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The Green Bean Casserole is in a white ceramic dish topped with French onions.
1" x 3/4"
Scale: 1/12
Assembly Required:
No1/12 scale, also referred to as one-inch scale (or 1" scale), means 1 inch = 1 foot
I was very happy with this casserole dish. It is very realistic looking and a perfect compliment to my Easter ham platter and crescent rolls.
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Yucaipa, CA's finest, a line-up changing band lead by Davey Marvich, with layers of vocal and guitars that bring At the Drive-In comparisons. Their only album "Your New Face Of Corruption" self-released in 2003 was called "9 tracks and 35 minutes of pure goodness." The band parted ways shortly after the release, but left behind tracks leaving listeners wondering "what if…". Autumn's Leaves featuring dueling vocals, heavy guitars, and melodic keyboards became a quick hit with listeners and online fans of early social network sites like notpopular.com. The members have gone on to form other bands including Eva Elliott.
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text: We booked the court yard room, expecting it to lead into a court yard or somewhere close to a court yard...it didn't. Besides that, the room was old, gave an air of not being clean, was dark, lacked decor, the air conditioner was old, the tv didn't work and there was no remote for the tv to begin with. The... More


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Bristol Bay: Washington senator, chefs protest Pebble Mine
Donna L. Hansen, congressional staffer
GOP promise of immigration reform fades a year after election
EPA urges protection for Bristol Bay, putting new Alaska mine at risk
As Hispanic voters' numbers increase, politicians come calling
CO2 sensitivity possibly less than most extreme projectionsStory | Nov 25, 2011A new study in the journal Science suggests that the global climate may be less sensitive to CO2 fluctuations than predicted by the most extreme projections, and maybe slightly less than the best estimates of the Intergovernmental Panel on Climate Change....
Doug Brinkley, Rep. Don Young squabble over Arctic refugeStory | Nov 22, 2011Famed biographer Doug Brinkley and Alaskan Rep. Don Young clashed bitterly last Friday as Brinkley, a professor at Rice University and the author most recently of "The Quiet World: Saving Alaska's Wilderness Kingdom 1979-1960," testified...
Inupiat whaling, drilling at stake in recent Alaskan mayor's raceStory | Dec 6, 2011Independent photojournalists Will Rose and Kajsa Sjölander were on Alaska's North Slope in November to document traditional whaling by the native Inupiat people, and found themselves at the height of a highly charged mayoral election season, with...
Year in Review: Congress' 10 biggest enemies of the EarthStory | Dec 14, 2011Republicans launched an unprecedented frontal assault against environmental protections and regulations this year, prompting Rep. Henry Waxman (D-Calif.) to call his chamber "the most anti-environment House in history." Here are the 10 most powerful and...
Sarah Palin emails: Governor had icy relationship with state's congressional delegation
Sarah Palin sought, got federal porkBlog | Sep 2, 2008by Frank James Alaska Gov. Sarah Palin apparently likes a good earmark as much as most other politicians. The watchdog group Taxpayers for Common Sense found that when Palin was mayor of little old Wasilla, Alaska she hired a well-connected......


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If the New Year's Resolutions you made six months ago are a distance memory, the Summer Solstice offers is a great time to stop and take stock of where you are, where you want to be, and how much you have to be grateful for. Think of today as an opportunity to reset and...
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Dr. Jay Williams from Virginia Tech joins us in the podcast today to talk about using social media to translate sports medicine to the public, especially in the area of soccer. Jay actually works in the area of molecular biology and sports and in the last few years has really been working to make Sports Science understandable to the public. So join us for this fun conversation!
In the past few months, there have been several football players that have collapsed and died away from the field. So how much risk do these athletes have for sudden death. Dr. Stephen Crouse, an expert in athletic medical screen joins us in the podcast today to talk about what we know about athletic sudden death and the real risk to athletes.
We've got a great conversation with Mr. Adam Davis who is the Strength and Conditioning Coach for Stewart-Haas Racing, the parent company of the race teams of Tony Stewart and Ryan Newman in NASCAR's Spring Cup Championship Series. We talk about strength training of pit crew athletes and injury issues for the pit crew athlete
Phone: 979-845-3475 Fax: 979-845-6505


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The Crotch Test
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True Blood
True Blood's Alexander Skarsgard "Tied Up": Yes or No? (PHOTOS)
True Blood's Alexander Skarsgard may be in the running to play Fifty Shades of Grey's S&M-loving Christian, but he's the one we want to see tied up.
Well, in his suit, that is.
At premieres, A. Skars typically rocks a crisp, dark-colored suit, but we never know if he's going to show up in a tie. And although he occasionally changes it up with a bow, he typically wears solid-colored, no-frills neckwear.
During the Japanese premiere of Battleship on April 3, 2012 (pictured right), Alex wore a dark grey, pinstripe suit with a perfectly-coordinated tie. Even with one button of his jacket undone, he looked polished and incredibly sexy.
On the flip side, he ditched the tie in favor of a gorgeous navy suit and plain white button-down at the 2012 Film Independent Spirit Awards on Feb. 25, 2012. In the photo, he's shown buttoning up his jacket, sporting a large black watch and his signature smirk.
We love Alex, no matter what he is (or isn't) wearing, but we want to know which you prefer. Do you like him "tied up" or looking more casual without anything around his neck? Vote below!
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Florida bacteria alert: Beware of warm saltwater if you have open cuts
There's lots of ways Florida can kill you, not the least of which is Vibrio vulnificus, a rare and potentially deadly bacteria found in warm salt water.
There's lots of ways Florida can kill you, not the least of which is Vibrio vulnificus, a rare and potentially deadly bacteria found in warm salt water.
Not all brain cancers are the same but together they represent a deadly disease that has been difficult to identify and treat. Scientists at multiple institutions have found a new way of classifying brain cancers that could ...
Housing improvements could reduce malaria cases by half in some settings, according to research published in the open access Malaria Journal.
Sierra Leone on Wednesday berated the "selfish and shameful" behaviour of people risking a resurgence of the Ebola virus by flouting quarantine restrictions, as authorities announced a spike in cases.
Health officials say fewer Americans are getting sick from a nasty germ sometimes found in undercooked hamburgers.
More than 26,000 people have been infected with Ebola since the outbreak began and more than 10,800 have died, the World Health Organization said Wednesday.
Australia Sunday unveiled a Aus$26 million (US$20 million) package to increase child vaccination rates, as it removed a religious exemption allowing parents unwilling to immunise their children to claim some government benefits.
Patients with chronic heart failure, a deadly disease that worsens as the heart pumps less blood through the body, are getting a much-needed new option.
Guinean President Alpha Conde has declared a 45-day "health emergency" in five regions of the Ebola-hit nation in a bid to stem the spread of the deadly disease.
A new study, published today in the journal PloS Neglected Tropical Diseases has given new insights into the spread of rabies in the Middle East, showing that the deadly disease regularly moves between countries in the re ...
A Liberian woman who last week became the country's first Ebola patient in more than one month has not passed on the infection to anyone else, a senior official said Wednesday.
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The young people who learn martial arts at a studio north of Detroit are not considered students.
The United Nations must learn lessons from the Ebola crisis and begin preparing now for the next outbreak of deadly disease, Secretary General Ban Ki-moon said Monday.


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STARmeterSEE RANK
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Faune A. Chambers
Faune A. Chambers was born on September 23, 1976 in Florida, USA as Faune Alecia Chambers. She is known for her work on The Curious Case of Benjamin Button (2008), Epic Movie (2007) and White Chicks (2004). She has been married to Fonzworth Bentley since 2010. They have one child. See full bio »
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- Bachelor of Arts
- MA in Clinical Psychology
- Graduate Education
- Continuing Education
PsyD in Clinical Psychology Faculty
- Betsy Bates Freed
- Allen Bishop
- Peter Claydon
- Bella DePaulo
- Jody Eng
- Lisa Firestone
- Christopher J. Howard
- Dean Janoff
- Steven Kadin
- Brett Kia-Keating
- Heather LaFace
- Christine Lewis
- Denise Mock
- Sharleen O'Brien
- Rachel Penton
- Ron Pilato
- Indhushree Rajan
- Gil Reyes
- Richard F. Sperling
- Salvador D. Treviño
- Marlene Valter
- Radhule Weininger
- Lee Weiser
- Randy Wood
Lisa Firestone, PhD
Adjunct Faculty
Lisa Firestone, PhD, received her PhD from the California School of Professional Psychology in 1991. Since 1987, she has been involved in clinical training and applied research in suicide and violence. In collaboration with Dr. Robert Firestone, her studies resulted in the development of the Firestone Assessment of Self-Destructive Thoughts (FAST), the FASI, and Firestone Assessment of Violent Thoughts (FAVT), and the FAVT- A (for adolescents).
She has been a practicing clinical psychologist in Santa Barbara and Los Angeles for the last 20 years and works as the Director of Research and Education at The Glendon Association. Dr. Firestone has published numerous peer reviewed articles, and is the co-author of Sex and Love in Intimate Relationships (2006), Conquer Your Critical Inner Voice (2002), and Creating a Life of Meaning and Compassion: The Wisdom of Psychotherapy (2003).
Dr. Firestone is a much requested presenter at national and international conferences in the areas of couple relations, parenting, and suicide and violence prevention. Dr. Firestone is the Senior Editor for the psychological website for the public www.psychalive.org and she is a regular blogger on Psychology Today and the Huffington Post.


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Are you wondering what Pickemfirst is all about ?
Watch this 2-minute YouTube video...
Player Timeline
May 27:
Iglesias's knee is still dealing with some minor swelling, but it available to pinch hit and can take grounders that are hit "right at him" according to manager Brad Ausmus, Lynn G. Henning of The Detroit News reports.
May 25:
Manager Brad Ausmus indicated Monday that he's be "shocked" if Iglesias required a stint on the disabled list, James Schmehl of MLive Media Groupreports.
May 24:
Manager Brad Ausmus said that an MRI and X-rays on Iglesias' bruised knee showed no structural damage, MLive.com's Chris Iott reports.
May 23:
Iglesias left Saturday's game with a left knee contusion and should be considered day-to-day.
May 18:
Iglesias singled with two out in the seventh on Monday night to extend his hitting streak to nine games. He finished 1-for-3 with a stolen base.
May 14:
Updating a previous report, Iglesias will start at shortstop Thursday afternoon against the Twins, MLB.com's Jason Beck reports.
May 13:
Iglesias reached based in each of his first three plate appearances Wednesday night. He walked once and singled twice.
May 12:
There is still some chance Iglesias (groin) will be scratched from Tuesday's lineup against the Twins, as the Tigers want to see their shortstop run before making a final decision, Tony Paul of the Detroit News reports.
May 07:
Iglesias is still dealing with a groin issue and will likely be out until at least Saturday, MLive's Chris Iott reports. "It will probably be a couple days, I would think," manager Brad Ausmus said Thursday of when Iglesias might get back in the lineup.
May 06:
Iglesias (groin) is in the lineup Wednesday against the White Sox, Colleen Kane of the Chicago Tribune reports.
May 03:
Iglesias (groin) is hopeful that he'll be able to play Tuesday against the White Sox, James Schmehl of MLive.com reports.
Apr 18:
Iglesias delivered the Tigers the win Friday over the White Sox with his first-ever walk-off hit in the ninth inning. He put a single through the right side.
Apr 15:
Iglesias went 1-for-2 with a walk and his fourth steal of the year Wednesday against Pittsburgh.
Apr 14:
Iglesias went 2-for-3 including a double and scored a run Tuesday against Pittsburgh. He is now 12-for-25 (.480) on the season.
Apr 08:
Iglesias' strong start to the season continued Thursday as he went 4-for-4, including a double, and scored three times in the Tigers' rout of the Twins.
Apr 06:
After missing the entirety of the 2014 season with stress fractures in his shins, Iglesias had a strong debut Monday, going 2-for-3 with a pair of stolen bases.
Mar 29:
Iglesias played a full nine-inning game Saturday for the first time this spring, MLive.com reports.
Mar 12:
Iglesias (leg) plans to start at shortstop in Friday's spring game, and serve as the DH Saturday, James Schmehl of MLive Media Group reports.
Mar 05:
The Tigers will continue to bring Iglesias along slowly this spring, using him on alternating days for Grapefruit League games, the Detroit News reports.
Mar 01:
Iglesias is starting at shortstop and hitting second inf the Tigers' first spring lineup, Anthony Fenech of freep.com reports.
Feb 25:
Iglesias (leg) could serve as the designated hitter early in spring training to get in extra at bats, Anthony Fenech of the Detroit Free Press reports.
Feb 21:
Iglesias (shins) is only running at about 85-90 percent intensity, Anthony Fenech of the Detroit Free Press reports.
Feb 19:
Tigers manager Brad Ausmus admitted that "there's a little bit of concern" regarding how Iglesias' shins will hold up over the long grind of the season, MLive.com reports.


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Submitted by Rajvir Khanna on Mon, 04/07/2014 - 20:01
Odisha's Naveen Patnaik-led government has no objection to the allocation of the Khandadhar iron ore mines to South Korea's steel producer Posco, a senior official of the state government said.
The Khandadhar iron ore mines in Sundargarh to Posco-India in 2009 for its proposed 8-million-tonne steel plant in Jagatsinghpur district of the state. But, the state's High Court later annulled the allocation, forcing the Odisha government to approach the Supreme Court.
Submitted by Keshav Seth on Thu, 08/01/2013 - 17:39
South Korean steel giant Posco can start its $12 billion Odisha project as the road for the acquisition of nearly 3,000 hectares of land required for the first phase of the project is clear, Commerce & Industry Minister Anand Sharma said.
Speaking on the sidelines of CII's Asian Business summit on Wednesday, Mr. Sharma said, "For phase-1, now road is clear... To the best of my understanding, close to 3,000 hectares, if not more, of land parcel required for stage-1 is cleared."
Submitted by Gaurav Mehra on Wed, 07/17/2013 - 19:14
South Korea-based steel giant Posco on Tuesday confirmed that it has ditched plans to build a $5.3 billion (£3.5bn) steel plant in India's southwest state of Karnataka.
Posco announced in a statement that it decided to ditch the project due to delays in securing required mining rights, land and infrastructure and opposition by local people.
Confirming the decision, the company said, "We have agreed to drop the project given a delay in (acquiring mining rights) and opposition by local people."
Submitted by Dalbir Sahota on Tue, 07/16/2013 - 23:47
Bangalore, July 16 : Due to prolonged delay in land acquisition, South Korean steel major Posco has decided to pull out of Karnataka where it was planning to set up its $5.3-billion (Rs. 31,800-crore) steel plant, a top company official said Tuesday.
"We have decided to scrap the six-million tonne steel project in Karnataka due to long delay in acquiring the required land in the state," Posco India chairman and managing director Yong Won Yoon said in a statement here.
Submitted by Mitra Pathak on Tue, 07/16/2013 - 16:00
Political instability and ongoing opposition from residents have reportedly forced South Korea's Posco to reconsider its decision to build a $5.3 billion steel plant in Karnataka.
Citing an anonymous source, Reuters said in a report that Posco - the world's fifth-largest steel producer by output - is reviewing the plan and a decision on whether or not to drop the plan could be announced later this week.
Submitted by Hardeep Sidhu on Thu, 07/04/2013 - 20:47
Bhubaneswar, July 4 : Korean steel major Posco's plan to build a $12 billion steel project in Odisha got a boost with the state authorities Thursday declaring that land acquisition for it was complete and 2,700 acres of land had been acquired for the 12 million tonnes per annum greenfield steel project touted as India's single-largest foreign direct investment.
The administration has demolished all the betel vines over 2,700 acres in Jagatsinghpur district, where the project will come up, District Collector Satya Kumar Mullick told IANS.
Submitted by Divesh Sharma on Wed, 05/29/2013 - 23:01
The National Green Tribunal (NGT) has said in a new order on Tuesday that status quo must be maintained at the proposed Posco steel plant site in Jagatsinghpur district. The order will halt any further felling of trees by the state government for clearing the site for the proposed plant.
Submitted by Neha Malik on Sat, 05/11/2013 - 18:34
In a Friday verdict, the Supreme Court invalidated an Orissa High Court order which had annulled the State government's January 2009 recommendations in favour of granting an iron ore mining licence to South Korean steelmaker Posco.
The decision by the Supreme Court may pave the way for Posco to get the necessary go-ahead for a much-awaited preferential access to iron ore for the $12 billion project which the company has planned in Orissa.
Submitted by Keshav Seth on Fri, 05/10/2013 - 23:20
World's fourth-largest steel producer, POSCO of South Korea has said that it welcomes the latest order by the Supreme Court of India, in which it said that the government will decide on giving preferential access to iron ore to the company.
Submitted by Malini Ranade on Tue, 04/23/2013 - 22:51
The authorities in the state of in Odisha are acquiring land for the Posco steel plant in Jagatsinghpur district even as protestors gather to prepare for protest against the project.
Hundreds of angry villagers including large number of women gathered to protest against the land acquisition work in the Jagatsinghpur district, where the authorities have been deploying security arrangements to speed up the process of land acquisition work for the Posco Project.


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39 • Corona, CA • Man
I'm looking for
- Women
- Ages 25–43
- Near me
- Who are single
- For new friends
My details
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- Yesterday – 8:40pm
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- Straight
- Ethnicity
- Black
- Height
- 6′ 0″ (1.83m)
- Body Type
- Fit
- Smokes
- No
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- Not at all
- Drugs
- Never
- Religion
- Christianity, and very serious about it
- Education
- Graduated from university
- Job
- Law
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- $100,000–$150,000
- Status
- Single
- Speaks
- English
My self-summary
Write a little about yourself. Just a paragraph will do.
A fun outgoing guy who is passionate about life. I looking for a woman is ready to receive love and give love as well. Lets make a easy love connection and enjoy life having fun and being best friends. Life is so short.
What I'm doing with my life
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Enjoying my career. Helping others and traveling.
The six things I could never do without
Think outside the box. Sometimes the little things can say a lot.
The gym
A good meal
Love from my family
The gym
A good meal
Love from my family
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A luminescent sensory material for the detection of the presence of organo-halogen compounds is described. This material is based on a platinum chromophore functionalized with pyridylacetylide ligands, as shown in Formulae I and II below. These complexes exhibit positive luminescence upon exposure to the vapors of organ-halogen compounds like CH2Cl2 or CHCl3 with high selectivity over non-chlorinated common organic vapors. Direct relationships between vapor concentration and luminescence intensity are established using thin films prepared from these complexes.
2. The platinum complex of
3. The platinum complex of
4. The platinum complex of
5. The platinum complex of
6. The platinum complex of
7. The platinum complex of
8. The platinum complex of
9. A method of detecting the presence of organic-halogen compound in a sample including the steps of:
R1 to R10 to are each independently hydrogen, alkyl, aryl, alkoxy, halogen, amino or carboxy; and
Ar1 and Ar2 are each independently aryl or pyridyl; and
sensing or observing whether
a) the platinum complex changes color; or
b) the platinum complex causes luminescence after being irradiated by a beam of light,
wherein such a color change or luminescence indicate the presence of said organic-halogen compound.
10. The method of
11. The method of
12. The method of
13. A method for preparing the platinum complex as claimed in
in the presence of a base, wherein
R1 to R10 are each independently hydrogen, alkyl, aryl, alkoxy, halogen, amino or carboxy;
Ar1 and Ar2 are each independently pyridyl or substituted pyridyl;
X is selected from the group consisting of Cl, Br, I, —OSO2—CF3, and —OOC—CF3.
14. The method of
This invention relates to platinum complexes that can be incorporated into sensor devices for detecting organic-halogen compounds.
Organic-halogen compounds, including dichloromethane (CH2Cl2) and chloroform (CHCl3), are widely used solvents in laboratories, industry and hospitals. However, many of such halogenated compounds are suspected carcinogens and are irritants to the eyes, skin and respiratory system. For example, inhaling the vapors of dichloromethane and chloroform can damage the health of operators due to the extremely high volatility and relatively low olfactory-sensitivity of these two solvents. Also, other organic-halogen compounds such as polychlorinated alkanes and biphenyls have become a significant environmental problem because extremely minute levels are believed to present a health risk. Therefore, there is an increasing need to monitor and screen the presence of organic-halogen compounds in the environment. In particular, sensory materials for dichloromethane, chloroform and other volatile organic compounds (VOCs) with high sensitivity and selectivity are in demand for in vivo environmental monitoring and evaluation.
Luminescent probes provide a convenient method for sensor device design and application. The most common photoluminescence sensor utilizes intensity responses to analytes under conditions of constant irradiation. Ideally, the photoluminescence intensity change is selective, reversible, and sensitive to the analyte of interest. Regardless of the origin, intensity-based sensing has the advantage of being straightforward, inexpensive, and easy to implement. Noble metal complexes have been extensively studied as luminescent sensory materials for pH, cations, anions and so on. Recent progress has also shown that some of these complexes may exhibit vapochromic properties and give luminescent responses in the presence of VOCs and gases. These luminescent probes can be divided into three main types in view of the nature of the vapor-complex interaction mechanism: (a) discrete metallocyclophanes possessing large cavities that can accommodate VOC molecules; (b) oxygen-quenching phosphorescent lumophores tailored into mesoporous materials such as zeolite, rubber and sol-gel; (c) molecular solids that change their crystal lattice or chemical structures upon interaction with vapors.
The electronic structures of square-planar platinum(II) complexes are often sensitive to solid-state effects and the polymorphism of diimine Pt(II) complexes is well known. Recently, the development of luminescent Pt(II) complexes has revealed low-energy excited states. Coordinately unsaturated platinum(II) luminophores and their applications as molecular sensors have also generated immense interest. Many investigations have shown that the color and emissive properties of crystalline Pt(II) diimine salts are highly dependent upon the chosen anion and solvent(s) for the precipitation/recrystallization and differences in the extent of π—π and/or Pt—Pt interactions are usually presumed to be the reason of these phenomena. However, practicable sensory devices for VOCs are still sparse, largely due to ineffective coupling of vapor inhalation (trigger) to emission change (response). Technologically, a "switch-on" sensor is more desirable than a "switch-off" one; that is, there is higher practical value for a solid sensory material that can provide a positive luminescent response for the appearance of vapors and gases.
U.S. Pat. No. 5,766,952 by K. R. Mann et al describes a vapochromic double-complex salt of platinum(II) which changes its color, absorption or emission spectra upon exposure to VOCs, and can therefore be used in sensor devices for environmental evaluation. These Pt(II) complexes are chemically represented by the formulae [Pt(CN—C6H4-alkyl group)4][Pt(CN)4] and [Pt(diimine)(CN—C6H4-alkyl group)2][Pt(CN)4]. The deviations of Pt—Pt contacts induced by vapor inhalation are believed to account for the changes in the electronic spectra. However, such complexes are "switch-off" sensors showing negative luminescent response in the presence of CH2Cl2.
Very recently, a report on detection of volatile organic compound vapors by using a sol-gel material doped with a vapochromic complex of formula [Au(PPh2C(CSSAuC6H5)PPh2Me][ClO4] appeared on Appl. Phys. Lett. 2000, 77, 2274. However, the sensing mechanism relies on vapor-induced changes in the refractive index of the film, which may give rise to false signals and therefore may not be specific.
Therefore, it is an object of this invention to resolve at least one or more of the problems as set forth in the prior art. As a minimum, it is an object of this invention to provide the public with a useful choice.
Accordingly, this invention provides a platinum complex of the formulae I or II
It is another aspect of this invention to provide a method of detecting the presence of organic-halogen compounds in a sample by exposing the sample to the above platinum complex of the formulae I or II. If the platinum complex changes color or causes luminescence after being irradiated by a beam of light, such phenomena indicates the presence of said organic-halogen compounds.
It is yet another aspect of this invention to provide a method for preparing the above platinum complex of the formulae I or II. The above platinum complex of the formulae I or II may be synthesized by reacting a platinum complex of the formulae III or IV
The alternative embodiments of this invention may be apparent to one skilled in the art, and will be described in the following section.
Preferred embodiments of the present invention will now be explained by way of example and with reference to the accompany drawings in which:
This invention is now described by ways of example with reference to the figures in the following paragraphs.
In the definitions of the complexes below, collective terms were used which generally represent the following groups:
The term "partially or fully halogenated" is meant to express that in the groups characterized in this manner the hydrogen atoms may be partially or fully replaced by identical or different halogen atoms as mentioned above.
The objects of the present invention may be fulfilled by a novel chemosensory material for the detection of organic halogen compounds. This material is based on the diimine platinum complex functionalized with pyridylacetylide ligands. The chemical structure of this complex is shown in Formulae I and II below:
This novel material provides 'switch-on' luminescence upon exposure to organic-halogen compounds, like the vapors of CH2Cl2 or CHCl3, with high selectivity. The compounds may be prefered to be used as a crystalline powder. If the compounds are used in solution, the detection speed may be lower due to the time required to exchange the solvated solvent molecule by the organic-halogen compounds. The vapor inhalation and corresponding emission changes may be reversible, and the monitored emission wavelength (450–650 nm) for complex 1 that will be described below falls into the visible range. Quantitative studies show that thin films of this sensory material display substantial luminescence enhancement in the presence of organic-halogen compounds like CH2Cl2 and CHCl3 vapors but not for other VOCs, for example, acetonitrile, acetone, toluene, methanol and ethanol. No obvious difference is observed when the carrier gas is oxygen or air. Quantitative studies with thin films of this material show that good linearity is obtained in complex 1 between vapor concentration and luminescence intensity for CH2Cl2 and CHCl3 respectively in the concentration range of 0–3�104 ppm. A film deposited with complex 1 is more sensitive for CH2Cl2 (detected limit ˜25 ppm) compared to CHCl3 (detected limit ˜450 ppm).
The present invention is generally directed to syntheses, and structural and spectroscopic properties of a novel luminescent sensory material and its applications in detecting the vapors of dichloromethane and chloroform. Special design features of this sensory material include:
The starting materials [Pt(diimine)Cl2] (K. D. Hodges et al, Inorg. Chem. 1975, 14, 525) and 4-ethynylpyridine (L. D. Ciana et al, J. Heterocyclic Chem. 1984, 21, 607) were prepared according to literature methods. The other chemicals were obtained from commercial sources.
Generally, the platinum complexes of this invention is synthesized by reacting a platinum complex of the formula III or IV
Complex 1: A mixture of [Pt(4,4′-di-tert-butyl-2,2′-bipyridine)Cl2] (0.18 g, 0.34 mmol), 4-ethynylpyridine (0.12 g, 1.2 mmol), diisopropylamine (3 mL) and CuI (5 mg) in degassed dichloromethane (30 mL) was stirred for 12 h under a nitrogen atmosphere at room temperature in the absence of light. The resulted yellow solution was evaporated to dryness. The crude product was purified by flash chromatography (neutral Al2O3, CH2Cl2 as eluent) and recrystallized from dichloromethane/diethyl ether to give greenish-yellow needles (0.2 g, 88% yield) or from acetonitrile to give yellow prisms. IR (Nujol): ν=2116, 2128 (m, C≡C) cm−1; FAB MS: 668 (M++H); elemental analysis (%): calcd for C32H32N4PtCH2Cl2: C 52.66, H 4.55, N 7.44; found: C 52.83, H 4.54, N 7.05; 1H NMR (300 MHz, CDCl3, 22� C., TMS): δ=9.56 (d, 2H, J=6.0 Hz), 8.46 (d, 4H, J=4.6 Hz), 7.99 (s, 2H), 7.63 (d, 2H, J=6.0 Hz), 7.35 (d, 4H, J=4.6 Hz), 1.45 (s, 18H). 13C{1H} NMR (400 MHz, CD2Cl2, 22� C., TMS): δ=166.1, 157.9, 152.4, 151.0, 137.4, 127.9, 126.6, 121.1, 101.3, 97.0, 37.5, 31.6. Depending on the recrystallization solvent, two types of solvated crystals, namely 1 CH2Cl2 and 1 CH3CN were obtained and resolved by X-ray crystallography; these revealed different crystal lattices related to deviations in C—H..π (C≡C) interactions. In 1 CH2Cl2, a structure with C2v symmetry was found (
Complex 2: A mixture of [Pt(3,3′-dimethyl-2,2′-bipyridine)Cl2] (0.15 g, 0.30 mmol), 4-ethynylpyridine (0.12 g, 1.2 mmol), diisopropylamine (3 mL) and CuI (5 mg) in degassed dichloromethane (30 mL) was stirred for 12 h under a nitrogen atmosphere at room temperature in the absence of light. The resulted suspension was filtered and the orange powder was collected after washing with CH2Cl2 and diethyl ether. FAB MS: 583 (M++H); 1H NMR (300 MHz, DMSO-d6, 22� C., TMS): δ=9.24 (d, 2H, J=6.5 Hz), 8.58 (s, 2H), 8.40 (d, 4H, J=4.0 Hz), 7.71 (d, 2H, J=6.4 Hz), 7.28 (d, 4H, J=4.3 Hz), 2.52 (s, 6H).
Complex 3: A mixture of [Pt(COD)Cl2] (0.50 g, 1.3 mmol), 4-ethynylpyridine (0.31 g, 3.0 mmol), diisopropylamine (10 mL) and CuI (20 mg) in degassed dichloromethane (100 mL) was stirred for 12 h under a nitrogen atmosphere at room temperature in the absence of light. The resulted suspension was filtered and the off-white powder was collected after washing with CH2Cl2 and diethyl ether. 1H NMR (300 MHz, CDCl3, 22� C., TMS): δ=8.44 (d, 4H, J=4.6 Hz), 7.22 (d, 4H, J=4.6 Hz), 5.73 (s, 4H, with 195Pt satellites, JPt-H=45.1 Hz), 2.61 (s, 8H). A mixture of the obtained powder (0.10 g, 0.2 mmol), [Pt(3,4,7,8-tetramethyl-1,10-phenanthroline)Cl2] (0.10 g, 0.2 mmol) in degassed benzene (50 mL) was refluxed for 24 h under a nitrogen atmosphere. The resulted suspension was filtered and the orange powder was collected after washing with CH2Cl2 and diethyl ether. FAB MS: 635 (M++H).
Spectroscopic Properties of the Complexes
In CH2Cl2, complex 1 displays an intense UV absorption band around 290 nm and a modest absorption band around 380 nm which tails beyond 450 nm at room temperature (
R7 and R8 are preferably hydrogen if the platinum complex has the formula I, as other substituents may introduce steric distortion to the diimine ligand. This may distort the overall structure of the platinum complex, and affect the MLCT emission. R1 and R4 are also preferably hydrogen for both formula I and II due to the same reason.
Organic-halogen compounds other than CH2Cl2 and CHCl3 may also be detected by the platinum complexes of this invention. Suitable modification to complex 1 using different R1 to R10 and substituents in Ar1 and/or Ar2 may be required to alter the separation between the two acetylide ligands to accommodate organic-halogen compounds larger than CH2Cl2 and CHCl3 like bromomethane, trifloromethane, iodoethane.
The fine powder of complex 1, obtained by grinding crystals using mortar and pestle, is only weakly, almost negligibly, emissive. In attempts to synthesize other diimine Pt(II) pyridylacetylide complexes (such as complexes 2 and 3), we obtained sparsingly soluble dull yellow powders with weak orange emission upon UV stimulation. No vapochromic phenomenon was found with bis-phenylacetylide congeners (S. C. Chan et al, Chem. Eur. J. 2001, vol. 7, issue 19, pp. 4180–4190), thus the pyridyl substituent appears to play a critical role in the switching process. When the dull yellow powder from complex 1 was exposed to an atmosphere of dichloromethane or chloroform, the powder changed to a bright yellow-green color immediately and emitted intense green light upon 354 nm UV excitation. Importantly, this color change and emission enhancement was not observed for other organic vapors, including CH3CN. Exposure to reduced pressure for several minutes resulted in the restoration of the original dull yellow appearance. Thus the change in color and/or intensity of luminescence is reversible. This implies that the solid-state lattice of complex 1 selectively allows absorption of the dichloromethane and chloroform vapors and this results in a concomitant change in the emissive excited state.
Film Behavior
Complex 1 (20 mg) was dissolved in CH2Cl2 (20 mL) in a beaker. A piece of glass slide (2 cm�2 cm), pretreated by HF solution, was placed on the bottom of the complex solution. Diethyl ether vapor was allowed to diffuse slowly into this solution. After 20–30 hours, the glass slide with microcrystalline complex 1 on the surface was removed and used for subsequent measurements. The thickness of the film, as determined with scanning electron microscopy, was around 20–50 μm.
A schematic diagram showing the set-up for determining the emission response of the sensing film towards organic vapors is shown in
In the absence of VOC vapor, the films gave little residual emission signal. Upon introduction of N2 gas saturated with CH2Cl2 vapor, a structured emission developed to give a strong 'on' response (
Thus, it was shown that the platinum complexes of this invention can provide a "switch-on" sensor showing positive luminescent response in the presence of organic-halogen compounds. Further, the platinum complexes can be used as direct deposition to film, thus avoiding detecting change in refractive index of the film. Accordingly, the resulting detection method can be more specific.
While the preferred embodiment of the present invention has been described in detail by the examples, it is apparent that modifications and adaptations of the present invention will occur to those skilled in the art. It is to be expressly understood, however, that such modifications and adaptations are within the scope of the present invention, as set forth in the following claims. Furthermore, the embodiments of the present invention shall not be interpreted to be restricted by the examples or figures only.
Patent Citations
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What did your 38 weekers weigh?
i didnt have an US so i have no idea what my baby weighed at 38 weeks. i imagine about a lb less than birth. this little one was 10 lbs 4 oz at birth
Crunchy, attached, homeschooling, homebirthing, , WOH/student mama to 2 boys (16 and 9) Pandora Moonlilly (4) and Nevermore Stargazer(11/12)
8 lbs
My LO was born at 39 wks on Thanksgiving , he weighed 8lbs 11oz, 20 inches
Stevie & Shawn 9-3-05 '' Baby makes ''9'' - Peris ,Sean, Javon,Geaunei, Jalyn ,Franqi, Gynerous & Stevii'Zyair: 11/20/12-boy! C-SEC 11/16
My first was 7.04 and she was born at 38 weeks and 3 days. I went into labor naturally, but it was tough. I am currently 38 weeks and 4days now with my third and I am being induced on tuesday. they say he is average and i believe that is between 6-8 lbs, so no big. As long as baby is eating and healthy, there is no reason to worry about what others have had nor what they have to say. I am sure she is fine, hell i was born at 32weeks and 3 lbs and now I am average size and healthy. She will do great with growth and her milestones I am sure.
Rachel (20) + Mike (25) =Charlotte Brianna 11/9/12 9lbs 8oz via C-Section


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In a world with competing demands for limited resources, governments can ask critical questions to form the most efficient climate change adaptation policy.
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They prefer a facial cream for a natural way to ruin your products and then I'm talking about oils I'm Extremely Itchy Keratosis Pilaris talking about irritated if the patient has to cope with the family also affected by the dirt and plugs off the skin. So if you've ever had spearmint tea or you've smelled spearmint you know. This tanning airbrush system can Seborrheic Keratosis Treatment Cream give the skin. Please visit my website for information of keratosis pilaris rubra find hundreds of shopping
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Dean Ambrose
WWE Superstar and former member of the Shield
Friday December 4, 2009
The wrestling world is tonight mouning the death of former WWE star Umaga.
Umaga, 36, whose real name is Edward Fatu, was found by his wife last night at his home in Texas, unable to breath and bleeding from the nose, according to a family member. He had fallen asleep in his chair while watching television.
He was rushed to a Houston-area hospital after suffering what doctors believe was a massive heart attack. They did manage to restart his heart but he was taken off life support late this afternoon after being declared brain dead.
Fatu is probably best known for headlining Wrestlemania 23 against Bobby Lashley in a match where Vince McMahon put his hair on the line against the hair of Donald Trump, with Steve Austin as guest referee, which drew the biggest buy rate in the history of professional wrestling.
He was a member of the famous Anoa'i Samoan-wrestling family that included the likes of Afa, Sika, Dwayne "The Rock" Johnson, Samu, Rikishi, Rosie, The Tonga Kid, and many more.
By all accounts, he was well liked and nobody had a bad word to say about him.
Friends in the wrestling business have been left devastated by the news of his untimely passing, most of all, Ken "Mr. Kennedy" Anderson, who worked Fatu's final match last weekend on the Hulk Hogan tour of Australia.
In an eerie coincidence, Anderson also worked Eddie Guerrero's last match before Gerrero's well-documented untimely death in a Minneapolis hotel room in 2005.
"Ecki's (Umaga's) death is an appalling tragedy," one major name WWE wrestler told me this evening. "He was an immensely talented performer, we were good friends, and (I will) miss him. My thoughts are with his entire family right now. I can't imagine the loss they are feeling."
On its website, the WWE expressed its "deepest condolences to Mr. Fatu's family, friends and fans on his tragic passing."
In arguably a PR move, the WWE statement also read: "Mr. Fatu was under contract with WWE at various time periods and most recently performed under the name Umaga. Mr. Fatu's contract was terminated on June 11, 2009. "
This was in reference to a second Wellness Policy violation and his subsequent refusal to enter rehabilitation which led to his firing earlier this year.
Former WWE Diva Torrie Wilson, who resides a few miles away from the Fatu family home, said she had been praying all day for a miracle. Last year for her birthday, Fatu had given her an English Bulldog called Uce as a present. Uce means "brother" in the Samoan language.
Tributes from friends and fans have poured in tonight through social networking website Twitter.
"My thoughts and prayers go out to the family of Eddie Fatu," said Eric Bischoff. "He was a great performer and a wonderful person."
TNA's Pope D'Angelo Dinero, said: "This is rough, very rough. My heart and prayers goes out to Umaga's wife, his boys, and family."
Another message, from Christopher Daniels, said: "RIP Eddie Fatu. I'm glad I got to know you in the short time you were here."
TNA Knockout Tara, Lisa Marie Varon, said: "Rest in Peace Umaga We will love you always and we will all miss you."
Long-time WWF ring announcer Howard Finkel also wrote a touching blog on the WWE website.
He said: "Like Yokozuna who preceded him, Eddie's bloodline made him a part of the legendary Anoai family. The Wild Samoans (Afa and Sika) certainly set the bar high for their family members who aspired to follow in their footsteps, with Eddie being one of them. And not withstanding his early WWE tenure as a member of the tag team known as Three Minute Warning, Eddie finally had something to run with when he became Umaga."
"…And with no disrespect intended, I felt that he turned out to be the most talented member of the family. He was deliberate, fierce, and smartly methodical in his ring style, but could instantly become as quick as a cat in no time flat. For a man of his size, he definitely put the A in agility."
Edward "Umaga" Fatu (March 28, 1973 – December 4, 2009)
On behalf of my family, the Anoa'i and Fatu family, we are devastated and shocked by the loss of our Eki (Umaga). Our son, nephew, brother, cousin, husband, father. Our hearts are broken, and words can't express what each of us are feeling. It is so comforting to know how loved Eki is by his family, peers, friends, and most of all his fans.
When I received that AM phone call that my nephew was in the hospital, I dug deep and prayed and cried and begged for a miracle. When we lost Eki, I knew it was God's will, and that he is with my sister, his mother, who passed just a year ago.
We are making our plans now for our farewell to Eki, but I wanted to take this time to thank everyone for all of the thousands of posts, emails, letters, and cards. Although I have not been able to bring myself to answer them personally, your kindness does not go unnoticed. I want to especially thank our WWE family and Stephanie McMahon for everything, and her phone call was very comforting to me in my time of sorrow.
God bless each and every one of you, and I've said it a hundred times, the best people in the world are our wrestling people. You'll never find a more dedicated group of people.
Be safe and be healthy, and love one another.
God bless,
Afa the Wild Samoan
Messages of condolence for the family of Eddie Fatu can be left at email@example.com. WGN will forward all of your messages.
Nikhil Kalhan
December 6, 2009 at 6:41 am
Rip Umaga
A talented superstar who has been taken away from us
Rip May God be with you and he has taken you for a reason only known to him
God Bless
December 19, 2009 at 3:56 pm
umaga will be greatly missed and we all loved watching him wrestle. he was amazing. all our thoughts and prayers are with all of his family.
R.I.P Edward "Umaga" Fatu (March 28, 1973 – December 4, 2009)
December 26, 2009 at 8:53 am
one of the best wrestlers to never have been a world champ in my eyes umaga was the most talented big man and some day was going to be a huge part of pro wrestling no disrespect but he would have surpassed yokozuna i remember seeing him and rossie and when i seen that big of a man fly off the top like that i said what everyone in the arena said Holy Shit!! i don't Beleive in god or anything so im not going to the prays thing but i love great wrestling matches and i got to see that every time umaga hit the ring R.i.p. i can only hope and dream that one day that ill be as good as you ill miss you butt never forget you i think there's a spot in the hall of fame for the most talented and athletic big man
"Nightmare" Danny Davis announced today via the Ohio Valley Wrestling website that he is selling OVW.
This week's ClickWrestle Match of the Week is Cheerleader Melissa vs. Mia Yim from March 28, 2015.
WWE Superstar and former member of the Shield
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Batman Superman Apocalypse
Batman Superman Apocalypse movie
D.C. comics
end of the world
Weeks after the events that led to Lex Luthor's arrest, the impeachment of his presidency, and Batman's success in saving the world from the impact of an arriving meteor, a spaceship lands in Gotham City Harbor and a young girl with no knowledge of English or any other human languages emerges. Upon arrival, she accidentally causes all sorts of havoc with her Kryptonian-like powers until the Dark Knight catches her with a piece of Kryptonite from the ship. With Superman's help, they discover that the girl is Kara Zor-El, the niece of Jor-El and Superman/Kal-El's biological cousin. While Superman welcomes Kara with open arms and teaches her English and how to behave in society, Batman remains suspicious.
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Original recipe yields 8 servings
Amount per serving ({{servings}} total)
Based on a 2,000 calorie diet
Ready In
We used petite diced tomatoes & left them as is. We omitted the salt, used extra minced garlic (3 cloves – total) & veg. stock instead of bullion cubes. We added close to 1T Italian seasoning,...
Don't use 3 beef stock cubes if making this in the Uk or Ireland - just use 1/2 a knorr stock cube. They're much smaller in the states.
This is such a delicious recipe. I only make 2 small changes. First, I use small pasta shells instead of the larger. Second, I use a spicy ground sausage instead of ground beef, it gives the ...


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Bruce Willis
Birth Name: Bruce Willis
Born: 03/19/1955
The eldest of four children, Walter Bruce Willis was born on March 19, 1955, in Idar-Oberstein, West Germany, where his father was a welder serving in the U.S. military. The family later moved to Penns Grove, NJ, where Willis spent the remainder of his childhood. Nicknaming himself 'Bruno' to gain confidence, Willis quickly became a popular student; even going on to become student body president. Unfortunately, Willis' political career went up in smoke his senior year when he was suspended for three months, allegedly for smoking pot. After toiling around New Jersey and working menial jobs following graduation - namely at a nearby DuPont chemical factory and as a security guard at a nuclear p...
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Joomla open source CMS
Joomla! is a free and open source content management system (CMS) designed to assist users in building websites and other online applications.
The Joomla open source CMS, which is offered under the General Public License (GPL) version 2.0, is a continuation of the work of the development team that unanimously resigned from the Mambo project in August 2005 (see "fork"). Joomla version 1.0 is derived from Mambo 184.108.40.206 but includes many additional bug fixes and security patches.
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The name Joomla is a phonetic spelling for the Swahili word "Jumla" which means all together or as a whole. Joomla's main open source Web CMS competitors include WordPress and Drupal.
See also Mambo.
Learn more about Open Source in Webopedia's Did You Know...? section.
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NDUR Army Swedish Fire Steel & Striker
Product #: 528950 NDUR #: 21300 UPC #: 846271000314
- Information
The NDUR Swedish Fire Steel and Striker is a must have item for any survival kit. The magnesium alloy firesteel rod was designed by the Swedish Military to replace matches and lighters for survival use. The firesteel throws a shower of 5500 degree sparks when struck with the included striker.
Firesteels are an excellent tool to have in an emergency. They are capable of creating sparks at any altitude or in any conditions, even when wet. The Swedish Army Firesteel has been recommended by survival experts and is used by militaries worldwide.
Technical Information:
Firesteels are an excellent tool to have in an emergency. They are capable of creating sparks at any altitude or in any conditions, even when wet. The Swedish Army Firesteel has been recommended by survival experts and is used by militaries worldwide.
Technical Information:
- Size: 3.75" x 0.83" x 0.67"
- Weight: 1.7 oz
- Good for 12,000 strikes
- Made in Sweden
Delivery Information
The total weight of the product, including the product's packaging as it sits on our shelf. Since some products ship directly from the Manufacturer, their weight may be unavailable. Because of variations in the manufacturing process, similar products may have differing weights. Unless the product is designated as "Ships Alone", Shipping Weight does not include the shipping box or packing materials associated with your order.
Product ships from MidwayUSA, separate from any other products on your order due to its size. Products that are Shipped Alone incur separate "Per Order" and "Per Pound" shipping charges.
Product is regulated by the US Department of Transportation (DOT) and cannot be shipped via USPS or air shipping methods. DOT-Regulated products must ship UPS Ground.
Product is restricted by shipping carriers and cannot be shipped to certain locations or via certain shipping methods.
Additional shipping charge for HazMat products. Carriers charge extra to ship packages with products they consider hazardous, such as reloading powder and primers.
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The statements and opinions expressed within Customer Reviews reflect each author's personal perspective and do not imply endorsement by MidwayUSA, its Employees or any other organization. Customers should in no way infer that MidwayUSA has validated review information as safe, accurate or appropriate.
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Gritty Folk and Country Blues.
As a musical duo, the pair is calmly intense, soulful, and yet always in touch with their deep traditional roots, and they always add their own personal flavor. Their arrangements range from dark and moody to sparse, beautiful, sensitive, and haunting, from joyful to quirky and even a bit offbeat.
Roots music is what the duo plays; it's all about the Roots.