontradicted evidence of Dr. Meyer is that these were not burns.
United States
#27 Apr 7, 2016
Read here about Topix's rules on posting Tiny URLs:
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#28 Apr 7, 2016
Thank you again for your concern. You might want to note the word PREFER- like (one thing or person) better than another or others; tend to choose.
( no where is it against any rule)
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|Publication number
|Publication type
|Publication date
|May 6, 1947
|Filing date
|Jul 9, 1941
|Priority date
|Jul 9, 1941
|Publication number
|Adams Roger
|Original Assignee
|Adams Roger
|Export Citation
|BiBTeX, EndNote, RefMan
|Patent Citations (1), Referenced by (15), Classifications (4)
|External Links: USPTO, USPTO Assignment, Espacenet
Patented May 6, 1947 No. Drawing; Application. July 9, 1941,
Serial N 0. 401,656
The present application is directed to pharmacological compounds characterized by marihuana activity and the process of preparing the same, and-is. a continuation-in-part of my co-pending application Serial No. 358,306, filed on September 5 'I'hesubject. matter of the present invention may: be illustratedbythe following basic reaction formulas.
= RMg halide CH3 \L .7 ;oo 00 I heoooztm- A oooctnr (.ILB)
27 Claims. (01. 260- 333) ClHo c0 Q00 caHs A OOOGaHs coo-cine In Formula I-A above R1 represents hydrogen. In the other formulas (I B to ID) R1 repre sents a lower alkyl group which as shown in Formula I may be attached to either of the 3, 4, 5or 6 positions.
Formula II above represents a 1,3-dihydroxy- 5-alkyl benzene of which the 5-methyl-(orcinol) and S-n-amyl-(olivetol) are typical. examples. Other examples where R2" represents the following alkyl groups are the methyl, ethyl, propyl; bufiyl, n-amyl', iso-amyl, hexyl, heptyl, 4-methyl-hexyl, 3-ethyl-amy1, octyl', nonyl and decyl derivatives. These compounds may be prepared by known processes (J. A. 0. 3., 61, 232); the preparation of the 1,3-dihydroxy-S-n-octylbenzene described in my co-pending pulegone condensation application, Serial No. 401,655, being illustrative.
In the preparation of the'compounds of the present invention a cycloheXan0ne-2-carboxylate I is first condensed with a 1,3-dihydroxy-5-alkyl benzene II to form a dibenzopyrone III. The benzopyrone is then reacted with a Grignard reagent'to form the desired dibenzopyran IV. The following examples will serve to illustrate the present invention.
Example I 1-hydroxy-3-n-amyl-6,6,9 trimethyl 7,8 9,10- tetrahydro-S-dibenzopyran.
A- solution of about 2% grams of 1,3-dihydroxyfi-mamylbenzene- (olivetol), 24' grams of ethyl 5- methyl-cyclohexanone 2 carboxyl'atefi and" 16 grams of phosphorus oxychloride in 1800. c.'of dry benzene is first refluxed for about seven hours. After' completion of the refluxing} the reaction mixture is first Washed with dilute aqueous sodium bicarbonate and is thenwashedrwith water. The benzene layer is then separated in theusual manner, the benzene evaporatedand the residue .(1- hyd roxy 3-n-amyl-9 m'eth'yl 'Z,8, 9,l0"-"tetrahy'- dro fi-dibenzopyrone) after purification byr'e crystallization from ethyl acetate, is obtained'a's' white needles with a melting. point of 180-181 C. If desired, the crude residue after crystallization from methanol may be converted to the pyran as described below.
A suspension of about 9 grams of I-hydroxy- 3 3 n amyl -9- methyl -7,8,9,ltetrahydro-fi-dibenzopyrone in 140 c. c. of solvent made up of about 3 parts of dry benzene and 1 part of dry di-n-butyl ether is next mixed with a solution Grignard reagent made up from about 9 grams of magnesium and 22.5 cc. of methyl iodide in '75 c. c. of dry ether and the total mixture then refluxed for about eight hours. After refluxing the reactipirmixtpre is poured'onto"iced ammo accordance with the general process of Example I by refluxing for four hours about 6 grams of ethyl 4-methyl-cyclohexanone-2-carboxylate and 1,3-dihydroxy-5-n-amy1-benzene in about 55 cc. of dry benzene containing 4.8 grams of phosphorus oxychloride. After treating with excess aqueous sodium bicarbonate, cooling, washing with water and benzene and crystallization from methanolthepyrone prcdu ct'is'obtained'as White nium chloride sclution the organiclayer sep 1o crystals with an ielting pointof-169 1695 C.
arated, the aqueous layer extracted once with benzene and the combined benzene solutions? The desired pyran derivative may be prepared by reacting the pyrone intermediate with the washed successively with water dilute aqueous ,proper al1ylfirignard reagent in accordance with sodium bicarbonate and water.
residue dissolved or taken up in ab9ut 1 50 c. c.
is then boiled on a hot: plate for about thirty minutes While maintaining the volume substantially constant by addition of more solvent as necessary. 'Attergseparation of thereaction solution, e. g;; {1y decantation, from: a smallaamount of insolubleimateirial, the solvent iseyaporated in the usual manner and'theresidua' l-hydroxy- 3-n-amyl-6, ,9- trimethyl 7,8,9,10-. tetrahydro-6- dibenzopyran distilled. This product is obtained asaaiviscous.oil,..B.., R. 71751 180. (1. (0,0 2 mrn ljath1te'mpeiaEIreJQ5 -2001QJJLZZQ QLSQBZ; "o tandingjitisolidifle andiln m cg ur i .by rc'ryst'allizatioiijfrom glacial'acetica d;
white crystals with" a melting point '12f. 7.3.".. C. p
l l zcmpl ll =hydroxy+3'-n-;-amyl-fifiediethylelk methyl-7;8,- 9,10 tetrahydro fi-dibenzopyram; r. *1;- .IBy'followin 'thetgeneral process ofExamD I except for .the-us eoi an'ethyl ,Grignard reagent .(e; g; ethyl magnesium bromide) the'cfiediethyl derivative may be-xobtained-having: a;-;B. 1?; of about 1855495? C. bath"200-2-10f;C.;).
-l3yfollowingthe general proeessot Example;
xc p 1 use i l. .G i ne rr i lei-g, npropyl magnesium bromide) the 6, 6di;n propyl derivative may be obtained-as a redresin having a 13.; P, of about -200f.l" C.; (2 -mm.,f-bath 1-hydroxy-3-n-amyla'7;8;9;10-tetrahydro-G-dibenzopyrone. Thispyrone intermediatemay-be'prepared in accordance with the general process of Example I by condensing ethyl cyclohexa'none z carboxylate W'ith"1,3 dihydroxy 5 n' arnylbenzene. Upon purification itifor'ms white crystals with a melting point-of'183183.5 C." f
JThe desired pyran derivative maybeprepared by' reacting the'tpy'rone intermediate with "the proper alkyl' Grignard reagent in accordance with thefabove examples.- By using a'methyl Grignard reagent in accordancewith: Example I the I-hydroxy'-'3-n=am'yl-6; 6-'dimethyl-.-'7,8, 9, IO-tetrahy drd-.6-'dib enzopyran is' obtained 'as' --a viscous 'oil With' a B;'P."0f"l75180 C;"(0.02 mm; bath 195-200C.); 1. 1 i
1 1 Eimmple V lghydroxy-3 n amyl=8 =methyl 7,8,9,l0tetrahy dro-G-dibenzopyron."' J j Thi r ro e n m d ate,m ybeprepared in of petroleum ether (B. P. (so-100 0.) 2x51 5195 drops of 48 per cent aqueous hydrobromic acidis next added to the petroleum ether solutiorrwhieh;
Theorganic so the above examples. vent (benzene, etc.) is then evaporated andthe 5 -5 l -hydroxy -K n-heptyl-9-methyl-'7,8,9,l0-tetra- Example VI tibd'ihe'itstitanium-172 173 c.-
The desired pyran may be prepared by -reactil the I pyrone "intermediate with the proper ialkyl Gi'lgh ard feag1t'-'ih--accordance ivith'thel'a "v examples. By using the methyl Grigfirdiagent in accordance with Example I the .1-hydroxy-3-n-heptyl-6,6,9-trimethyl -7,8,9,l0- tetrahydro-G-dibenzopyran isobtained with a .BQHP. of about 225 -22s-c. (c.05 min);
EwampYET/H. M 1-hydr0xy-3-n-hexyl-6,6,9-alkyl-7,8,9,IO-tetra hydro-G-dibenzopyran.
The pyrone intermediate. for these products may beprepared by condensing 1*,35dihydroxyhexanone-2-carb'oxy1ate in,raccordance with the above examples. By using ethyl 5emethyl-cycloheXanone-2-carboxylate a pyrone product is obtained with a melting point of about 173-174 C.
The pyran products may also be prepared in accordance with the above examples by reacting the pyrone with the proper alkyl Grignard reagent. By using the methyl Grignard reagent and the:Q-methyI-pyronepmduct a l-hydroxy- 3-n-hexyl-6,6;9etrimethyl 7,8,9,10-tetrahydro-6- dibenzopyran is obtained with a B. P. of about 190-192 C. (1 mm). This product is of particular interest as it has been found to be over er en -me e a ti t eme? c on n m l e fiva ve f xam lly liefiin-h x W) m le' lh s r e lby: lowin formula: v H I.
Eacaznp le VIII I 1-hydroXy-3-n-amyl 10-methy1-7,8,9,10-tetrahydro-G-dibenzopyrone.
A mixture'of about2 grams of ethyl G-methylcyclohexanone-2-carboxylate; 2 grams of 1,3-dihydroxy-5-n-amyl benzene; 1.75 rams of phosphorus oxychloride; 5 cc. of benzene and 15 cc.
.5. of toluene was refluxedfor about 12 hours. -'It was then" poured into excess saturated aqueous sodium carbonate solution and boiled until the solvent was removed. On cooling, the product was filtered and washed with benzene. White crystals purified from. a mixture of methanol and isopropanol :have a melting point of about 1944194,.5" C. 1
The l-hydroxy 3 n-amyl 6,6,,10 trimethyl- 7,8,9,10-tetrahydro-6-dibenzopyran formed from the above pyrone in accordance with processes outlined above has a B. P. of about l8l-185 C. at 0.5-1.0 mm. (bath 214-218 0.).
Additional examples prepared in accordance with the general processes outlined above are the 1- hydroxy-3-n-propyl 6,6,9-trimethy1- 7,8,9,10- tetra-hydro-fi-dibenzopyran' (B. P. 185 0., 2 mm.) 1-hydroXy-3 n butyl 6,6,9 trimethyl- 7,8,9,10-tetrahyclro-6-dibenzopyran (B. P. 178- 180 C., 1 mm); 1-hydroxy-3-n-octyl-6,6,9-trimethyl '7,8,9,l0 tetrahydro-G-dibenzopyran (B. E.;, 2l5.220,C., 0.01 mm), etc. Other pyran products, coming within the scope of the. present invention maybe prepared by condensing the proper, alkylated-cyclohexanone 2 carboxylate withthe proper 1,3dihydroXy--alkylated benzene and reacting the pyrone product obtained with the proper alkyl-magnesium-halide in accordance with the above exam les. The compound of Example 1 has the same .empirical formula as the compound given the same name in my co-pending application, Serial Number 440,971. The difference therefrom is that, because it is synthetically derivedfrom materials other than charas, it is definitely free of even chemical traces of nonacosane and certain terpenes and other'contaminants' found in products derived from hemp. It also may difier with respect to the position of the labile bonds in the all-carbon rings.
The products of the present invention form at the 1-position themonoacyl and monoalkyl ether derive,tives. Upon reduction with one mole equivalent of-hydrogen the double bond in the lefthand ring is eliminated and the correspondinghegtahydro analogs are produced. These hexahydro products differ from the hexahydrocannabinolsynthesized from cannabidiol by isomerizat ionhiollowed, by reduction, in that they are optically inactive. "The pyran products of the present invention differ from the pyran products prepared from cannabidiol in the position of the double bond in the lefthand ringand from the pulegone. condensation pyrans described in my copending application Serial No. 401,655 in that they are also optically inactive. The tetrahydro cannabinols prepared from cannabidiol by acidic isomerizing agents are described in my (toing" application Serial No. 352,931. Using very dilute 'ethanolic hydrochloric acid as the isomeriziri'g agent a low rotating tetrahydrocannabinol an-130:9 is produced, while using isomerizing agents such as p-toluene-sulfonie acid in benzeneor a drop of sulfuric acid (100%) in cycylohexane .a high rotating tetrahydrocannabinol d"D-265:5 is produced. These products while optically active diifer from the pulegone condensatiorr pyrans in the position of the double bond on the-lefth-and ring.
The lower alkyl ethers (e. g., methyl, ethyl, etc.) and lower acyl derivatives -(e. g., acetate, propion-ate, etc.) may be prepared in accordance with standard practices such as the processes described in my co-pending application Serial No, 352,931. :The h'ekahydro products may also be preparedby reducing the tetrahydre products in hydro Formula A corresponds to Formula B as illustrated below: 1
It will also be understood where R1 islan alkyl group, that the alkyl group replaces one of the Hatoms shown ,inFormula B.
The products of tho present invention have utility in the therapeutic field as, for example, in the treatment of dope addicts and alcoholics. A specific use is to eliminate or ameliorate the withdrawal symptoms experienced in the treatment of opiate derivative addictions.
It will be obvious to those skilled in the art that the present invention is not limited to the illustrative examples described above. All modific.a-' tions of the present inventionare intended to be covered by the claims annexed hereto.
l. The process of preparing a tetrahydrodibe'm zopyran which includes the following steps: (a) condensing an R1-cyclohexanone-2-carboxylate with a 1,3-dihydroxy 5-RzCHz-benzene and (b) treating the pyrone reaction product formed by step (a) with an R-Grignard reagent toform the corresponding tetrahydro-G-dibenzopyran, where R1 represents a member selected from the group consisting of hydrogen and lower alkyl groups, R2 represents a member selected from the group consisting of hydrogen and alkyl groups having 1-10 carbon atoms and R represents a lower alkyl group.
2. The process of preparing a tetrahydrodibenzopyran which includes the following steps; (a) condensing a lower alkyl-cyclohexanone '2 carboxylate with a 1,3-dibydroxy 5-R2CH2-benacne and (b) treating the pyrone reaction prodnot formed by step (a) with a lower alkyl-magnesium halide to form the corresponding tetrahydro-G-dibenzopyr-an, where R2 represents a 'member selected from the group consisting of hydrogen and alkyl groups having 'l-10 carbon atoms.
3. The process of preparing a tetrahydrodibenzopyran which includes the following essential steps: (a) condensing a lower alkyl-cyclohexanone-2-carboxylate with a 1,3-dihydroXy-5- amylbenzene and (b) treating the pyrone reaction product formed by step (a) with a lower alkyl magnesium halide to form the: corresponding tetrahydro-6-dibenzopyran.
4. The process of preparing a tetrahydrodibenzopyran which includes the following essential steps: (a) condensing a lower alkyl-cyclohexanone-2-carboxylate with a 1,3-dihydroxY-5- hexylbenzene and (b) treating the pyrone reaction product formed by step (a) with a lower alkyl magnesium halide to form'the corresponding tetrahydro-6-dibenzopyran.
5.. The process of preparing a tetrahydrodibenzopyran which includes the following essential steps: (a) condensing a lower alkyl-cyclohe'xanone-Z-carboxylate with a l,3-dihydroxy-5- alkyl magnesium halide to forrnl the correspond+j ing tetrahydro fi-dibenzopyrari. v
6..The process of preparing a". tetrahydrodibenzopyran which includes the following essentiahsteps: (a) condensing a 5-methyl-cyclohex-' anone-Z-carboxylate with 1,3-dihydroxy-5-n"- h'exylbenzene, and (b) treating the reaction product of step (a) with methyl magnesium halide to form 1-hydroxy-3-n-hexyl-6,6,9-trimethyl-'7,8,9, l-tetrahydro-6-dibenzopyran.
'7. The process of preparing a tetrahydrodibenzopyran which includes the following essential steps: (a) condensing a -methyl-cyclohexanone-Z-carboxylate with 1,3-dihydroxy-5-nhe'ptylbenz'ene, and (17) treating'the reaction product of step (a) 'with methyl magnesium halide to form l-hydroxy-3- n-heptyl-6,6,9 -trimethyl-7,8,9,lfl-tetrahydro-fi-dibenzopyran.
8, In the preparation of a tetrahydro-dibenzopyran, the process which includes the following steps: (a) condensing a'cycIoheXanOne Z-carboxylate with a' 1,3-dihydroxy 5-alkylbenzene in the presence of phosphorus oxychloride to form the corresponding dibenzopyrone intermediate, andlb) treating the pyrone intermediate with a lower 'alkyl Grignard reagent to form the corresponding dibenzopyran. s
9. A tetrahydro-dibenzopyran product represented by the following formula:
where R1 represents a member selected from the group. consisting of hydrogen and lower alkyl groups, R2 represents a member selected from the group consisting of hydrogen and ,alkyl groups having 1- 10 carbon atoms, R represents lower alkyl groups and Y is selected from the group consisting of hydrogen and lower alkyl and acyl groups; said product being substantially free of cannabidiol and of toxic impurities, and optically in ive- .7 A A 10. A productrepresentedby the formula of; claim 9 in which R2 is a butyl group. 11. A tetrahydro-dibenzopyran product represented by the following formula: y
where R1 represents a member selected from the group consisting of hydrogen and lower alkyl groups, R represents lowe'r'alkyl groups and Y is selected from the group consisting 'of hydrogen and lower alkyl and acyl groups.
-12; A product represented by'the; formula" of claim 9'in which R2 is 'a hexyl group;
13. A product represented by the formula ofc1aim9 in which R1 is a'lower alkyl 8130111351: ia-a n-butyl group and Yxis hydrogen. v 14: A- product represented by the formula.- Jo! claim 11 in which R1 is a lower alkyl group, the C5H11 is a n-amyl group, and Y is hydrogen; 153A product represented by the formula-o1 claim 9 in which R1 is a lower alkyl grouprRa is an-hexyl group andYis hydrogen. 1' 16. A tetrahydro-dibenzopyran product repre sented by the following formula:
inwhich R represents lower alkylgroups. I w
191 Aproductrepresnted by the formula of claim 16 in which R2 is a hexyl group.
20, The product 1-hydroxy-3-n-amyl-6,6,9tri methyl-7,8,9,lQ-tetrahydro-G-dibenzopyran; said product being substantially free of cannabidlol and of'toxic impurities, and optically inactive.
21. The product, l-hydroxy-3-n-hexyl-6,6,9- trimethyl-7, 8, 9, 10-tetrahydro-6-dibenzopyran.
22. A product represented by the formula of claim 16 in which the Rs represent methyl groups and R2 a n-hexyl roup. v H 3. chemical intermediates useful in organic synthesis, tetrahydrodibenzopyrones havingall four extra hydrogens on the same all-carbonring remotefromjthe oxygen of thepyronering. .24. As chemical intermediates ,useful in organic synthesis, dibenzopyrone substituted in 1 position by a grouprselected from the ,class hydroxy, acyloxyvand alkoxy; substituted in 3 position by a groupLCI-IzRlin whichR is selected from the class allgyl having from onetoten carbon atoms; substituted once in the all-carbon ring remote from the. oxygen of the pyrone ring by methyl in a, position selected from' the 'class, 8, 9,10.
25; As a chemical intermediate useful in organic synthesis, 1-hydroxy-3-n-amyl-9 -inethyl- 7,8, l @t a r6-d b n pyrqn 26. Asa chemical intermediate useful, in gore n c syn i lrhy r -n-he y -9-methy 'Z,8,9,1 0-tetrahydro-fi dibenzopyrone. no-
27, {The process of preparing atetrahydrondle benzopyran which includes the following essenttal 9 steps: (a) condensing a B-methyI-cyglohexanone- Z-carboxylate with 1,3-dihydroxy-5-n-amylbenzene, and (b) treating the reaction product of step (a) with methyl magnesium halide to form 1-hydroxy-3-n-amyl 6,6,9 trimethyl 7,8,9,10- tetrahydro-B-dibenzopyran.
REFERENCE S CITED The following references are of record in the file of this patent:
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|U.S. Classification
|International Classification
|Cooperative Classification
|European Classification


text:
Go Green With Kason
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- //Home
- //News
- //The Walking Dead
LOS ANGELES — AMC has renewed zombie drama "The Walking Dead" for a third season, the network announced Tuesday.
Currently in its second season, the series has brought in impressive ratings in the coveted 18 to 49 demographic. This season's 90-minute premiere, which aired Oct. 16, drew 7.3 million total viewers — with 4.8 million in the 18 to 49 demo.
In addition to the ratings success, the renewal is more good news for the show considering how the recent exit of series creator and executive producer Frank Darabont called to question how the show would perform under the leadership of Glen Mazzara.
The series follows a group of survivors, led by police officer Rick Grimes, after a zombie apocalypse as they search for security.
The 13-episode second season will take a break over the holidays, with the remaining six episodes returning in February.
Shabazz Palaces "Dawn in Luxor" (Singles Going Steady) // Music
Randy Rogers and Wade Bowen "West Texas Rain" (audio) (premiere) // Music
Kaytranada "Lite Spots" (Singles Going Steady) // Music
Rachael Sage "I Don't Believe It" (video) (premiere) // Music
Supernatural: Season 11, Episode 22 - "We Happy Few"
// Channel Surfing
"The show serves up an Avengers-esque character round-up, but the plot is powerless.READ the article


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From Editorial License by Karen Kapsanis
Years ago, when I joined JPCL as the editorial assistant, I told myself that I...
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A CRACKDOWN on employers that set up offshore trusts for top earners has started to pay off, helping HM Revenue & Customs more than double its takings from investigations into big companies' payroll tax avoidance last year.
HMRC stepped up its attack on banks and other businesses that paid salaries and bonuses through trusts, ratcheting up an extra compliance bill for the 770 companies in the large business sector by 160% to £533m in the year to April 2013, the Financial Times reports.
Companies came under pressure to dismantle structures that put money into trust for employees and members of their families, after a string of legal defeats and a change in legislation in 2011, Accountancy Age's sister publication IFAonline.com reports.
These structures, known as employee benefit trusts, allow employees to postpone – or avoid completely – paying tax while potentially benefiting from loans or property bought with the cash.
Ray McCann, a partner at Pinsent Masons, an international law firm, said the sharp increase in revenue was a sign that the tax authority's 15-year-long effort to tackle the structures was now bearing fruit.
"HMRC has made a concerted effort to crack down on employee benefit trusts and this has finally started to pay off after a slow start."
HMRC said: "We will not allow the abuse of employee benefits trusts (EBT) for tax avoidance purposes. The government has made almost £1bn available to HMRC to police the tax rules and we have specialist inspectors making sure any past abuse of EBTs is effectively challenged and the tax paid."
Related reading
Government deliberates secondary adjustment to transfer pricing rules
HMRC launches a consultation document that looks to strengthen government efforts against transfer mispricing
HMRC stumped in ECB VAT surcharge battle
The England and Wales Cricket board has hit HMRC for six in its VAT battle with the government department
EC adopts country-by-country reporting
EC adopts rules on the reporting by multinational companies of tax-related information
Google's Paris HQ raided in tax avoidance probe
The search engine's tax affairs have come under further scrutiny following a dawn raid on its Paris offices


text:
|By Chris Pollach
Article Rating:
|March 31, 2014 02:16 PM EDT
** Hot News **
Integrated Foundation Classes (Update)
Service Pack #2 (SP02)
(for PowerBuilder "Classic", Appeon Web and Appeon Mobile)
Software Tool & Die Inc (STD) is very pleased to announce that they have just released an updated version of their Integrated Foundation Class library today for PowerBuilder "Classic", Appeon Web and Appeon Mobile!
The latest version contains the following updates and has been tested with Appeon 2013R2 build 0110.00 using the official MR (maintenance releases) of PowerBuilder "Classic". Testing inside of PB included Win32 (both p-code & m-code) deployments while testing inside of Appeon included Web (IE10/11 - 32 & 64bit) , latest Apple Tablet/Smart Phone and Android Tablet/Smart Phone deployments.
The FC's are *free* and can be downloaded (along with an updated sample Order Entry application) from the SourceForge website!
|New ToolBar menu pop-up language support.
Release 12.1.0 Changes ... March 31, 2014 GA - SP02
- Added new code to the visual OLE container's (vs_ole_master) "externalexception" event.
- Added new code to the visual OLE container's (vs_ole_master) "error" event.
Note: Items #1 & #2 bring the visual OLE container to be at par with its non-visual counter-part.
- Removed old Webform and WPF code from the abstract Window classes "wn_controller_master" and "wn_main_master".
- Corrected code in the base wn_master class that sets the Window titles on the PB application's tool bar RHMB
Note: Original code was broken during the creation of the "integrated" framework.
- Toolbar pop-up menu item text now translated properly into alternate languages
- Abstract window class wn_zoom_master controls enlarged to allow easier gesture control when running on Tablets and Smartphones.
- Error handling code improved on the DataWindow and DataStore base classes
- Removed unnecessary duplicate object class "wn_log_viewer" from the English, French and Spanish PB Libraries
- Added new messages to the base message DataWindow "dw_messages_e /f /s".
- Added new "Filter" option to the "Log viewer" class (wn_log_viewer_master".
- Unit tested all code changes with PB 12.1 build 6518, PB 12.5.1 build 4015 and Appeon 2013R2 ( Build 0110.00 - 64 bit)
- Web Tested on IE 10 & 11 and Mobile tested on iO/s iPad4 and Android based Nexus 10 devices.
- Application Controller changed to check the Application Object's class mappings (ie: Error, Message, SQLCA, etc)
Note: If these mappings do not point to the STD FC's objects, mapping errors will be logged and a message displayed.
- The Calendar base object "wn_calendar_master" now has new English, French and Spanish extensions!
- The "wn_calendar_master" was changed to allow either a String or Structure to pass the intial date.
- The "VGA" INI parameter and its associated code were removed from the FC's.
(this was only used for Pocket PowerBuilder which is now deprecated).
- Fixed a bug handling the "Debug_Mode=" INI file setting
- Changed the Appeon INI setting in the default INI file to use the "Logging" keyword.
- Added new code to the FC's Logging feature to also simultaneously write to the Appeon Log file if "Logging=Y" in the APPEON section of the INI file.
- A new "oe_std_fc" event added to the Message, Transaction, Error, SQL Stage, and SQL Description base classes.
- A new "of_get_HPos" method added to the DataWindow Control base class to allow DC's to get the amount the user has already scrolled the DW object inside the control.
- Added new "of_log" to the "ghost" appeonextfuncs object in the "STD_FC_Appeon.pbl" to match the updated Appeon WorkArounds.pbl
(Note: This is to ensure Appeon2013R2 compatibility).
- The PB.NET version of the framework was officially deprecated and is no longer supported!
Futures1) Tune the PB, Appeon Web and Appeon Mobile single source framework.
2) Add more PB, Web and Mobile features.
3) Integrate Open Source tools like Spell Checking, OCR, Imaging and more!
4) Add new GUI controls
5) Extend the IIS (Web Services) framework
Note: There will be another release of the FC's coming soon for Appeon 7.0 (multiple browser support) ... Please stay tuned to this blog for more news releases!
Regards ... Chris
CIO, CTO & Developer Resources
Read the original blog entry...
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Pigland Railroad, a favorite attraction of Oogie
The Pigland Railroad's restored coal-powered viewliner will take you on a grand squashed-circle tour facing away from the park. After stops in many lands, the viewliner will take you around the amazing Untamed Canyon and Primieval Trolley models, in which you can ride yawningly past stiff animals and monstrous robotic creatures from millions of bad dinosaur movies in the past.
Please don't try Princess Mode
© copyright 2011–2016
A Pants Aflame production


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For Mikey – 1978-2009One of the founders of Colt Monday (Both the website and the weekly Emerson "soiree"), Mike Morrison passed away in May 2009. He was the best friend anybody ever had. It might not be much, but this website is dedicated to his memory. We love you and we miss you, Mikey.
FOLLOW US ON TWITTER – @coltmonday
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Is this a feasible solution, or am I on the wrong path?


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- Anonym
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text:
Mashed Potatoes and Carrots
Total Time
Prep 10 mins
Cook 30 mins
Although found as a holiday recipe, this dish can be enjoyed anytime of the year. It was found in The Thanksgiving Cookbook, 1991.
Ingredients Nutrition
- 1 1⁄2 lbs russet potatoes, peeled, rinsed, cut into large chunks
- 3⁄4 lb carrot, trimmed, cut into 2-inch pieces
- 1 1⁄2 tablespoons unsalted butter, softened
- 1⁄4 cup heavy cream
- 1 teaspoon salt
- 1⁄4 teaspoon black pepper
- Put potatoes & carrots in a large saucepan, then cover with about 2 inches of lightly salted cold water.
- Bring to a boil, then reduce heat, cover & boil slowly for about 20 minutes, or until both vegetables are very tender. Drain thoroughly & reserve 3/4 cup of the cooking liquid.
- Mash vegetables, then add the butter & the reserved hot cooking liquid, beating until the mixture is fairly smooth.
- Add the cream, salt & pepper & beat until nearly smooth ~ Small lumps of carrot are not a problem!
- Reward over low heat, beating constantly, then serve. DO NOT COVER AFTER THEY ARE MASHED, OR THE VEGETABLES WILL BECOME MUSHY.
Most Helpful
Great veggie dish! I used lowfat milk instead of heavy cream and it worked just fine. The carrots tasted great with the potatoes; they didn't mash up quite as well so they were a little chunky but that was ok - tasted great - thanks for sharing the recipe!
I've been doing this for years except just using regular milk. Good way to get your children to eat carrots. Tried it with peas one time -- didn't work. Thanks for sharing.


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Voices from the Nest
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The Life of Marine...
Hardcover: $29.95
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