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Supplier: MSA - The Safety Company
Description: A temporary anchorage connector useful near sharp edges or in high heat.
- Type: Anchorage Connectors
Control and Instrumentation Cables - MXI-2/M2 Cable,Straight-Point to Right-Angle Daisy-Chain, 4 m -- 777164-04Supplier: National Instruments
Description: and the right-angle connector. Daisy-chain connectors are required in systems with several MXI-2 devices.
- Product Type: Multiconductor Cable
Supplier: Molex
Description: Compact Robot Connector Power Crimp Pin, Lead Free, Chain
- Applications: PCB Connectors
- Gender: Male / Plug
- Terminal Option: Crimp
Supplier: National Instruments
Description: You can use the SCXI-1351 one-slot cable extender to connect the extra 50-pin male breakout connector of an SCXI cable assembly to an SCXI-1181 breadboard module installed in an adjacent slot. The SCXI-1351 includes a second 50-pin male breakout connector to daisy-chain the signals to an additional
- Applications: PCB Connectors
- Connector Type: Other
- Gender: Female / Jack
Supplier: European Automation
Description: FIP tap-off or Daisy Chain Connector
Supplier: Prism Sound
Description: from the dScope's generator outputs). Many I/O Switchers can be cascaded together to make larger input or output switching matrices by connecting the second XLR connector to a daisy-chain of I/O Switchers. Alternatively, one of the I/O Switcher's buses can be used as an 8-into-1 input switcher
Supplier: Demag Cranes & Components
Description: E 11 and E 22 electric travel drives were specially developed for operation with the new DC-Pro chain hoist. This provides you with additional benefits of this state-of-the-art hoist unit. The travel drives can be adapted to the U 11/U 22 trolleys. The drive is simply connected to the DC-Pro chain
- Type: Electric Trolley
- Connection: Lug
- Load Capacity: 2426 lbs
Supplier: IHS Product Design
Description: ASSEMBLY OF CHAIN TO CONNECTOR, NO. 8 UNC
Supplier: RS Components, Ltd.
Description: Connector A:Logistics chain; Connector B:Logistics chain; Propagation Mode:Single Mode; Fibre Type:OS1; Length:3m; Sheath Colour:Yellow; Communication Channels:Duplex; Core Diameter:9/125m
- Cable Type: Duplex
- Fiber Mode: Single Mode
- Cable Diameter: 4921 inch
Supplier: R. S. Hughes Company, Inc.
Description: Plier - Chain Nose w/ergo handles (Length: 6). Plier - Chain Nose w/ergo handles
Supplier: Mueller Electric Company
Description: BNC Female Cap with retention Chain. Used to protect a female BNC connector when a cable is not installed.
- Cover or Base?: Cover
- Cover / Plug Shape or Application: Round
- Length: 0.5800 inch
- Connector Diameter: 0.5700 inch
Supplier: Smiths Connectors
Description: Set against the backdrop of this year's Elektra Awards in London, Smiths Connectors, a world-leading provider of high- performance interconnect solutions for demanding applications, announced today the launch of its new Transformer Connector Range. This innovative family of high-density
- Applications: Rectangular Connectors, Heavy Duty, Modular Connectors and RJ Connectors, Other
Supplier: Digi-Key Electronics
Description: MIL-E-QUAL CAP & CHAIN
Supplier: Digi-Key Electronics
Description: .062 CHAIN FORM TERMINAL 5006T
- Applications: Rectangular Connectors, Heavy Duty
- RoHS Compliant: Yes
- Terminal Option: Crimp
Supplier: Gefran
Description: . The command input is configurable and accepts 0-10V, 0/4-20mA signals, potentiometers, logic signals, including with PWM modes for cost effective solutions. The device can also be operated via Modbus RTU serial communication, with IN/OUT chain connections facilitated by plug-in RJ10 (telephone
- Controller Inputs: DC Voltage Input, Current Loop (Transmitter) Input, Resistive / Potentiometer Input, Serial / Digital Input
- Control Signal Output: Analog Voltage, Current Loop, Switch / Relay Output
- Control Technique: Limit / Set Point Control, PID Control
- Special Capabilities (if required): Temperature Controller
Supplier: Gefran
Description: is configurable and accepts 0-10V, 0/4-20mA signals, potentiometers, logic signals, including with PWM modes for cost effective solutions. The device can also be operated via Modbus RTU serial communication, with cascade chain connections facilitated by plug-in RJ10 (telephone) connectors, or with various types
- Controller Inputs: DC Voltage Input, Current Loop (Transmitter) Input, Serial / Digital Input
- Control Signal Output: Analog Voltage, Current Loop, Serial / Digital
- Control Technique: Limit / Set Point Control
- Special Capabilities (if required): Temperature Controller
Supplier: Pivot Point, Inc.
Description: ; to connect chain, cable assemblies, lanyards, pins and more. The possibilities are infinite! Quick Connector Easy On & Off No Tools Needed Secure Tangle Free Storage Reusable
Supplier: Schmersal Inc.
Description: • thermoplastic enclosure • Connector M12, 8-pole • Max. length of the sensor chain 200 m • Self-monitoring series-wiring of 31 sensors • 3 LEDs to show operating conditions • Sensor tech0logy permits an offset between actuator and interlock of ± 5 mm vertically
- Interlock Switch Style: Keyed or Tongue Style Interlock Switch
- Number of Normally Open Contacts: 0.0
- Number of Normally Closed Contacts: 0.0
- Number of Changeover Contacts: 0.0
Supplier: B+B SmartWorx
Description: wavelengths Module performs multiplexing with no external power requirement Requires two slots in a compatible chassis Perfect for a variety of applications Daisy chain 2 modules together for 8 CWDM channels + one 1310nm over duplex fiber Designed with industry standard LC fiber connectors Modular
- Multiplexer Type: Coarse Wavelength Division Multiplexer (CWDM)
- Connector Type: LC
- CWDM Wavelength Range: 1310 nm
- LED Indicators: Yes
Supplier: HUBER+SUHNER AG
Description: Properties • Strain relieved with Aramide yarn • For direct connector assembly • Tube can be stripped minimal 30 mm in one piece • High chemical resistance against acids and alkalies • For high mechanical and thermal stability • Halogen free and non-corrosive fire
- Cable Type: Multifiber Cable
- Connector Type: None
- Cable Diameter: 0.5118 inch
- Cable Weight: 0.1979 lbs/ft
Supplier: ValueTronics International, Inc.
Description: , that provides 8 x 8 matrix topology, is included. The Keysight Agilent HP E1468A matrix switches both high and low on each crosspoint. Multiple modules can easily be interconnected with the Keysight Agilent HP E1468-80002 daisy-chain cable. The Keysight Agilent HP E1468-80002 daisy-chain cable
Supplier: Karl Kruse GmbH & Co. KG
Description: and produce solutions that reduce your cost. With innovativeness, a clear commitment to quality, and extensive technological expertise we work side by side with our customers along the entire value-creation chain,supporting them as an expert partner in development and solution creation.
- RoHS Compliant: Yes
Description: workmanship backed by a lifetime warranty. QUIETER OPERATION 80% reduction in sound pressure as compared to the classic Lodestar. IMPROVED LOAD SAFETY Clutch is located outside the load path which prevents slipping of the load in an overload condition when brake is not powered. IMPROVED CHAIN LIFE
- Power Source: Electric
- Load Capacity: 551 lbs
- Lift: 720 inch
- Maximum Lift Speed: 3.2 in/sec
Supplier: Acromag, Inc.
Description: The AXM-75 is a multi-function I/O module that adds A/D, D/A, and digital I/O signal processing functions to an FPGA board. These extension I/O modules plug directly onto many Acromag reconfigurable FPGA cards equipped with an AXM mezzanine connector. Analog Input There are sixteen differential
- Signal Converter Type: Analog-to-Digital Converter, Digital-to-Analog Converter
- Analog Input Channels: 16
- Differential Channels: Yes
- Resolution: 16 bits
Supplier: New Pig Corporation
Description: Round, closed-cell polyethylene foam flotation cylinders corral liquids and debris up to 6" above water line Skirting barrier hangs 12" below the water line to keep pollutants from creeping under; galvanized steel chain runs the length of the boom to add weight and rigidity Heavy-duty
Supplier: B+B SmartWorx
Description: connector. Each 3-pin connector has one Vcc pin, one ground and one signal pin. According to different applications, the users can choose suitable modules. The FR-2000 I/O module has an FRnet interface. The users can daisy chain several FR-2000 modules together. Via FRnet, the FR-2000 modules can
- Digital I/O Channels: 16
- Isolation: Isolated Digital Output
- Voltage Output: Yes
- Current Output: Yes
Supplier: Rego Electronics Inc.
Description: Rego is capable of integrating a chain of manufacturing starting from raw materials such as PVC colloidal particles to finished products, copper wire to cable assembly. We also provide custom product designs to meet the market demand and accomplish innovation. We currently include Computer Cables
- Product Category: Cable Assembly
- Number of Conductors: 40 to 120 #
- Cable Shielding: No Shielding
- North American (AWG): 30 AWG
Supplier: Infineon Technologies AG
Description: Infrared Remote Control Summary of Features: Transmitter Single layer flexible PCB 3V battery powered Touch wheel and two buttons Connector for programmer Receiver Form factor 16pin DIP IR Receiver module Docking Station USB to UART bridge Receiver board socket Transmitter board
- Category: Development Board
- Function: Break Out Board
Supplier: General Pipe Cleaners
Description: cables and operator against sudden torque build-ups. Sections come in two styles: all-purpose Flexichain, which has a chain center, and the stiffer Proflex, which has a spring center. A chain assures easier cable retrieving if the Flexichain spring should break. The inner spring in the Proflex gives
- Type: Electric
- Pipe Diameter (Nominal): 3 to 10 inch
- Flexible Cable Length: 2400 inch
- Features: Interchangeable Cutter, Stationary, Variable-Speed Cable Feed, Wheeled
Supplier: J.D. Neuhaus
Description: Travel limit switch Trolley drive with cross lever valve Energy chain trolley drive (vertical version) Junction box with air distribution Filter regulator (or maintenance unit) with main air emergency stop valve Energy chain crane drive (vertical version) Crane drive type EDL Hoist with trolley
- Crane Type: Bridge / Overhead Crane, Other
- Load Capacity: 3822 to 11240 lbs
- Horizontal Available Span: 413 to 984 inch
- Motorized Motion: Yes
Description: The Endevco® model 28959F/FV portable calibrator is designed to provide precision calibration for various types of accelerometers in the field. It is also perfect for test engineers and technicians needing on-site end-to-end calibration of their complete measurement chain. Model 28959F/FV
- Frequency Range: 10 to 10000 Hz
- Technology: Mechanical
- Application: Accelerometer Calibration
Supplier: Vision Research
Description: ports to daisy chain or tree branch to another JBox, significantly increasing the number of cameras in a configuration. The Miro C210, as well as other Phantom Miro cameras, can also connect to the Miro JBox, offering users additional configuration flexibility. Motion Analysis: The Miro C210J
- Camera Function: Video
- Monochrome / Color: Monochrome, Color
- Imaging Technology / Camera Type: CMOS, Digital
- Horizontal Resolution: 8 to 1024 lines
Supplier: Data Connect Enterprise, Inc.
Description: +Metal Casing ANS206-SM-M 4 10/100 ports + 2 100 Base-FX fiber-Single mode SC+Metal Casing The Data Connect ANS206-FT (ST Connector; Multi-mode) is a Unmanaged 4-Port Industrial 10/100 Base-T(X) with Dual 100 Base-FX Switch that secures data transmission by using fiber optic transmission to provide
- Network Equipment Type: Switch
- Area Network Type: LAN Capable
- Form Factor: Module
- Protocols / Networks: Ethernet, 10/100 Ethernet
Supplier: Scantek, Inc.
Description: The LRF-04 frequency filter sound level logger-limiter spectrally controls the entire sound chain in octave bands. The unit consists of an integrating-averaging frequency band (octaves) sensor and an attenuator of over 40 dB, which functions by analysing and calculating the power of the octaves
- Meter Style: Sound Level Meter
- Frequency Range: 20 to 20000 Hz
- Sound Level Range: 60 to 120 dB re 20µPa
- Control Panel: Digital
Supplier: Tripp Lite
Description: mounting tabs and up to 4 transformer plug outlets offers convenient protection of desktop computer equipment and accessories. Lifetime warranty with $100,000 connected equipment insurance (USA & Canada Only). Key Features 433 MHz key chain remote turns GREEN outlets on/off through walls
- Device Type: Plug-in Style
- Mounting: Wall / Panel / Backboard Mount, Plug-in Module
- Applications: Other
- Standards: UL 1449 Third Edition, UL, RoHS Compliant, Other
Find Suppliers by Category Top
Featured Products Top
Perfect Parts Corporation
Supply Chain Solutions
Perfect Parts offers the best supply chain solutions for its customers. We have many programs in place to optimize your purchasing power with over two-thousand manufacturers' lines. We offer drop shipments and expediting services so you get your products fast! Our excess inventory solutions offer you multiple options to help get you the asset recovery you need to ensure your return on investments. Our distribution and procurement processes give you access... (read more)
Browse AC-DC Adapters Datasheets for Perfect Parts Corporation
Karl Kruse GmbH & Co. KG
Supply Chain Solutions and Consulting Services
Together with our customers we develop pioneering solutions. We offer Supply Chain Solutions. up-to-date market information for our customers. One-stop-Shopping. Bill of materials cost reduction analysis. Buffer/Security Stock. Just-in-Time Deliveries. Worldwide marketing of excess inventories. KANBAN logistics. Consignments storage of excess inventories. Kitting. Last-time-buy and end-of-life analyses. Component Life-cycle Management. Further Value Added services we offer: Bar coding. Bill... (read more)
Browse Electrical Connectors Datasheets for Karl Kruse GmbH & Co. KG
Columbus McKinnon Corporation Hoists & Rigging Products
New Lodestar Electric Chain Hoist Features
Columbus McKinnon Corporation, a leading designer, manufacturer and marketer of material handling products, is proud to announce the addition of new features to the popular Lodestar Electric Chain Hoist. After receiving rave reviews and becoming highly recognized in environments around the world, Columbus McKinnon has made the legendary Lodestar electric chain hoist even better. By incorporating new features that provide steady lifts for an array of applications, the latest Lodestar... (read more)
Browse Hoists Datasheets for Columbus McKinnon Corporation Hoists & Rigging Products
Smiths Connectors
New Innovative Modular Connector Range
three contacts, and cross section cables can be covered from 25mm ² to 350 mm ². No specific tool is required, with consequent reduction of supply chain, maintenance and cabling costs. Made with a plastic insulator and aluminum frame the Transformer optimizes against ballast and enables weight savings contributing to reduced energy consumption. The materials used ensure compliance with fire and smoke standards, according to NF F 16-101 & NF F 16-102 and EN 45545. "Through... (read more)
Browse Modular Connectors and RJ Connectors Datasheets for Smiths Connectors
Protective Cover for MIL-DTL-38999 Receptacle
PEI-Genesis' dust covers, also known as protective caps, provide protection against live circuits and environmental contaminants when a connector is not in use. PEI-Genesis offers many styles of dust caps with a variety of chain connections available in different finishes. Caps for circular receptacles have internal threads and are used on MS3102, MS3101, and MS3100 receptacles. Caps for circular plugs have external threads for use on all plugs where a coupling nut is provided (MS3106... (read more)
Browse Circular Connectors Datasheets for PEI-Genesis
Interplex Industries, Inc.
Custom Medical Flex Assembly Solutions
at the lowest price, packaged and delivered to your specific requirements. Our Customer Flex Circuit and Connector Assemblies include supply chain management of all of your component needs. In addition we provide complete design services for custom interconnects and custom connectors. Additional services include stamping, plating, automation, component placement and soldering, conformal coating, testing, molding and insert molding. Assembly Capabilities: Flex... (read more)
Browse Electronic Manufacturing Services (EMS) Datasheets for Interplex Industries, Inc.
PIC Wire & Cable
Custom Aircraft Cable Assemblies
Assembly. Qualified Assembly Experts. Complete Lot Traceability. High Reliability in Harsh Environments. Improved Supply Chain Efficiency... (read more)
Browse Cable Assembly Services Datasheets for PIC Wire & Cable
Microwave Photonic Systems, Inc.
Optical Cable Distribution and Payout Reel
including OEM supplier, design consultant, and contract manufacturer. MPS has been providing proprietary technology solutions to military agencies, defense contractors, research facilities, and commercial customers since 1997. MPS is a privately held company whose strengths include Project Management, Operations Research, Design and Life Cycle Engineering, Quality Control, and Supply Chain Management. MPS maintains a professional and multi-disciplined engineering staff with the requisite skills... (read more)
Browse Fiber Optic Cables Datasheets for Microwave Photonic Systems, Inc.
Carlisle Interconnect Technologies
Automotive Industry Product Offering
Carlisle Interconnect Technologies recognizes the increased level of sophisticated electronics that are being incorporated into today 's passenger vehicles. We offer equally sophisticated interconnect, wire and cable and assembly solutions. Whether your need is associated to the vehicle 's RSE (Rear Seat Entertainment), GPS or antenna system, CarlisleIT is your supply chain partner. Our product offerings include RF connectors and assemblies as well as fiber... (read more)
Browse Cable Assemblies Datasheets for Carlisle Interconnect Technologies
Karl Kruse GmbH & Co. KG
Passive Parts - Capacitors
and produce solutions that reduce your cost. With innovativeness, a clear commitment to quality, and extensive technological expertise we work side by side with our customers along the entire value-creation chain,supporting them as an expert partner in development and solution creation. (read more)
Browse Capacitors Datasheets for Karl Kruse GmbH & Co. KG
Conduct Research Top
Flat Connectors for Conveyors
If you do not like technical jargon but still appreciate qualified information on further developments, please read on: We refer to chain conveyors for underground applications and in particular to the connector elements required by them. RUD has already taken a decisive step in their development
Chainflex Cables Available With Over-Molded Connectors
Igus Inc., the leading developer of Energy Chain cable carriers, Chainflex continuous-flex cables and iglide plastic bearings, now offers Chainflex cables with over-molded connectors. , the leading developer of Energy Chain cable carriers, Chainflex continuous-flex cables and iglide plastic
Throwing it All Away
and vertically into various niches through the process chain. Plastic bags replaced steel tanks for media and buffer storage, then morphed into mixing containers and bioreactors. Plastic tubing, valves and connectors encroached on stainless steel pipes and manifolds. Membrane filters appeared housed
An Innovative Cabling Concept Improves Reliability for Multi-Axis Stage Systems
shown in Figure 1, instead of a huge number of moving wires, there are 3 moving control modules, a tiny three wire shielded CAN-bus cable in a daisy chain configuration and two wires for power. In total, the complete system needs just 2 separate cables with diameters of 7 mm and 12 mm independent of how
More Information Top
Anchor Leg System Integrity - From Design Through Service Life
Experience has shown that these systems though having a lower initial cost have had issues with reliability due to the clump weight/weight chain connectors failing resulting in loss of station keeping performance as addressed in a later section of this paper.
Study on Manufacture Technology for Enhancing the Life of Mining Flat Type Chain Connector Units
• Study on Manufacture Technology for Enhancing the Life of Mining Flat Type Chain Connector Units p.153 .
Friction of an elastomer sliding on polymeric model surfaces
During sliding of a network on a grafted surface at a velocity V , tethered chains ( con- nectors with Z monomers of length a, grafted at an areal density Σ) are pulled out on paths imposed by the surround- ing obstacles like entanglement …
Collapse of a semiflexible polymer in poor solvent
In particular, we have performed simulations with a bead-rod model, where the chain connectors are rigid rods rather than stiff elastic spring.
Study on Enhancing the Strength and Life of Mining Flat Type Chain Connector Units Based on CAE
• Study on Enhancing the Strength and Life of Mining Flat Type Chain Connector Units Based on CAE p.722 .
A Historical Review on Integrity Issues of Permanent Mooring Systems
Mechanical chain connectors to the vessel hull shall be inspectable, and bushing's wear measured on a regular basis to ensure that the chains subject to OPB or in-plane bending (IPB) are operating within their design envelope.
Scrap tire ring as a low-cost post-tensioning material for masonry strengthening
The developed STR chain connector shown in Fig. 8 is a simple, efficient, and low cost connector.
Interim design status and operational report for remote handling fixtures: primary and secondary burners
Prediction of solution properties of flexible-chain polymers: a computer simulation undergraduate experiment
Chain connectors .


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subset: commoncrawl


text:
Tim in AZ
So the pluses. Lighter. Quieter. Let's the frame flex as designed. Now here's where things went negative. 1 out of the only 3 bolt holes lined up. No extra brackets or reinforcements. The fitment is absolutely terrible. Ended up drilling out all holes to make fit properly. Used a torch to mold skid plate to fit properly. Also added an extra bolt to top of skid where there is an actual threaded hole already. I expected a better product. They need to mold the product correctly for a better fit and finish.Read All Reviews
Jeffrey in MD
not only is this Chain Guide an HUGE upgrade to OEM in many Ways, But I noticed there's less Resistance in the entire drive system, the back wheel turns much MUCH Easier Which translates to More Power being put to the Ground!Read All Reviews
Nicholas in WA
I had to remove the metal bushing in one of the bolt holes to fit this on my LTR. I was not impressed. It also wears quickly. One dune trip of 5 days and it is half worn through.Read All Reviews
SAM in UT
I've had this on my bike for over 100 riding hours and besides riding damage it still looks like new!Read All Reviews
mike in OR
got this with the TM designs slider and guide. seems fineRead All Reviews
Matthew in NV
better than stock and wear like iron so far. have had for about three months now.Read All Reviews


text:
- Detail Images
When winter's cold breath tries to blow out your flame, keep calm and shine on with the superior warmth of the DC Star Shearling Full-Zip Hoodie.
- Fully lined with with Sherpa fleece for heavyweight winter warmth
- Made from a soft and comfortable cotton-poly blend you won't want to take off
- Custom DC trim throughout shows those around you how much of a 'details guy' you really are
Share your thoughts
Not to shabby
The looks awesome but I don't like how the description says "FULLY lined with Sherpa fleece" when it's not. Its only on the hood and inside, not on the arms, I live in Alaska and it gets pretty chilly up here. Good look tho!


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Ta Som
Compact and scenic
What we say:
Ta Som is a compact temple — laterite enclosure wall, reasonably well preserved gopuras and central shrine — all recently renovated. Of particular note is the much photographed eastern gopura covered in tree roots.
A satellite temple of Preah Khan, this is the third Jayavarman VII temple in a row along the north side of the Grand Circuit road, but this one's a bit larger, a bit more popular and does possess postcards, cold drinks and bamboo flutes as opposed to the previous two, which are devoid of any vendors.
Make sure you walk to the very back of the temple to look back at the tree-framed door.
It's all very scenic but increasingly popular with large tour groups, which makes us less inclined to stop here if you're touring the Grand Circuit as picturesque trees can be found elsewhere at sites like Ta Prohm and Preah Khan, while other small sites offer a greater chance of a people-free visit, including Banteay Prei and Prasat Prei on the Grand Circuit, or a quiet site like Ta Nei.Last updated: 31st January, 2015
Caroline swapped the drizzle of Old Blighty for the dazzling sunshine of Siem Reap and she spends most weekends cycling the temple-studded terrain that she can call her backyard.
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The above sights are all the sights in Angkor we list on Travelfish.org.


text:
Fifth-seeded Lakeland will play second-seeded Wayne Hills in the Passaic County boys volleyball tournament championship game on Saturday at Clifton High School at 5 p.m.
Lakeland (13-8) defeated fourth-seeded Passaic Tech and top-seeded Wayne Valley, the 2010 and 2011 PCT champions, in the semifinals to reach the final.
The Lancers have won six county crowns, more than any other school since the tournament began in 1997.Lakeland last took the title in back-to-back years in 2006 and 2007.
Wayne Hills (15-6), the second seed, will be looking for its second championship as the Patriots took the 2008 title.
Wayne Hills advanced to the final by defeating seventh-seeded Kennedy in the quarterfinals and sixth-seeded Clifton in the semifinals.
Lakeland features junior opposite L.J. Barthelemy, sophomore middle hitter Petko Ljusic, junior setter Andrew Rodgers and junior libero Jared Holm.
Wayne Hills has been bolstered by the return to the lineup of senior middle hitter Luciano Blumetti. Also sparking the Patriots should be senior outside hitter Jason Gold, junior defensive specialist Hunter Beck, junior setter Emir Sahmanovic and senior libero Rob Salviano.
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Darren Cooper is from Slidell, La., and is a graduate of Louisiana State University. He covers any North Jersey sport — including soccer, gymnastics, wrestling, swimming and softball — within walking distance of an ice cream parlor.
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Mark J. Czerwinski has been at The Record since 1985, covering everything from high school sports to the NHL. Mark also writes The Record's weekly hunting and fishing column.
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JJ Conrad joined The Record in January 2012 and graduated from Pace University in 2010 with a degree in Media and Communications. He's a 2006 graduate of Wallkill Valley High School in Sussex County, where he played baseball, football and basketball.
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Greg Mattura has been a sports writer for The Record since 1989 and has covered everything from Little League to the U.S. Open. A Fair Lawn native, Greg graduated from Hofstra University.
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Jim McConville has been covering high school sports in North Jersey since 1974 for the Ridgewood News. A graduate of Midland Park High School, he is also a member of the Executive Committee of the North Jersey Junior Football League.
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Ed Mills has been at the Record since November of 1988 covering high school sports. A graduate of Columbia High School in Maplewood and Utica College of Syracuse University in Utica, N.Y.
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Gregory Schutta joined The Record in 1987. He was part of the award-winning team that exposed the financial workings inside the NJSIAA. Greg covers boys soccer, wrestling and boys tennis.
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Paul Schwartz is a practicing attorney in workers' compensation in Ridgefield Park. Since 1971, he has been a part-time sports writer at the Record and now covers track and cross-country.
View all of his posts
Greg Tartaglia has covered North Jersey sports from football to bowling to volleyball for various local media since 2001. He grew up in Franklin Lakes and graduated from two BC's, Bergen Catholic and Boston College.
View all of his posts


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sleeper train (6 community guides)
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My account of a delightful budget break in Scotland featuring a journey on the Caledonian sleeper train and short stays in Inverness and Pitlochry... read more »
Air travel might be quicker, but taking the Trans-Siberian Railway from Moscow to Beijing is an experience that few could forget... read more »
Booking a cosy compartment on one of the many sleeper trains that run between St Petersburg and Moscow is a chance to relive the golden age of rail travel. And learn the rules of water polo...... read more »
Iran may seem like an unusual travel destination, but taking the Trans-Asia Express from Istanbul to Tehran gives a real sense of travelling to a different world... read more »
Sydney to Perth on the Indian Pacific is one of the world's great rail journeys – 3,000 miles taking in vast deserts, mountain ranges, tiny ghost towns and some the finest cities you'll ever see.... read more »
You don't have to ski to enjoy the snow. Forget the flight, pass over the pistes, cut your carbon footprint and take the train to the Dolomites this winter ... read more »


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After you enable Windows Azure Diagnostics with Web and/or Worker Role please make sure to use correct Windows Azure Storage account and key. After it, please run your web or worker role in compute emulator and then verify at Windows Azure Storage for any diagnostics details. This way you can assure the Azure diagnostics is working within the role and diagnostics data is logged at Windows Azure Storage.
Here are a few things you can verify:
1. Now after you deploy your application to Windows Azure and experience problems with Windows Azure Diagnostics, you can RDP to your Windows Azure machine to verify DiagnosticsAgent.exe is running.
2. While you are still in your Windows Azure VM please look at the following folder for <RoleHostProcessName>.log for any error with Windows Azure Diagnostics:
3. Windows Azure Diagnostics use Blob Storage and Table Storage so it is always good to check if Storage Emulator is working correctly or not. Please start your Azure Storage already before starting the debugging process using:
4. In your development machine please try editing your service configuration to target a real storage account for "Microsoft.WindowsAzure.Plugins.Diagnostics.ConnectionString" setting.
5. Please make sure the storage account is not set to "UseDevelopmentStorage=true".
6. Check the blobs in the wad-control-container blob container in the diagnostics storage account.
7. Check the logs in the WADDiagnosticInfrastructureLogsTable table in the diagnostics storage account and filter on DeploymentId GUID.
8. A common problem is not querying the diagnostics storage correctly, thus returning no results and assuming that diagnostics are not being captured.
9. If you have multiple instances and only a few of them aren't transferring diagnostics correctly, you can try to Reimage the VM from the Management Portal. This might fix the issue, but then you will lose the ability to determine root cause for why the problem was happening. This should be used as a last resort.
If you still see the problem please contact Windows Azure Support Team @ https://support.microsoft.com/oas/default.aspx?gprid=14928&st=1&wfxredirect=1&sd=gn
Suggest Tools to Access Azure Diagnostic data from Windows Azure Storage:
- Azure Storage Explorer @ http://azurestorageexplorer.codeplex.com/
Good one!!!
Thanks Karthikeyan!! I am glad you liked the post.


text:
Firewood stolen in KillingtonNovember 15,2012KILLINGTON Police are looking for information regarding stolen firewood missing from a Killington home.
Helen Mercer, 55, of Gilsum, N.H., told police an entire cord of firewood has gone missing. She told police her wood had been disappearing from her property since Oct. 14.
Anyone with information is encouraged to contact the Vermont State Police in Rutland at 773-9101. Information can also be submitted anonymously online at www.vtips.info or text CRIMES (274637) to Keyword: VTIPSMORE IN This Just In
The Rutland City Fire Department responded to an alarm Friday at the General Electric plant... Full Story
A driver ran a red light and crashed into another vehicle Friday afternoon at the entrance of... Full Story
WEST HARTFORD — A teenager was killed and another person was critically injured when... Full Story
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text:
The 5 Elements Hotel
Filling a midrange gap in the market
What we say:
Chinatown may be able to boast of many excellent budget options, but when it comes to decent midrange choices, the cupboard is somewhat barer. The 5 Elements is one of the few places that successfully bridges the gap between the low and high ends of the market. For your money, you get good sized, comfortable rooms, with mostly tasteful contemporary decor, modern attached bathrooms, tea- and coffee-making facilities and flat screen televisions. The highest floor rooms, not surprisingly, have the best views, and are as a result more pricey. Room rates include a basic breakfast and WiFi.
Make a reservation online now
Contact details:Lot 243 Jalan Sultan. T: (03) 2031 6888 F: (03) 2031 6811
Email them at: email@example.com
Visit website
What we were quoted
|Type of room
|Low season
|High season
|Standard - Double
|150 ringgit
|150 ringgit
|Upto 170 ringgit
|Superior - Double
|180 ringgit
|180 ringgit
|Upto 199 ringgit
|Deluxe- Double
|190 ringgit
|190 ringgit
|Upto 230 ringgit
Added to Travelfish on: 15th October, 2011
Last visited or updated on: 24th October, 2011
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The above hotels and guesthouses are the most popular places in Kuala Lumpur that people are reading about on Travelfish.org.
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The above are all within 200km of Kuala Lumpur.


text:
Former landfill employee charged with theft, fraud
The Salt Lake County District Attorney's Office filed 11 felony charges Friday against a West Valley City woman for allegedly stealing more than $25,000 while collecting entry fees at the Salt Lake Valley Landfill.
Christina Joy Patton, 26, faces one count of second-degree felony theft, another second-degree felony for allegedly being involved in a pattern of unlawful activity and nine third-degree felony charges alleging she forged receipts.
Second-degree felonies are punishable by up to 15 years in prison. A third-degree felony could carry a maximum 5-year term, said County District Attorney Sim Gill.
Efforts to reach Patton were unsuccessful on Friday.
The charges allege that when Patton worked in the "scale house" collecting fees for dumping refuse at the landfill, 6030 W. California Ave., she developed a scheme that defrauded the county of thousands of payments in a six-month period between April 20, 2012, and Oct. 27, 2012.
In a probable-cause statement, District Attorney's Office Investigator Michael Leary alleged that Patton often printed "duplicate tickets" when a customer paid at her window.
Patton then allegedly cut the words "Duplicate Ticket" off the duplicate receipts she kept. When a new customer came up who paid in cash, the charges allege, she would hand back an altered duplicate ticket and put the money in the till, but would not enter the transaction into the computer system.
The charges contend Patton kept track of how much money was not entered into the computer system and, at the end of the day, would "consult her notes of how much unaccounted for cash was in the till and remove it to her own pocket."
She did it frequently, the district attorney's office alleged.
"Evidence shows Patton to have printed and altered at least 2,200 duplicate receipts, government documents, and passed them on to customers," Leary wrote, noting that on two days alone June 2 and June 23, 2012 "Patton provided 185 altered duplicate receipts to customers entering the solid waste facility."
County Public Works Director Russ Wall, who oversees the waste facility, said complaints by other employees led to a probe of agency books by county auditors and attorneys.
"They could see there was something fishy," he added, noting that a "meticulous" yearlong investigation uncovered Patton's alleged scheme and led to reforms.
"Once the method of fraud was discovered people always try to find holes in your system we immediately took steps to safeguard our cash transactions," Wall said, citing a ban on printing duplicate receipts and installation of better tracking software.
"You're never 100 percent sure," he added, "but we're confident there's no continued illegal activity going on."


text:
Known to make relentless scathing comments on various celebrities without batting his eyelids, KRK has now taken a big-time panga with none other than Shah Rukh Khan.
Kamaal Khan with a friend during his house warming bash in Mumbai on July 29, 2012. (Pic: Viral Bhayani)
Celebrities across the globe are facing serious trouble owing to their accounts being hacked!
Actor Kamaal Rashid Khan is not too pleased, for Anna apparently went on to say that while the janta votes, it is in an inebriated state. Khan vent his anger on Twitter.
Interest Networkitimes


text: 8 minutes read June 6, 2014 Interview: On two important exhibitions devoted to African diasporas during the slave trades (Part I) Two important exhibitions devoted to African diasporas in the age of slave trades have just closed. The first, "Revealing the African Presence in Renaissance Europe," was organized by the Walters….. Read More 7 minutes read November 21, 2012 The end of "the colonial gaze"? The weekend after Hurricane Sandy hit NYC, AIAC's Sean Jacobs and I (we're academics in our day jobs) attended Encounters with the African Archive, a symposium at New York University. The symposium….. Read More


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Barley with Shiitakes and Spinach
Although barley isn't a commonly used grain, it's great for baby because of its mild flavor. In this recipe, barley provides a quick yet hearty base for vegetables, cheese, and rosemary, which can be served as a meatless main or side dish.
For baby:
For baby:
• Omit black pepper.
• Serve the barley mixture in a small bowl.
• Cut the mushrooms and spinach into bite-sized pieces, if needed.


text:
2006 BMW X3 • 100,000 miles
Tried to boost a 06x3 but no response at all, no click, no turn over
December 26, 2012.
December 26, 2012.
You are taking a large risk "boosting" that car. EWS alignment seems as likely a culprit as any, the BMW service provider in your region should be consulted as we can only speculate with the data provided.
Dr. Hagerty
Dec 29, 2012.
Dec 29, 2012.
I have a 1994 D21 PU, with 2.4, A/T. My problem began when I went to start the truck. Turned the key and had nothing -just the clicking of the relays, etc. Thought it was the battery ...
4 answers • 1994 Nissan Truck • 135,000 miles
I have a 97 Ford F150. went out to start my truck but got a sudden clicking noise but the truck wont start. We checked the cam sensor and the crack sensor. Still no luck so we checked ...
8 answers • 1997 Ford F-150 • 169,000 miles
My name is ray i have a 1993 infiniti g20 it has 76,550 miles on it just replace starter has new altenator oil changed regulary no check engine lights on its a great car.but for some ...
1 answer • 1993 Infiniti G20 • 76,550 miles
My car is making a clicking noise when I am at a stop, my car is in park, or my foot is off the gas. Sometimes it is quieter then others but it is a pretty fast like click click click. ...
1 answer • 2003 Hyundai Elantra


text:
um yeah well the short story is that i have an xbox that won't play games it will play cd's and dvds it just won't play games.
it tells me that my xbox needs a service but i can't give it to MS because it has been tampered with.
basically i have come in contact with a guy who says he can fix it by putting a chip in it and re entering the software then removing the chip.
as i don't want anyone touching the thing because that's how it got broken in the first place i want to fix it and mod chip it myself because i don't trust anyone anymore.
can someone give me information on how to fix it and where i can buy the modchip from so i can do it myself.
i am able to access a very good computer so if i need to use a top of the range computer then i can.
Stuffed Software
Started by hardcorecheck , Aug 04 2003 12:29 AM
2 replies to this topic
Posted 04 August 2003 - 12:29 AM
Posted 04 August 2003 - 12:44 AM
need more information...
Posted 04 August 2003 - 01:06 AM
what info is needed?
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text:
In conjunction with the 3rd PANIC conference in La Jolla, California, a 1-day NMR validation workshop was held that attracted approximately 80 interested participants. The agenda of the meeting is provided at this link (http://www.nmrvalidation.org/index.php/events/event-review) and registered participants can now download the presentations presented at the meeting. At the meeting it was decided to proceed with the idea of founding an organization dedicated to the development of validate NMR methods for use throughout all industry sectors.
Organizational Scope:
NMR spectroscopy provides a means to evaluate material with high compound and high material specificity. Information as to the chemical structure, stereochemistry, quantity, material composition, and material identity is encoded in the NMR spectrum. The high reproducibility of NMR spectroscopy from instrument to instrument and lab to lab makes NMR an excellent tool for material validation. Approaches to utilizing NMR as a material validation tool include using (1) targeted approaches, the identification and quantification of specific components, and (2) non-targeted approaches, the use of chemometric methods to evaluate the spectrum as a whole. Efforts to increase the number and the speed of validated NMR methods are underway. This promises to move NMR technology from R&D to a mainstream analytical tool for production leading to high quality product assessment.
Quantitative NMR spectroscopy (qNMR) provides the most universally applicable form of direct purity determination without the need for reference materials of analytes or the calculation of response factors, with the only requirement being the exhibition of suitable NMR spectral properties. Due to recent advances in the technical development of NMR instruments, such as acquisition electronics and probe design, detection limits of components in liquid mixtures have been improved into the lower ppm range (approx. 5–10 ppm amount of substance).
The development of validated procedures and qualified standards will give users the tools to routinely exploit qNMR and enable them to speed up analytical method development, with the added advantage of reducing the time and financial burden of multiple analytical testing.
Over the last few years a number of efforts have been made to include NMR in routine testing and analysis – especially in regulated fields such as those operating under GMP or GLP guidelines. Unfortunately it has been observed that approval authorities, standard method organizations, and auditors prefer to take analytical routes derived from classical chromatographic methods. Since NMR represents a direct comparison analysis method such decisions clearly fail to take advantage of the benefits that NMR can provide.
The PANIC validation group proposes to become a driving force in getting NMR methods validated, publicized, and supported by documentation and qualified standards. The organization will also provide a mechanism for repeatability/reproducibility assessment of NMR methods as well as the round-robin accreditation of NMR labs. We aim to proactively promote the technology and improve its acceptance by the analytical community across all industry sectors.
What we want:
It is expected that there will be an annual 1-day meeting in conjunction with future PANIC conferences. A website has been been created as an organizational repository. The website can be found here: http://www.nmrvalidation.org/index.php and details of future events and, eventually, contact information will be provided.
1H quantitative NMR (qNMR) has been utilized to assess the the small molecule and carbohydrate chemistry of a number of home-brewed and commercial alcoholic ciders. A quantitative chemistry distribution of the products of the various fermentations that occur in cider making. Malolactic fermentation as well as fermentation by saccharomyces and wild yeasts occur in the cider making process which traditionally occurred without the intentional addition of yeast by the manufacturer. The distribution of small molecules produced by the yeast and bacterial metabolomes at work in the process can yield information of the sensory perception of ciders produced in different ways. An investigation of the residual sugar chemistry of commercial ciders gives some indication of the process of sweetening commercial cider products with sugar additions after fermentation is complete. These typical commercial ciders are very different in chemistry distribution compared to very dry cider styles such as those found in the Basque region of Spain where fermentation is taken to the extreme resulting in complete conversion of sugars to alcohol but also glycerols to 1,3 propandiol. Finally it was decided to determine how much quantitative chemistry information could be obtained from benchtop NMR systems operating in the 60 MHz range. These benchtop NMR systems have a price and cost-of-ownership that would allow small laboratories of manufacturers to think about their use in QA and QC roles.
1H qNMR analysis of molecular components in hard cider – targeted and non-targeted quantitative chemical analysis
John Edwards of Process NMR Associates will be presenting 4 papers at the 2015 ACS Northeast Regional Meeting that will be held in Ithaca, NY, June 10-13, 2015.
ABSTRACT TITLE: 1H qNMR of Alcoholic Cider – Analysis of Small Molecule and Residual Sugar Chemistry (final paper number: 43)
SESSION: Food Chemistry
PRESENTATION FORMAT: Poster
DAY & TIME OF PRESENTATION: Wednesday, June, 10, 2015, 5:00 PM – 9:00 PM
ROOM & LOCATION: Emerson Suites – Campus Center
ABSTRACT TITLE: Nutritional Supplement and Diesel Fuel Application Development for Benchtop NMR Systems Operating at 42, 60, and 80 MHz – Equivalency with Supercon NMR (final paper number: 336)
SESSION: Analytical Chemistry
PRESENTATION FORMAT: Oral
DAY & TIME OF PRESENTATION: Friday, June, 12, 2015 from 9:45 AM – 10:05 AM
ROOM & LOCATION: 222 – Williams Hall
ABSTRACT TITLE: Survey of Low Field NMR Spectrometer Platforms for Successful Screening of Sexual Enhancement and Weight Loss Supplements for Adulteration with Drugs and Drug Analogs (final paper number: 386)
SESSION: Medicinal Chemistry
PRESENTATION FORMAT: Oral
DAY & TIME OF PRESENTATION: Friday, June, 12, 2015 from 2:20 PM – 2:40 PM
ROOM & LOCATION: 302 – Williams Hall
ABSTRACT TITLE: From Mash to Bottle: Chemistry of the Beer Brewing Process and NMR-based Quality Control (final paper number: 284)
SESSION: Food Chemistry
PRESENTATION FORMAT: Oral
DAY & TIME OF PRESENTATION: Thursday, June, 11, 2015 from 1:35 PM – 1:55 PM
ROOM & LOCATION: 202 – Williams Hall
1H NMR shows excellent promise to be utilized in the quality control and authentication of essential oils. In order to ascertain if benchtop NMR systems reveal adequate "1H spectral fingerprints" for this purpose we have run several hundred essential oils at 300 MHz (Varian Mercury-300 MVX by 1H, 13C, COSY, HETCOR, DEPT) as well as at 82.3 MHz (Picospin 80), 60 MHz (Aspect-60), and 42.5 MHz (Magritek Spinsolve). The results plainly show that the spectrometers all yield similar proton line-widths with the difference in field strength leading to different levels of spectral dispersion and resolution. Though each spectrum is different it can plainly be seen that they all contain the same information with varying degrees of overlap. Chemometric and database comparative methods are being developed to allow identification of various essential oils as well as screening and quantifying different levels of adulteration. The figures below show examples from 6 different essential oils showing spectra obtained from all 4 spectrometers and plotted in the normalized chemical shift scale (ppm) as well as the absolute frequency scale (Hz).
1H NMR is an excellent tool for monitoring the residual olefin content of polymers after hydrogenation reactions. The fact that the olefin fall in a unique region of the spectrum means that it is a straightforward measurement to quantify the %H present as olefin or to correlate that olefin content with other analyses such as bromine number. Here is an example of a polyalphaolefin residual olefin analysis. The olefin proton content (%H) was plotted against bromine number values obtained on each of the samples. A linear correlation was obtain but two different correlations were observed that were dependent on the viscosity index of the polyalphaolefin being analyzed. Figure 1 shows the 1H NMR spectra obtained on neat samples on a Picospin-80 spectrometer operating at 82.3 MHz. The methyl and methlene protons of the polymer backbone are plainly seen and the olefin and alpha-olefin protons are observed.
Figure 2 shows the linear correlation between %H olefin and bromine number with the two correlations caused by different VI grade being indicated. The analysis shows that for the two viscosity grades the grade can be identified from the linear correlation that the data falls onto and the %H olefins content can directly yield the bromine number. This NMR method provides an alternative to the following ASTM standards: D1159 Test Method for Bromine Numbers of Petroleum Distillates and Commercial Aliphatic Olefins by Electrometric Titration D1491 Test Method for Test for Bromine Index of Aromatic Hydrocarbons by Potentiometric Titration D1492 Standard Test Method for Bromine Index of Aromatic Hydrocarbons by Coulometric Titration D2710 Test Method for Bromine Index of Petroleum Hydrocarbons by Electrometric Titration D5776 Test Method for Bromine Index of Aromatic Hydrocarbons by Electrometric Titration
Poster to be Presented at the 56th ENC, Asilomar CA, April 2015
|NMR Detection of Tomato Paste Spoilage in 1,000 L, Metal Lined Totes
|Michele Martin1; Paul Giammatteo2; Michael McCarthy1; Matthew Augustine1
|1University of California, Davis, Davis, California; 2Process NMR Associates, Danbury, CT
Low field nuclear magnetic resonance (NMR) is used as a non-invasive method for detecting spoiled tomato paste. It is shown that the 1H T1 and T2 relaxation times change as tomato paste spoils due to changes in viscosity and/or changes in the concentration of paramagnetic compounds. With the goal of developing a spoilage detector that can be used in a tomato processing facility, a γBo = 19.5 MHz single-sided handheld NMR instrument is used. Due to the dominance of diffusion on relaxation measurements made with the single sided instrument, the slope of the amplitude of a spin echo for three different delay times is used to provide a viscosity dependent parameter that permits the differentiation between pristine and spoiled tomatoes.
One-Sided NMR – Non-Invasive Analysis of Tomato Paste
Back in October we presented a talk at Gulf Coast Conference that concerned the prediction of the chemical and physical properties of heavy petroleum feeds being converted to higher value product in a residual catalytic cracker (RCC). Over the years we have analyzed these materials by 300 and 60 MHz NMR and obtained good PLS-regression models that can adequately predict properties for real-time process control and optimization in a petroleum refinery. With the advent of a large number of new benchtop NMR systems we have been convincing ourselves that these types of analyses can be performed by systems such as the Magritek Spinsolve 43 MHz. We ran a series of samples that had been sitting around our lab for 15 years by dissolving them at about 50 volume% in a 50/50 CDCl3/CS2 solvent system. For each sample we had laboratory test data for a number of chemical and physical properties of interest to process engineers. We regressed the lab data variability against the variability in the Magritek 43MHz 1H NMR spectra and obtained cross-validated PLS models. The presentation material is given here at this link – Gulf Conference Presentation – 43 MHz RCC Feedstream Regression Models
PNA has been conducting a number of studies into the adulteration of male enhancement herbal suplements with PDE5 inhibitors such as viagra, cialis and a wide number of analogs (Mw approximately 475 amu). Standard materials for the analogs are quite expensive so in th eprocess of developing ID and purity methods on our NMR systems we ran the 1H NMR on our 300, 60, and 43 MHz NMR systems at a concentration of 5mg/ml which equates to 0.01 Molar. This PDF of the NMR data demonstrates the sensitivity and resolution obtainable on these bench-top 5mm NMR systems. They can readily look at samples at these concentrations. They can readily be utilized as screening tools or as quantitation and identification analyzers.
The PDF file containing the Varian 300, Aspect-60, and Magritek 43 MHz data can be found here: NMR Data-0.01 Molar_PDE5 Analogs 300_60_43_MHz
Here is an example of spectral reproducibility. We are doing a lot of beer NMR at the moment on our 300 MHz NMR and for "giggles" we are running many samples through the various bench-top systems in our lab. We have been quantifying small organic acids (lactic, acetic, succinic , malic, citric, etc.) as they can give some idea of yeast activities and health during fermentation. We are also quantifying and studying the 1,4/1,6 linkage distribution of residual dextrins. The series of superimposed spectra below consists of 28 spectra of a freeze dried beer sample (a unique Belgian Dubbel. Each spectrum was 128 pulses and took approximately 30 minutes per spectrum. So the superimposed data represents a 14 hour continuous stability test.The data was automatically processed with 16K zero-fill and autophase.It looks pretty damn good.
We've been looking at a lot of sour beers – here is a home-brewed Flemish Red aged in an oak barrel – note the high lactic and acetic content.
We've also been analyzing a lot of hard ciders – commercial and home-brewed varitieties of various styles – very different from one sample to another in the small molecule and sugar chemistry.
1H qNMR at 300MHz or 60 MHz can be utilized to identify and quantify small molecule chemistry in fermentations. Below is an example of a quantitative chemistry report on a series of ciders.
Beer and Cider Analysis is offered with similar quantitative results is offered for $100 per sample in our analytical lab.
Survey of Low Field NMR Spectrometer Platforms for Successful Screening of Sexual Enhancement and Weight Loss Supplements for Adulteration with Drugs and Drug Analogs
John C Edwards1, Kristie M Adams2, and Anton Bzhelyansky2
1Process NMR Associates, Danbury, CT
2United States Pharmacopeial Convention, Rockville, MD
The adulteration of dietary supplements (or natural health products) with synthetic pharmaceuticals is an area of increasing concern, which presents substantial risk to public health. Widely available in retail and via the Internet, these products are often marketed as sexual enhancement, weight loss and/or bodybuilding supplements. Unlike prescription drugs, supplements do not require premarket approval by FDA before they are made available for public consumption. In fact, the agency can only take investigational action after the adulterated product has caused harm and the adverse event has been reported via MedWatch (FDA's online portal for voluntary reporting of adverse events associated with drugs, medical devices and dietary supplements).
Development of analytical tools for screening and identification of adulterated products in the marketplace represents a significant step forward in the fight against adulterated dietary supplements. Several organizations, including AOAC and USP, have undertaken initiatives to evaluate and recommend analytical methodologies for screening supplements for adulteration. HPLC and mass spectrometry have so far dominated the screening and quantitation studies published in the literature, with NMR spectroscopy often relegated to the status of structure elucidation tool. In this work, we investigate the ability of several-low field NMR spectrometric platforms to successfully identify and quantify the presence of adulterating drug substances in sexual enhancement and weight loss supplements purchased online and in US retail. 1H qNMR of both types of samples was performed with 300 MHz NMR to confirm the presence of adulterants such as sildenafil, tadalafil, and their structural analogues (sexual enhancement supplements) and various synthetic stimulants (weight loss supplements). We have concluded that a simple sample preparation protocol combined with straightforward 1H NMR spectroscopic analysis yields a rapid, robust and reliable screening test for adulterated supplements, presenting an attractive alternative to more labor-intensive, expensive and expertise-demanding techniques du jour.
This was presented by John Edwards at SMASH in September 2014, and at the Carolina NMR Symposium in November 2014
presentation can found here: Benchtop NMR – Herbal Supplement Adulteration Screening
1H Benchtop NMR has great potential to increase the throughput of both routine and emergency fuel sample analysis in refinery laboratories. Currently fuel samples must be passed through multiple dedicated analyzers to obtain information such as density, H-Content, aromatics, olefins, saturates, benzene,
Octane numbers, cetane index, cetane number, distillation curves, vapor pressure, flash point, pour point, freeze point, cloud point, etc. Correlation of the 1H NMR spectra of these refinery fuel samples to these primary test results will allow all parameters to be predicted in about 40 seconds from the 4 pulse spectrum of the pure fuel. Here we have a few examples obtained on some diesel fuels that were submitted to our lab for ASTM D7171 – Hydrogen Content by TD-NMR. We had density, H-content, and aromatics wt% by GC. Below are three example correlation obtained on the Picospin 80 system (that requires 32 pulses per sample due to the capillary sample size). The results were very similar for the 300, 60, and 42 MHz data obtained on the three other NMR system in our laboratory. The comparative results are shown in Table II. The results are very similar independent of the field strength of the NMR system. The data from all 4 NMR systems is provided in this section.
Benchtop high-resolution NMR systems are available at a number of field strengths and probe configurations. However beyond the obvious academic instruction market for these instruments very few applications have been demonstrated across all available platforms and thus proving the general applicability of benchtop NMR technology to industrial quality control. We will present two chemometric-based applications that have been developed at 4 different field strengths utilizing Varian Mercury 300 MHz, Magritek Spinsolve 42 MHz, Aspect AI 60 MHz, and Thermo Picospin 80 MHz NMR systems. Partial-least-squares (PLS) regression correlations were obtained on all 4 platforms relating to:
1) Omega-3 fatty acid composition of samples taken from various points in a nutritional supplement manufacturing process. Excellent correlations were obtained on all 4 NMR instruments proving that NMR technology is applicable to in-lab, at-line. or on-line analysis of fish oil derived omega-3 fatty acid supplements. The 40 second NMR analysis effectively replaces a 60+ minute GC analysis.
2) Physical and chemical property determination of diesel fuels where excellent correlations were obtained between 1H NMR variability and parameters such as density, aromatic content by GC, hydrogen content by 1H TD-NMR (ASTM D7171 method), and sulfur content. Many more physical and chemical properties can be correlated to the 1H NMR spectrum allowing a single 40 second NMR experiment to predict 10-15 parameters that each require dedicated analyzers.
Finally, we will present the concept and initial results from an independent server-based NMR application software that can be utilized in conjunction with the NMR software of the current benchtop NMR systems, or alternatively as a stand-alone application platform. This software would effectively make chemometric and direct measurement NMR application ubiquitous across all NMR platforms.
A link to this presentation in PDF form is given here: PLS-Regression – 300_80_60_43 MHz NMR of Fish Oil Supplements and Diesel Fuel
Adam DiCaprio (ex PNA) gave an excellent Science Cafe Talk under the auspices of the ACS North Carolina Section at the Busy Bee Cafe in downtown Raleigh on December 2, 2014. CHanging gears from his previous talks he centered the discussion on malt and hop chemistry as well as an start-to-finish NMR analysis of production runs of a bottled commercial tavern ale. If you are interested in having Adam give a detailed chemistry seminar on beer at your section meetings please contact him directly at email@example.com.
A PDF version of his talk is available here …. ACS Science Cafe Talk – Dicaprio – Busy Bee Cafe – Raleigh NC – 12-2-14
Process NMR Associates is currently developing NMR applications based on direct measurement of chemometric modeling on NMR data obtained on numerous NMR platforms. Our intention is to develop solutions that can be executed on any NMR platform. With this in mind we are currently developing a fish oil analysis application that can provide the EPA and DHA omega-3 fatty acid content of fish oil supplements manufactured by an ethyl ester esterification process. We have obtained data at 42 MHz, 60 MHz, 82 MHz and 300 MHz. The chemometric modelling yielded PLS models for all 4 field strengths that yield effectively the same result – DHA can be measured to +/- ~1.1 wt% and EPA can be measured to +/- ~2.2 wt% by a 40 second 1H NMR measurement. THe correlation is derived from a regression of the 1H NMR variability with primary GC analysis values.
This analysis has been shown for the 300 and 60 MHz data in a previous post on this blog. The same analysis was also obtained, with similar results, on 42 and 82 MHz platforms proving that individual applications can be automated and provided at all relevant frequencies of NMR analysis whether on superconducting lab systems or permanent magnet benchtop systems.
At each field strength the relative lineshapes are pretty much the same (<1 Hz at half height). The field strength differences mean that the same spectrum is dispersed across frequency space proportionate to the magnetic field. Figure 1 below shows the frequency space spectra obtained at all 4 field strengths on the same sample.
Figure 2 shows the same spectra displayed on the usual normalized chemical shift scale (ppm). In these spectra the data is stretched in order to allow the chemical shift comparison of the data. IN effect the 42 MHz NMR is stretched by a factor of 7, the 60 MHz data by a factor of 5 and the 80.2 MHz data by a factor of 3.7. The effect of the relative size of J coupling compared to the frequency space occupied by 1 ppm is an interesting observation to see directly. In traditional NMR analysis the resolution of various peaks was always the driving force for increasing the magnetic field strength of NMR instruments. With todays powerful PC's and advanced software information can be garnished readily from any of these spectra by way of global spectral deconvolution or multivariate statistics.It is no longer necessary to obtain baseline resolution in order to integrate a resonance and obtain quantitative information.
THough the data is more closely packed together in the low field spectra it can be acknowledged that the same information is present in all 4 spectra. Automation approaches can be developed that will allow accurate measurement of quality parameters, component quantification, or structural verification to be performed on data obtained from any of these NMR systems.
The development of readily deployable NMR benchtop systems at an affordable price point must surely lead to the development of NMR into a more widely utilized technique outside of the realms of scientific study and quality control that NMR has thus far been involved.
Poster presented by Adam Dicapro at the 3rd Carolina NMR Symposium, Kannapolis, NC, November 6, 2014
Agilent Technologies to Close Nuclear Magnetic Resonance Business
SANTA CLARA, Calif., Oct. 14, 2014
Agilent Technologies Inc. (NYSE: A) today announced it is exiting its Nuclear Magnetic Resonance business. Agilent entered the NMR business in 2010, with the acquisition of Varian. Since then, the business has not met growth and profitability objectives.
"Today's announcement represents a difficult decision necessary to drive improved profitability," said Mike McMullen, president and chief operating officer, and CEO-elect. "The NMR team has been extremely dedicated and has made many excellent contributions. However, this action is a step in ensuring that our investments are placed on higher-value life sciences, applied markets and diagnostics solutions that will continue to drive growth across the company."
Agilent will stop taking new NMR system orders immediately, but the company will continue to meet customer commitments for orders in progress and for ongoing support contracts. Agilent will continue to provide service on all installed NMR systems.
The company expects that this decision will eliminate about 300 jobs, mostly within the next 12 months. The majority of the affected positions are located in Yarnton, U.K., and Santa Clara, California.
Today's announcement is part of Agilent's strategy to address the business shortfalls of its Research Products Division. In early 2013 Agilent announced its exit of the OEM and Specialty Magnet business and later the MRI business to focus resources on the core NMR portfolio. Despite these adjustments, the NMR business has continued to fall short of growth and profitability objectives.
To cover the cost of exiting this business, Agilent will take an approximate $72 million restructuring charge in the fourth quarter. It expects a $20 million to $30 million decline in revenues in fiscal year 2015 due to the NMR business closure, but a positive impact of about $10 million in operating profit in FY15.
For the fourth quarter of 2014, Agilent anticipates non-GAAP earnings per share of $0.87 to $0.91, and projects revenues to be negatively affected by currency at about $13 million, and lower NMR-related revenues by about $12 million.
Keysight has posted its investor roadshow slide deck on its website at www.investor.keysight.com. "New Agilent" will post its investor roadshow slide deck on Friday, Oct. 17, after the market closes at www.investor.agilent.com.
About NMR
Nuclear magnetic resonance (NMR) spectroscopy is an analytical chemistry technique used in quality control and research for determining the content and purity of a sample as well as its molecular structure. It is used primarily in academia and government, the pharmaceutical, biotech and chemical industries.
About Agilent Technologies
Agilent Technologies Inc. (NYSE: A) is the world's premier measurement company and a technology leader in chemical analysis, life sciences, diagnostics, electronics and communications. The company's 20,600 employees serve customers in more than 100 countries. Agilent had revenues of $6.8 billion in fiscal 2013. Information about Agilent is available at www.agilent.com.
On Sept. 19, 2013, Agilent announced plans to separate into two publicly traded companies through a tax-free spinoff of its electronic measurement business. The new company is named Keysight Technologies, Inc. The separation is expected to be completed in early November 2014.
Forward-Looking Statements
This news release contains forward-looking statements as defined in the Securities Exchange Act of 1934 and is subject to the safe harbors created therein. The forward-looking statements contained herein include, but are not limited to, information regarding the separation of Agilent's electronic measurement business; future revenues, earnings and profitability; the future demand for the company's products and services; and customer expectations. These forward-looking statements involve risks and uncertainties that could cause Agilent's results to differ materially from management's current expectations. Such risks and uncertainties include, but are not limited to, unforeseen changes in the strength of our customers' businesses; unforeseen changes in the demand for current and new products, technologies, and services; customer purchasing decisions and timing, and the risk that we are not able to realize the savings expected from integration and restructuring activities.
In addition, other risks that Agilent faces include those detailed in Agilent's filings with the Securities and Exchange Commission, including our latest Form 10-K and Form 10-Q. Forward-looking statements are based on the beliefs and assumptions of Agilent's management and on currently available information. Agilent undertakes no responsibility to publicly update or revise any forward-looking statement.
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"Beer Manufacturing and Analysis by NMR", John C. Edwards and Adam Dicaprio, Presented at the Mestrelab MNova Users, Meeting – SMASH, Atlanta, GA, September 7, 2014
Get PDF Here
"Survey of Low Field NMR Spectrometer Platforms for Successful Screening of Sexual Enhancement and Weight Loss Supplements for Adulteration with Drugs and Drug Analogs", John C. Edwards, Kristie Adams, Anton Bzhelyansky , Presented at SMASH Conference, Atlanta, GA, September 7-10, 2014.
Get PDF Here
"Liquid and Solid-State 27Al qNMR of an Elemin Senonian Trace Minerals Supplement for Identification, Chemical Structure, Quantitation of Active Ingredient in the Product, and Product Stability", Boris Nemzer, John C. Edwards, presented at XII International Conference on the Applications of Magnetic Resonance in Food Science: Defining Food by Magnetic Resonance, Cesena, Italy, May 20-23, 2014.
Get PDF Here
"Liquid and Solid-State Multinuclear 13C and 11B qNMR FruitexB Fructoborate Complex Nutritional Supplement. Identification, Chemical Structure, Quantitation of Active Ingredient in Product, and Product Stability", Boris Nemzer, John C. Edwards, presented at XII International Conference on the Applications of Magnetic Resonance in Food Science: Defining Food by Magnetic Resonance, Cesena, Italy, May 20-23, 2014.
Get PDF Here
"1H qNMR of EPA and DHA Omega-3 Fatty Acid Esters – PLS Regression Models Obtained by 60 and 300 MHz NMR – At-Line and On-Line Monitoring of a Fish Oil Nutritional Supplement Manufacturing Process", John C. Edwards, Paul J. Giammatteo, invited oral presentation at XII International Conference on the Applications of Magnetic Resonance in Food Science: Defining Food by Magnetic Resonance, Cesena, Italy, May 20-23, 2014.
"Application of High Field and Cryogen-Free Bench-Top NMR Platforms to the Monitoring and Quantitation of PDE5 Inhibitor Adulteration of Male Sexual Enhancement Supplements", John C. Edwards, Paul J. Giammatteo, Kristie Adams, Anton Bzhelyansky , presented at XII International Conference on the Applications of Magnetic Resonance in Food Science: Defining Food by Magnetic Resonance, Cesena, Italy, May 20-23, 2014.
Get PDF Here
"NMR Based Authentication of Nutraceuticals, Herbal Supplements, and Food Additives: Economic- and Efficacy-Driven Adulteration of Aloe Vera, Herbal Erectile Dysfunction Supplements, and Acacia Gum", John C. Edwards, invited presentation at the 2nd PANIC, Charlotte, NC, February 3-5, 2014.
Get PDF Here
"Development of an Automated Complex Mixture Analysis qNMR Method within Mestrelab MNova – Application to Aloe Vera and the Beer Brewing Process", John C. Edwards, Adam J. Dicaprio, Michael A. Bernstein, presented at the 2nd PANIC, Charlotte, NC, February 3-5, 2014.
Get PDF Here
"Small Molecule Chemistry of Spontaneously Fermented Coolship Ales", Adam J. Dicaprio, John C. Edwards, presented at the 2nd PANIC, Charlotte, NC, February 3-5, 2014.
Get PDF Here
"Liquid and Solid-State 1H, 13C, and 11B qNMR Analysis of Fruitex-B®– A Calcium Fructoborate Comple: Chemical Structure and identification, quantitative analysis and stability study", Boris Nemzer, John C. Edwards, presented at the 2nd PANIC, Charlotte, NC, February 3-5, 2014.
Get PDF Here
I have been invited to be a guest editor for Wiley publishing to pull together 2 special issues of Magnetic Resonance in Chemistry. I am putting out a general "call for papers" but I will harass people personally. We are looking for 10-20 papers for each issue.
The deadline for submission of the papers is June 30 so no-one has an excuse that there isn't enough time. I do ask that you email me at the contact below to let me know that you are thinking of submitting and a title would be nice also (though I won't hold you to it). We hope to have the review and revide papers (if necessary) by late October and then publish by December 2014.
The first will be on high resolution benchtop NMR in which I would like to include all permanent magnet systems capable of obtaining a spectrum. This is an open invitation to all the vendors and their customers of (in no particular order) Anasazi, Nanalysis, One Resonance Sensors, Magritek/ACT, Aspect, Qualion, Picospin, Resonance Systems, Oxford Instruments, Bruker, home built devices, I would also make the exception that HTS systems be included as they are also cryogen free.
Any papers on spectrometers, magnets, educational, industrial, academic applications, chemometrics, automated approaches, reaction monitoring, online/at-line utilization, 2D NMR, combined spectral/relaxation applications.
The second will be on low resolution benchtop NMR but I would like to exclude applications that have been around for decades (H content, SFC, oil content, spin finish). I would like to encourage new applications to be submitted and they should include hardware, magnets, spectrometers, probes, 1D/2D Laplace inversion (I'd love a review/overview of that software aspect), applications. Again – all vendors and all users of commercial and home grown benchtop TD-NMR systems please submit.
We're looking for articles on FPGA spectrometers, software approaches (1D/2D Laplace, chemometrics), magnet design and construction, dedicated rheology analysis instruments, field cycling NMR, unilateral NMR, core analyzers, applications of all whether educational, academic, industrial.
The types of articles can be Reviews, Mini-Reviews, Tutorial, Historical, Spotlight, Perspective, Communication, Article, Application Note, Case Report, Spectral Assignments, Correspondence.
Here is the official word on the use of color (note you can have all the color figures you wish in the online version but the print version is restricted): two colour illustrations per submission are allowed free of charge, however further colour illustrations are allowed at the Editors discretion and where they are justified. Authors can have as much colour as they like in the online version as the restrictions are just for the print version.
Please contact me directly if you would like to make a submission of your work to either of the two issues: firstname.lastname@example.com
I have posted the authors instructions for special Issues that I was given on my website at:
The MRC author guidelines can be found at:
A herbal supplement marketed to alleviate erectile dysfunction was recently submitted for testing in our laboratory because it was surprisingly effective considering it should only contain the traditional herbals utilized for this problem such as Oyster, 2-Deoxy-D Glucose, Barberry, Snow Lotus, Bombyx Mori L., Ginger Root, Salfron Crocus.
Above: 1H NMR of ED Herbal Supplement – this is an extract of the powder from the capsules into 80:20 CD3CN:D2O – Observed suspicious specific small molecule peaks – herbals are usually broad featureless complex mixture spectra. This is something in different – a specific drug material appears to have been added.Comparison with the spectrum of Viagra (Sildenafil Citrate) below shows a strong similarity between the 2 active ingredients.
We also obtained the COSY, 13C and DEPT NMR Spectra on the ED herbal supplement. These are shown below.
The analysis of the NMR data led us to find that the extractable components of the sample contained predominantly Sulfoaildenafil (thioaildenafil) which is a strutural analog of Sildenafil (Viagra) and is not approved by any health regulation agency for use in erectile dysfunction medicines or supplements. Apparently these structural analogs to Viagra are found widely in herbal supplements sold for this malady. I guess we have one more for the list that the FDA keeps on such dangerously adulterated products.
We have an excellent solid-state Doty Scientific Supersonic 7mm CP-MAS probe for our Varian UP-200 spectrometer. This is a nice field strength for solid-state 13C analyses as it allows for spectra at higher sensitivity than a 100 MHz but still has the advantage that 7 kHz is enough to push the aromatic MAS sidebands beyond 0 ppm so that more accurate aromaticity values can be calculated. The probe is still working after 20 years and we are using the original rotors and have never had to replace any of the capacitors. We have run approaching 20,000 experiments with this probe. Here are some of the nice spectra we have been getting recently on drug API and tablets.
Above: Solid-State 13C NMR of Rapamycin API
Above: Solid-State 13C NMR of Ranitidine HCl – Zantac Tablet
Above: Solid-State 13C NMR of Simvastatin 20 mg Tablet


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Re: TTC... I read this write-up and I find it hard to believe that Brokerage houses would resort to this kind of action... or why it would even be legal and allowed. There is so much to-do about compliance and all.. governing the way individuals trade ... that you would think that there should be some compliance reguarding these Brokers...I must be considered very Naive by most of you traders.... ,but , tell me do you think this is Right.?