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The invention relates to thermoplastic molding materials containing the following main components: A) 2 to 97.9 wt. % of at least one polyester; B) 0 to 95.9 wt. % of at least one polycarbonate; C) 1 to 80 wt. % of at least one graft polymer which is made up of c1) 40 to 80 wt. % of a graft base consisting of a rubber elastic polymer based on alkyl acrylates with 1 to 8 C-atoms in the alkyl radical and with a glass transition temperature of less than 10° C., c2) 20 to 60 wt. % of a graft support consisting of c21) 60 to 95 wt. % styrene or substituted styrenes of general formula (I), wherein R represents an alkyl radical with 1 to 8 C-atoms or a hydrogen atoms and R1 represents an alcohol radical with 1 to 8 C-atoms and the value of n is 1, 2 or 3 and c22) 5 to 40 wt. % of at least one unsaturated nitrile; D) 1 to 80 wt. % of a copolymer consisting of d1) 60 to 95 % styrene or substituted styrenes of general formula (I) or mixtures thereof and d2) 5 to 40 wt. % of at least one unsaturated nitrile; E) 0.1 to 10 wt. % of an epoxyde resin; and F) 0 to 80 wt. % other additives, the sum of the weight percentages of components A) to F) being 100%.
1. A thermoplastic molding composition comprising, as substantial components,
A) from 2 to 97.9% by weight of at least one polyester,
B) from 0 to 95.9% by weight of at least one polycarbonate,
C) from 1 to 80% by weight of at least one graft polymer built, up from
c1) from 40 to 80% by weight of a graft base made from an elastomeric polymer based on alkyl acrylates having from 1 to 8 carbon atoms in the alkyl radical and with a glass transition temperature below 10° C.,
c2) from 20 to 60% by weight of a graft made from,
where R is alkyl having from 1 to 8 carbon atoms or hydrogen and R1 is alkyl having from 1 to 8 carbon atoms and n is 1, 2 or 3, and
c22) from 5 to 40% by weight of at least one unsaturated nitrile,
D) from 1 to 80% by weight of a rubber-free copolymer consisting essentially of,
d1) from 60 to 95% by weight of styrene or of substituted styrenes of the formula I or mixtures of these, and
d2) from 5 to 40% by weight of at least one unsaturated nitrile,
E) from 0.1 to 10% by weight of an epoxy resin, and
F) from 0 to 80% by weight of other additives, where the total of the percentages by weight of components A) to
F) is 100%.
2. A thermoplastic molding composition as claimed in
4. A thermoplastic molding composition as claimed in
5. A molding, film or fiber obtainable from the molding compositions as claimed in
6. The molding composition defined in
7. A thermoplastic molding composition as claimed in
8. The molding composition defined in
9. A thermoplastic molding composition as claimed in
10. The molding composition defined in
The invention relates to thermoplastic molding compositions comprising, as substantial components,
The invention further relates to the use of the novel molding compositions for producing moldings of any type, and to the resultant moldings.
Industry is increasingly interested in polymer mixtures, since they can provide tailored combinations of properties. Of particular interest here are polymer mixtures made from incompatible polymers which have unusual combinations of properties.
Polymer mixtures based on polyesters and on polycarbonates have been known for some years (U.S. Pat. Nos. 4,522,797, 4,764,556, 4,897,448, EP-A 180 648, DE-A 3302124). The industrially important products also comprise impact modifiers to improve toughness, in particular at low temperatures, and those preferably used are MBS modifiers, acrylate graft rubbers and ethylene copolymers with polar comonomers.
Blends based on polyesters and on styrene copolymers are likewise known (DE-A 3403 576, EP-A 310 976, EP-A 310 977, EP-A 310 978). DE-A 3733 839 moreover discloses mixtures made from polyesters and from at least two rubbers of different particle size, featuring good toughness.
For many applications there is still a requirement for polymer mixtures based on polyesters and on polycarbonate or, respectively, on styrene copolymers, having good toughness, high dimensional stability and good stability in long-term service.
It is an object of the present invention to provide polyester molding compositions which have improved mechanical properties (in particular toughness) and stability and long-term service.
We have found that this object is achieved by the molding compositions defined at the outset. Preferred embodiments are given in the subclaims.
Surprisingly, it has now been found that the thermoplastic molding compositions mentioned at the outset, which comprise epoxy resins as a substantial constituent, have a property profile which is improved over the prior art in relation to toughness and stability in long-term service.
The novel molding compositions comprise, as component (A), from 2 to 97.9% by weight, preferably from 5 to 90.8% by weight and in particular from 10 to 81.5% by weight, of a thermoplastic polyester.
Use is generally made of polyesters A) based on aromatic dicarboxylic acids and on an aliphatic or aromatic dihydroxy compound.
A first group of preferred polyesters is that of polyalkylene terephthalates having from 2 to 10 carbon atoms in the alcohol moiety.
Polyalkylene terephthalates of this type are known per se and are described in the literature. Their main chain contains an aromatic ring which derives from the aromatic dicarboxylic acid. There may also be substitution of the aromatic ring, e.g. by halogen, such as chlorine or bromine, or by C1-C4-alkyl, such as methyl, ethyl, iso- or n-propyl, or n-, iso- or tert-butyl.
These polyalkylene terephthalates may be prepared by reacting aromatic dicarboxylic acids, or their esters or other ester-forming derivatives, with aliphatic dihydroxy compounds in a manner known per se.
Preferred dicarboxylic acids are 2,6-naphthalenedicarboxylic acid, terephthalic acid and isophthalic acid, and mixtures of these. Up to 30 mol %, preferably not more than 10 mol %, of the aromatic dicarboxylic acids may be replaced by aliphatic or cycloaliphatic dicarboxylic acids, such as adipic acid, azelaic acid, sebacic acid, dodecanedioic acids and cyclohexanedicarboxylic acids.
Preferred aliphatic dihydroxy compounds are diols having from 2 to 6 carbon atoms, in particular 1,2-ethanediol, 1,3-propanediol, 1,4-butanediol, 1,6-hexanediol, 1,4-hexanediol, 1,4-cyclohexanediol, 1,4-cyclohexanedimethanol and neopentyl glycol, and mixtures of these.
Particularly preferred polyesters (A) are polyalkylene terephthalates derived from alkanediols having from 2 to 6 carbon atoms. Among these, particular preference is given to polyethylene terephthalate, polypropylene terephthalate and polybutylene terephthalate, and mixtures of these. Preference is also given to PET and/or PBT which comprise, as other monomer units, up to 1% by weight, preferably up to 0.75% by weight, of 1,6-hexanediol and/or 2-methyl-1,5-pentanediol.
The viscosity number of the polyesters (A) is generally in the range from 50 to 220, preferably from 80 to 160 (measured in a 0.5% strength by weight solution in a phenol/o-dichlorobenzene mixture in a weight ratio of 1:1 at 25° C. in accordance with ISO 1628.
Particular preference is given to polyesters whose carboxyl end group content is up to 100 mval/kg, preferably up to 50 mval/kg and in particular up to 40 mval/kg of polyester. Polyesters of this type may be prepared, for example, by the process of DE-A 44 01 055. The carboxyl end group content is usually determined by titration methods (e.g. potentiometry).
Particularly preferred molding compositions comprise, as component A), a mixture of polyesters which are different from PBT, for example polyethylene terephthalate (PET). The proportion e.g. of the polyethylene terephthalate in the mixture is preferably up to 50% by weight, in particular from 10 to 30% by weight, based on 100% by weight of A).
It is also advantageous to use recycled PET materials (also termed scrap PET), if desired in a mixture with polyalkylene terephthalates, such as PBT.
Recycled materials are generally:
Both types of recycled material may be used either as ground material or in the form of pellets. In the latter case, the crude recycled materials are isolated and purified and then melted and pelletized using an extruder. This usually facilitates handling and free flow, and metering for further steps in processing.
The recycled materials used may either be pelletized or in the form of regrind. The edge length should not be more than 6 mm, preferably less than 5 mm.
Because polyesters undergo hydrolytic cleavage during processing (due to traces of moisture) it is advisable to predry the recycled material. The residual moisture after drying is preferably from 0.01 to 0.7%, in particular from 0.2 to 0.6%.
Another group to be mentioned is that of fully aromatic polyesters deriving from aromatic dicarboxylic acids and aromatic dihydroxy compounds.
Suitable aromatic dicarboxylic acids are the compounds previously mentioned for the polyalkylene terephthalates. The mixtures preferably used are made from 5 to 100 mol % of isophthalic acid and from 0 to 95 mol % of terephthalic acid, in particular from about 50 to about 80% of terephthalic acid and from 20 to about 50% of isophthalic acid.
The aromatic dihydroxy compounds preferably have the formula
Examples of parent substances for these compounds are
Among these, preference is given to
It is, of course, also possible to use mixtures of polyalkylene terephthalates and fully aromatic polyesters. These generally comprise from 20 to 98% by weight of the polyalkylene terephthalate and from 2 to 80% by weight of the fully aromatic polyester.
It is, of course, also possible to use polyester block copolymers, such as copolyetheresters. Products of this type are known per se and are described in the literature, e.g. in U.S. Pat. No. 3,651,014. Corresponding products are also available commercially, e.g. Hytrel® (DuPont).
According to the invention, the molding compositions may comprise, as component B), from 0 to 95.9% by weight, preferably from 5 to 90.8% by weight and in particular from 10 to 81.5% by eight, of at least one polycarbonate.
Halogen-free polycarbonates are preferably used as component B). Examples of suitable halogen-free polycarbonates are those based on biphenols of the formula
The phenylene radicals of the biphenols may also have substituents, such as C1-C6-alkyl or C1-C6-alkoxy.
Examples of preferred biphenols of this formula are hydroquinone, resorcinol, 4,4′-dihydroxybiphenyl, 2,2-bis(4-hydroxyphenyl)propane, 2,4-bis(4-hydroxyphenyl)-2-methylbutane and 1,1-bis(4-hydroxyphenyl)cyclohexane. Particular preference is given to 2,2-bis(4-hydroxyphenyl)propane and 1,1-bis(4-hydroxyphenyl)cyclohexane, and also to 1,1-bis(4-hydroxyphenyl)-3,3,5-trimethylcyclohexane.
Either homopolycarbonates or copolycarbonates are suitable as component B, and preference is given to the copolycarbonates of bisphenol A, as well as to bisphenol A homopolymer.
Suitable polycarbonates may be branched in a known manner, specifically and preferably by incorporating from 0.05 to 2.0 mol %, based on the total of the biphenols used, of at least trifunctional compounds, for example those having three or more phenolic OH groups.
Polycarbonates which have proven particularly suitable have relative viscosities ηrel of from 1.10 to 1.50, in particular from 1.25 to 1.40. This corresponds to an average molar mass Mw (weight-average) of from 10,000 to 200,000 g/mol, preferably from 20,000 to 80,000 g/mol.
The biphenols of this formula are known per se or can be prepared by known processes.
The polycarbonates may, for example, be prepared by reacting the biphenols with phosgene in the interfacial process, or with phosgene in the homogeneous-phase process (known as the pyridine process), and in each case the desired molecular weight is achieved in a known manner by using an appropriate amount of known chain terminators. (In relation to polydiorganosiloxane-containing polycarbonates see, for example, DE-A 33 34 782).
Examples of suitable chain terminators are phenol, p-tert-butylphenol, or else long-chain alkylphenols, such as 4-(1,3-tetramethylbutyl)phenol as in DE-A 28 42 005, or monoalkylphenols, or dialkylphenols with a total of from 8 to 20 carbon atoms in the alkyl substituents as in DE-A 35 06 472, such as p-nonylphenyl, 3,5-di-tert-butylphenol, p-tert-octylphenol, p-dodecylphenol, 2-(3,5-dimethylheptyl)phenol and 4-(3,5-dimethylheptyl)phenol.
For the purposes of the present invention, halogen-free polycarbonates are polycarbonates made from halogen-free biphenols, from halogen-free chain terminators and, if desired, from halogen-free branching agents, where the content of subordinate amounts of hydrolyzable chlorine at the ppm level, resulting, for example, from the preparation of the polycarbonates with phosgene in the interfacial process, is not regarded as meriting the term halogen-containing for the purposes of the invention. Polycarbonates of this type with contents of hydrolyzable chlorine at the ppm level are halogen-free polycarbonates for the purposes of the present invention.
Other suitable components B) which may be mentioned are amorphous polyester carbonates, where phosgene has been replaced by aromatic dicarboxylic acid units, such as isophthalic acid and/or terephthalic acid units, during the preparation. For further details reference may be made at this point to EP-A 711,810.
EP-A 365 916 describes other suitable copolycarbonates having cycloalkyl monomer units.
It is also possible to replace bisphenol A with bisphenol TMC. Polycarbonates of this type are commercially available from Bayer with the trademark APEC HT®.
The novel molding compositions use, as component C), from 1 to 80% by weight, based on the total of components A to F, of a graft copolymer or of a mixture of different graft copolymers. Preferred novel molding compositions comprise from 2 to 60% by weight, particularly preferably from 5 to 50% by weight, of at least one graft copolymer C) which differs from elastomeric polymers F).
The graft polymers C) have been built up from
Possible polymers for the graft base c1 are those whose glass transition temperature is below 10° C., preferably below 0° C., particularly preferably below −20° C. Examples of these are elastomers based on C1-C8-alkyl acrylates, which may, if desired, contain other comonomers.
Preference is given to graft bases c1 which have been built up from
This type of graft base is known per se and is described in the literature, for example in DE-A 31 49 358.
Preferred grafts C2 are those in which c21 is styrene or α-methylstyrene or a mixture of these and in which C22 is acrylonitrile or methacrylonitrile. Especially preferred monomer mixtures are styrene and acrylonitrile or α-methylstyrene and acrylonitrile. The grafts are obtainable by compolymerizing components c21 and C22.
The graft base c1 of the graft polymers C) is also termed an ASA rubber and has been built up from components c11, c12 if desired and c13. Its preparation is known per se and is described in DE-A 28 26 925, DE-A 31 49 35B and DE-A 3414 118, by way of example.
The graft polymers C) may, for example, be prepared by the method described in DE-C 12 60 135.
The graft (graft envelope) of the graft polymers may be built up in one or two stages.
If the graft envelope is built up in one stage, a mixture of the monomers C21 and C22 in the desired ratio by weight of from 95:5 to 50:50, preferably from 90:10 to 65:35, is polymerized, preferably in emulsion, in the presence of the elastomer c1, in a manner known per se (cf., for example, DE-A 28 26 925).
If the graft envelope c2 is built up in two stages, the first stage generally makes up from 20 to 70% by weight, preferably from 25 to 50% by weight, based on C2. It is preferably prepared using only styrene or substituted styrenes or mixtures of these (C21).
The second stage of the graft envelope generally makes up from 30 to 80% by weight, in particular from 50 to 75% by weight, based in each case on c2. This preparation utilizes mixtures made from the monomers c21 and from the nitrites c22 generally in a weight ratio C21/C22 of from 90:10 to 60:40, in particular from 80:20 to 70:30.
The conditions for the graft polymerization are preferably selected to give particle sizes of from 50 to 700 nm (d50 of the integral mass distribution). Measures to this end are known and are described in DE-A 2826925, for example.
A coarse-particle rubber dispersion may be prepared directly via the seed-latex process.
To obtain very tough products it is frequently advantageous to use a mixture of at least two graft polymers with different particle sizes.
To achieve this, the particles of the rubber are enlarged in a known manner, e.g. by agglomeration, so that the latex has a bimodal structure (from 50 to 180 nm and from 200 to 700 nm).
The preferred embodiment uses a mixture made from two graft polymers with particle diameters (d50 of the integral mass distribution) of from 50 to 180 nm and, respectively, from 200 to 700 nm in a weight ratio of from 70:30 to 30:70.
The chemical structure of the two graft polymers is preferably the same, but the envelope of the coarse-particle graft polymer may in particular have a two-stage structure.
Mixtures made from component A and C, where the latter has a coarse-particle and a fine-particle graft polymer, are described in DE-A 36 15 607, for example. Mixtures made from components A and C, where the latter has a two-stage graft envelope, are known from EP-A 111 260.
The novel molding compositions comprise, as component D, from 1 to 80% by weight, based on the total of components A to F, of at least one copolymer based on styrene or on substituted styrenes and on unsaturated nitrites. Preferred novel molding compositions comprise, based on the total of components A to F, from 2 to 60% by weight, in particular from 3 to 50% by weight, of component D.
According to the invention, copolymers D have been built up from
The copolymers D are resin-like, thermoplastic and rubber-free. Particularly preferred copolymers D are those made from styrene or acrylonitrile, from α-methylstyrene and acrylonitrile or from styrene, α-methylstyrene and acrylonitrile. It is also possible for two or more of the copolymers described to be used simultaneously.
The copolymers D are known per se and may be prepared by free-radical polymerization, in particular by emulsion, suspension, solution or bulk polymerization. They have viscosity numbers of from 40 to 160, corresponding to average molecular weights Mw (weight average) of from 40,000 to 2,000,000.
The novel molding compositions comprise, as component E, from 0.01 to 10% by weight, preferably from 0.2 to 5% by weight and in particular from 0.5 to 3% by weight, of an epoxy resin. B. Ellis, Chemistry and Technology of Epoxy-Resins, Blackie Academic & Professional, 1993, describes the structure and preparation of epoxy resins, and any of these are in principle suitable.
Preferred epoxy resins have the formula II and are usually obtainable by condensing 2,2-bis(p-hydroxyphenylpropane)(bisphenol A) and epichlorohydrin:
Epoxy resins usually have an epoxy number to ISO 3001 of from 1.5 to 1.9, preferably from 1.68 to 1.75. The softening point to DIN 51920 is preferably from 75 to 100° C., preferably from 82 to 90° C. The melt viscosity to DIN 53018 Part 1 at 175° C. is preferably from 250 to 600 mPas, in particular from 350 to 480 mPas.
Other preferred epoxy resins have the formula III
Preferred R2 are propyl and butyl.
Other suitable expoxy resins have the formula IV
Cycloaliphatic epoxy resins (formula V) are also suitable:
It is, of course, also possible to use mixtures, and the mixing ratio may be as desired.
The novel molding compositions comprise, as component F), from 0 to 80% by weight, in particular up to 50% by weight, of other additives.
The novel molding compositions may comprise, as component F), from 0 to 5%, in particular from 0.01 to 5% by weight, preferably from 0.05 to 3% by weight and particularly from 0.1 to 2% by weight, of at least one ester or amide of saturated or unsaturated aliphatic carboxylic acids having from 10 to 40 carbon atoms, preferably from 16 to 22 carbon atoms, with saturated aliphatic alcohols or amines having from 2 to 40 carbon atoms, preferably from 2 to 6 carbon atoms.
The carboxylic acids may be mono- or dibasic. Examples are pelargonic acid, palmitic acid, lauric acid, margaric acid, dodecanedioc acid, behenic acid and, particularly preferably, stearic acid, capric acid and montanic acid (a mixture of fatty acids having from 30 to 40 carbon atoms).
The aliphatic alcohols may be mono- to tetrahydric. Examples of alcohols are n-butanol, n-octanol, stearyl alcohol, ethylene glycol, propylene glycol, neopentyl glycol and pentaerythritol. Glycerol and pentaerythritol are preferred.
The aliphatic amines may be mono- to tribasic. Examples of these are stearylamine, ethylenediamine, propylenediamine, hexamethylenediamine and di(6-aminohexyl) amine. Ethylenediamine and hexamethylenediamine are particularly preferred. Correspondingly, preferred esters or amides are glycerol distearate, glycerol tristearate, ethylenediamine distearate, glycerol monopalmitate, glycerol trilaurate, glycerol monobehenate and pentaerythritol tetrastearate.
It is also possible to use mixtures of different esters or amides or combinations of esters with amides. The mixing ratio may be as desired.
Examples of other additives F) are up to 40% by weight, preferably up to 30% by weight, of elastomeric polymers (also frequently termed impact modifiers, elastomers or rubbers) which differ from C).
These are very generally copolymers preferably built up from at least two of the following monomers: ethylene, propylene, butadiene, isobutene, isoprene, chloroprene, vinyl acetate, styrene, acrylonitrile and (meth)acrylates having from 1 to 18 carbon atoms in the alcohol component.
Polymers of this type have been described, for example, in Houben-Weyl, Methoden der organischen Chemie, Vol. 14/1 (Georg-Thieme-Verlag, Stuttgart, 1961), pages 392-406, and in the monograph by C. B. Bucknall, "Toughened Plastics" (Applied Science Publishers, London, 1977).
Some preferred types of such elastomers are described below.
Preferred types of such elastomers are those known as ethylene-propylene (EPM) and ethylene-propylene-diene (EPDM) rubbers.
EPM rubbers generally have practically no residual double bonds, whereas EPDM rubbers may have from 1 to 20 double bonds per 100 carbon atoms.
Examples which may be mentioned of diene monomers for EPDM rubbers are conjugated dienes, such as isoprene and butadiene, non-conjugated dienes having from 5 to 25 carbon atoms, such as 1,4-pentadiene, 1,4-hexadiene, 1,5-hexadiene, 2,5-dimethyl-1,5-hexadiene and 1,4-octadiene, cyclic dienes, such as cyclopentadiene, cyclohexadienes, cyclooctadienes and dicyclopentadiene, and also alkenylnorbornenes, such as 5-ethylidene-2-norbornene, 5-butylidene-2-norbornene, 2-methallyl-5-norbornene and 2-isopropenyl-5-norbornene, and tricyclodienes, such as 3-methyltricyclo[5.2.1.02,6]-3,8-decadiene, or mixtures of these. Preference is given to 1,5-hexadiene, 5-ethylidenenorbornene and dicyclopentadiene. The diene content of the EPDM rubbers is preferably from 0.5 to 50% by weight, in particular from 1 to 8% by weight, based on the total weight of the rubber.
EPM and EPDM rubbers may preferably also have been grafted with reactive carboxylic acids or with derivatives of these. Examples of these are acrylic acid, methacrylic acid and derivatives thereof, e.g. glycidyl (meth)acrylate, and also maleic anhydride.
Copolymers of ethylene with acrylic acid and/or methacrylic acid and/or with the esters of these acids are another group of preferred rubbers. The rubbers may also include dicarboxylic acids, such as maleic acid and fumaric acid, or derivatives of these acids, e.g. esters and anhydrides, and/or monomers containing epoxy groups. These monomers containing dicarboxylic acid derivatives or containing epoxy groups are preferably incorporated into the rubber by adding to the monomer mixture monomers containing dicarboxylic acid groups and/or epoxy groups and having the formula I, II, III or IV
where R1 to R9 are hydrogen or alkyl having from 1 to 6 carbon atoms, and m is an integer from 0 to 20, g is an integer from 0 to 10 and p is an integer from 0 to 5.
R1 to R9 are preferably hydrogen, where m is 0 or 1 and g is 1. The corresponding compounds are maleic acid, fumaric acid, maleic anhydride, allyl glycidyl ether and vinyl glycidyl ether.
Preferred compounds of the formulae I, II and IV are maleic acid, maleic anhydride and (meth)acrylates containing epoxy groups, such as glycidyl acrylate and glycidyl methacrylate, and the esters with tertiary alcohols, such as tert-butyl acrylate.
Although the latter have no free carboxyl groups their behavior approximates to that of the free acids and they are therefore termed monomers with latent carboxyl groups.
The copolymers are advantageously composed of from 50 to 98% by weight of ethylene, from 0.1 to 20% by weight of monomers containing epoxy groups and/or methacrylic acid and/or monomers containing anhydride groups, the remaining amount being (meth)acrylates.
Particular preference is given to copolymers composed of
Other preferred (meth)acrylates are the methyl, ethyl, propyl, isobutyl and tert-butyl esters.
Besides these, comonomers which may be used are vinyl esters and vinyl ethers.
The ethylene copolymers described above may be prepared by processes known per se, preferably by random copolymerization at high pressure and elevated temperature. Appropriate processes are well known.
It is, of course, also possible to use mixtures of the types of rubber listed above.
Examples of fibrous or particulate fillers are carbon fibers, glass fibers, glass beads, amorphous silica, asbestos, calcium silicate, calcium metasilicate, magnesium carbonate, kaolin, chalk, powdered quartz, mica, barium sulfate and feldspar, used in amounts of up to 50% by weight, and in particular from 1 to 40% by weight, particularly from 20 to 35% by weight.
Preferred fibrous fillers are carbon fibers, aramid fibers and potassium titanate fibers, and particular preference is given to glass fibers in the form of E glass. These may be used as rovings or chopped glass in the commercially available forms.
The fibrous fillers may have been surface-pretreated with a silane compound to improve compatibility with the thermoplastic.
Suitable silane compounds have the formula
Preferred silane compounds are aminopropyltrimethoxysilane, aminobutyltrimethoxysilane, aminopropyltriethoxysilane and aminobutyltriethoxysilane, and also the corresponding silanes which contain a glycidyl group as substituent X.
The amounts of the silane compounds generally used for surface-coating are from 0.05 to 5% by weight, preferably from 0.5 to 1.5% by weight and in particular from 0.8 to 1% by weight (based on F).
Acicular mineral fillers are also suitable.
For the purposes of the invention, acicular mineral fillers are mineral fillers with strongly developed acicular character. An example which may be mentioned is acicular wollastonite. The mineral preferably has an L/D (length to diameter) ratio of from 8:1 to 35:1, preferably from 8:1 to 11:1. The mineral filler may, if desired, have been pretreated with the abovementioned silane compounds, but the pretreatment is not essential.
Other fillers which may be mentioned are kaolin, calcined kaolin, wollastonite, talc and chalk.
The novel thermoplastic molding compositions may comprise, as component F), conventional processing aids, such as stabilizers, oxidation retarders, agents to counter thermal decomposition and decomposition by ultraviolet light, lubricants, mold-release agents, colorants, such as dyes and pigments, flame retardants, nucleating agents, plasticizers, etc.
UV stabilizers which should be mentioned and are usually used in amounts of up to 2% by weight, based on the molding composition, are various substituted resorcinols, salicylates, benzotriazoles and benzophenones.
Colorants which may be added are inorganic pigments, such as ultramarine blue, iron oxide and carbon black, and also organic pigments, such as phthalocyanines, quinacridones and perylenes, and also dyes, such as nigrosine and anthraquinones.
Nucleating agents which may be used are sodium phenylphosphinate, aluminum oxide, silicon dioxide and also preferably talc.
Other lubricants and mold-release agents, of which up to 1% by weight is usually used, are preferably long-chain fatty acids (e.g. stearic acid or behenic acid), salts of these (e.g. Ca stearate or Zn stearate) or montan waxes (mixtures of straight-chain saturated carboxylic acids with chain lengths of from 28 to 32 carbon atoms), or also low-molecular-weight polyethylene waxes or low-molecular-weight polypropylene waxes.
Examples of plasticizers which should be mentioned are dioctyl phthalates, dibenzyl phthalates, butyl benzyl phthalates, hydrocarbon oils and N-(n-butyl)benzenesulfonamide.
The novel molding compositions may also comprise from 0 to 2% by weight of fluorine-containing ethylene polymers. These are polymers of ethylene with a fluorine content of from 55 to 76% by weight, preferably from 70 to 76% by weight.
Examples of these are polytetrafluoroethylene (PTFE), tetrafluoroethylene-hexafluoropropylene copolymers and tetrafluoroethylene copolymers with relatively small proportions (generally up to 50% by weight) of copolymerizable ethylenically unsaturated monomers. These are described, for example, by Schildknecht in "Vinyl and Related Polymers", Wiley, 1952, pp. 484 to 494 and by Wall in "Fluoropolymers" (Wiley Interscience, 1972).
These fluorine-containing ethylene polymers have homogeneous distribution in the molding compositions and preferably have a particle size d50 (number average) in the range from 0.05 to 10 μm, in particular from 0.1 to 5 μm. These small particle sizes may particularly preferably be achieved by using aqueous dispersions of fluorine-containing ethylene polymers and incorporating these into a polyester melt.
Another preferred group of lubricants is that of ethylene oxide-propylene oxide copolymers.
The ethylene oxide-propylene oxide copolymers are generally prepared by ionic polymerization, and the preparation is described in N. Schönfeldt, Grenzflächenaktive Ethylenoxid-Addukte, Wissenschaftliche Verlagsgesellschaft mbh, Stuttgart 1976, pp. 53 et seq. To prepare the X—Y—X copolymers, a medial polypropylene oxide block Y is usually polymerized first, and a block made from ethylene oxide units is attached at the two ends of the same. The molar masses of these block copolymers are generally from 1000 to 15,000 g/mol, and the proportion of ethylene oxide is generally from 2 to 90% by weight, preferably from 5 to 85% by weight. It is moreover possible to use products having a central block of polyethylene glycol (Y—X—Y). In this case the proportion of polyethylene glycol is usually from 5 to 80% by weight, preferably from 7.5 to 75% by weight, and the molar masses are generally from 1000 to 15,000 g/mol. The molar masses (number-average) of these compounds are determined from the OH number in accordance with DIN 53240.
Particularly preferred additives F) are inorganic or organic transesterification inhibitors, from 0.01 to 5% by weight of which, preferably from 0.05 to 2% by weight, may be present in the novel molding compositions.
Suitable organic phosphonites have the formula
It is preferable for at least one R—O and at least one R1—O group to be a phenol radical which carries a sterically hindered group, in particular t-butyl, in the 2 position.
Particular preference is given to tetrakis(2,4-di-tert-butylphenyl) biphenylenediphosphonite, which is available commercially from Ciba Geigy AG as Irgaphos® PEPQ.
Preferred embodiments and process for preparing compounds of this type can be found in DE-A-40 01 397.
Suitable inorganic transesterification stabilizers are described, for example, in U.S. Pat. No. 5,674,928. Particularly suitable compounds which may be mentioned are acid salts of phosphoric acid, e.g. monozinc phosphate, calcium dihydrogen phosphate, sodium dihydrogen phosphate and potassium dihydrogen phosphate. It is also possible to use phosphates, e.g. zinc phosphate or copper phosphate. Other metal phosphates with metals of the first or second transition group are also suitable. Use may also be made of P-containing acids, e.g. phosphoric acid, phosphorous acid, polyphosphorous acid or hypophosphoric acid. Examples of suitable compounds are Na3HP2O7, K2H2P2O7, KaH2P2O7 and Na2H2P2O7.
The novel thermoplastic molding compositions may be prepared by processes known per se, by mixing the starting components in customary mixing equipment, such as screw extruders, Brabender mixers or Banbury mixers, followed by extrusion. The extrudate may be cooled and comminuted. It is also possible to premix individual components and then to add the remaining starting materials, individually and/or likewise mixed. The mixing is generally carried at from 230 to 290° C.
In a preferred method of operation, components B) to E), and also, if desired, customary additives F), may be mixed with a polyester prepolymer, compounded and pelletized. The resultant pellets are then condensed in the solid phase under an inert gas, continuously or batchwise, at below the melting point of component A) until the desired viscosity has been obtained.
The novel thermoplastic molding compositions feature a good combination of stability in long-term service, toughness, flowability and melt stability. They are suitable for producing fibers, films or moldings, in particular for applications in the motor vehicle sector or the electronics sector, or else as household items or devices in medical technology.
Component A:
Polybutylene terephthalate with a viscosity number of 130 ml/g and with a carboxyl end group content of 34 mval/kg (Ultradur® B 4500 from BASF AG) (VN measured in a 0.5% strength solution made with a 1:1 mixture of phenyl and o-dichlorobenzene, at 25° C. to ISO 1628).
Component B:
Polycarbonate based on bisphenol A, e.g. Lexan® 161 from General Electric, characterized by a viscosity number of 61 ml/g (measured in 0.5% strength by weight CH2Cl2 solution at 23° C.).
C/1 A fine-particle graft polymer prepared from
C/2 A coarse-particle graft polymer prepared as follows:
D) A copolymer made from styrene and acrylonitrile in a weight ratio of 80:20 with a viscosity number of 83 ml/g (measured in a 0.5% strength by weight solution in dimethylformamide at 23° C.), prepared by continuous solution polymerization by a process as described, for example, in Kunststoff-Handbuch, Vieweg-Daumiller, vol. V (Polystyrol), Carl-Hanser-Verlag, Munich 1969, p. 124, lines 12 et seq.
Epoxy number from 1.68 to 1.75 eq/kg
Component F/1
Glass fibers with an epoxysilane size
Component F/2
Irgaphos®PEPQ from Ciba Geigy Spezialitätenchemie GmbH (tetrakis(2,4-di-tert-butylphenyl) 4,4′-diphenylenediphosphonite)
Preparation and testing of the molding compositions Components A) to F) were mixed using a twin-screw extruder (barrel at 250° C.). The melt was passed through a water bath and pelletized. The test specimens were produced at a melt temperature of 260° C.
The mechanical properties were also tested on injection-molded specimens (melt at 260° C., mold at 80° C.). The HDT B heat distortion temperature was determined. The impact strength of the products as determined on ISO specimens to ISO 179 1 eU. To characterize heat resistance, tensile specimens and ISO specimens were stored for 500 h at 120° C. Specimens were removed after 100, 250 and 500 h for testing (tensile test to ISO 527 and impact strength test to ISO 179 1 eU).
Table 1 lists the makeups of the molding compositions and the results of the tests.
Patent Citations
Referenced by
Legal Events
Original Image


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Mario Martin Delgado Carrillo
Senate of Mexico
Economist, Instituto Tecnológico Autónomo de México (ITAM); Master's in Economics, Essex University. Former Minister of Education, Mexico City Government. Recognized for strong efforts in the promotion of reading, work against obesity, as well as the inclusion of gender, minorities and human rights, into the City's budget. 2006, appointed Minister of Finance, becoming the youngest person in the federative entity to ever hold this post; despite the global economic downturn, was able to keep and increase social programmes as well as infrastructure projects.

subset: commoncrawl


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I happened to be in the grounds of the Bishop's Palace, where a society wedding was having it's reception.
Shot on film some 4yrs ago.
Nice documentation of the event. And you're right, you had the best shot in the house!Jan 31st, 2013 Reply
My pleasure, sir! You can buy me a pint of bitter someday!Jan 31st, 2013 Reply
Ale is on my when you're on my side of the pond.Jan 31st, 2013 Reply


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Computers & Printers
Showing results 1 – 4 of 4.
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Networking, SuperG3 33.6K Fax Modem, 8 MB Standard Memory, 30-page document feed, 250-sheet paper capacity. Lower cost-per-page with high yield consumables.
A reliable, affordable monochrome laser all-in-one with an up to 35-page automatic document feeder for home or small office use, ENERGY STAR® Qualified


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Click here to see more deals on iPod Accessories, like:
$5 + $4 shipping
Refurb Logitech Ultimate Ears 200vi Noise-Isolating Headset
As one of its daily deals, MidnightBox offers the refurbished Logitech Ultimate Ears 200vi Noise-Isolating Headset in Gray or Purple for $4.95 plus $3.99 for shipping. That's a buck under the lowest total price we could find for a new set elsewhere. These headphones feature a frequency response of 20Hz to 20kHz, in-line controls for music and phone functions, and integrated microphone. Deal ends July 10.
A 30-day MidnightBox warranty applies.
Posted July 8, 2013
Buy Now from MidnightBox


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Jun 15, 2013
Losing Weight, Losing Psoriasis
The last few weeks have been a whirlwind for the family and me. It started with my daughter's graduation from high school a couple weeks ago. I remember back when Lori was pregnant with Lydia. I was taking...
Howard Chang
The Itch to Beat Psoriasis
Encouragement on the journey to hope and healing
May 9, 2013
Los Angeles Walk to Cure Psoriasis
On Saturday most of my family joined me at the Santa Monica Pier for the Walk to Cure Psoriasis event hosted by the National Psoriasis Foundation (See my previous post here) My soon to be graduating from high school daughter...
May 3, 2013
Dousing the Psoriasis Fire
Today I had a flashback to 2008 when I thought a large fire bearing down on our city had burned down my house. The map on the local newspaper erroneously showed my neighborhood in the fire zone. Thankfully the firefighters...
May 1, 2013
Can You Learn Helplessness with Psoriasis?
Nobody wants to admit they are helpless. Just the world helpless itself sounds so incredibly negative and distressing. But a disease like psoriasis can render an otherwise hopeful person feeling helpless and hopeless. I...
Apr 24, 2013
Walk to Cure Psoriasis Event
I am looking forward to the Walk to Cure Psoriasis here in Los Angeles on Saturday, May 4th. If you don't live in the Los Angeles area there are 21 different locations around the States where the National Psoriasis...
Apr 22, 2013
The Journey to Hope and Healing Psoriasis
Over the past couple of weeks the editors at Everyday Health helped me move the Itch to Beat Psoriasis blog over to a new platform with a new look and feel. The old blogs will still remain at the old site, while the new...
Apr 12, 2013
Stress Less with Psoriasis, Part 2
Welcome to the new version of my psoriasis blog – it has a different look and feel, and we hope you'll love it. Last week, I wrote a post about stressing less with psoriasis in which I offered the first four tips...
Apr 12, 2013
The Itch to Beat Psoriasis Blog Has Moved!
Howard Chang's blog, The Itch to Beat Psoriasis, in now in a new format and location (everydayhealth.com/columns/howard-chang-the-itch-to-beat-psoriasis). He'll still be keeping you up to date on this life with...
Mar 26, 2013
Stress Less with Psoriasis, Part I
If stress exacerbates psoriasis, then I'm clearly in a high-risk category for worsening my condition.


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Jaguar Prices: Jaguar Cars Ltd., headquartered in Whitley, Coventry, England, offers the Jaguar XF, Jaguar XK and Jaguar XJ models. Ford Motors once owned Jaguar Land Rover from 1989 to 2008, though both automotive brands, Jaguar & Land Rover, are held by Tata Sons Ltd.
2015 Jaguar XF
A beautiful design and an accommodating interior merge with sports-tuned handling and superior engineering, delivering a truly commendable luxury automobile.
2014 Jaguar XF
Now available in an ultra-high performance XFR-S trim level capable of 550 hp, the 2014 Jaguar XF is a mid-size luxury sports sedan available in a variety of trim levels.
2013 Jaguar XF
New for 2013, the Jaguar XF is a mid-size luxury sports sedan available with a standard 2.0-liter turbocharged 4-cylinder engine (240 hp), optional 3.0-liter supercharged V6 SC engine (340 hp), and a performance-oriented (XFR) 5.0-liter supercharged V8 engine (470 hp).
2012 Jaguar XF
The 2012 Jaguar XF is a mid-size luxury sports sedan available with a performance-oriented 5.0-liter supercharged V8 engine that produces 510 hp and 461 lb-ft of torque.
2011 Jaguar XF
An energetic sport sedan welcoming motorist to the Jaguar brand, performance credibility skyrockets on the 2011 Jaguar XF as the vehicle's base engine is now 385 horsepower.
2010 Jaguar XF
The 2010 Jaguar XF is a powerful luxury sedan with understated good looks and a host of upscale options to choose from including an 18-way power adjustable driver's seat and adaptive cruise control.
2009 Jaguar XF
A midsize luxury sport sedan with coupe-like styling, the brand-new 2009 Jaguar XF delivers a refined ride, sporty handling and powerful performance.


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Yes, we're deep into the year, but that's not going to stop us from showing you some of the new knives of 2015. We're continuing with new products from Condor Tool & Knife.
There's not as a robust offering of new products as some of the other brands, but the 2015 products from Condor TK are definitely worth a look.
Final Frontier
We're kicking things off with the Final Frontier. This is a nice fixed blade with a 4-inch blade that has a Scandi grind. The blade itself has epoxy black powder coating. Hollow rivets hold together the ergonomic handle made of Micarta. At the butt of the knife is a smashing pommel.
It comes with a sheath.
Primitive Bush Knife (Matt Graham edition)
The Primitive Bush Knife is a collaboration between Condor TK and survivalist Matt Graham. Using his experiences living off the land, Graham designed this knife for outdoor adventures. Its 8-inch blade is made of 420HC steel.
It has a hardwood handle and comes with an interesting handcrafted leather sheath that's supposedly more like a pouch.
Mini Duku Parang Machete
Next up are the two Mini Duku Parang Machetes. Both machetes feature blades made of 1075 high carbon steel with a natural finish and boast hardwood handles.


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Wilderness Poems. Below are examples of wilderness poems. This list of poems about wilderness is made of PoetrySoup member poems. PoetrySoup is a great resource for examples of wilderness poems or list of wilderness poetry. These examples illustrate what wilderness poems looks like and its form. There is also a link (below) to the definition where you can discuss wilderness poems.
The wilderness poem sub-topics listed below include many popular topics of poetry.
Note: The forms for these wilderness poems were selected by the poet. Often poems are assigned the wrong form. Please confirm the accuracy of the poetic form before referencing the poem.
Don't see what poems you want? Try our Advanced Poem Search for more results!


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picture of lighthouse on sos - orlando port/cococa
i have seen several pictures of the lighthouse you pass when on sovereign or the sea - it is either when the ship pulls out of the orlando port or on the way to cococay or maybe even when the ship is pulling in to nassau -- in any case i can't remember where i saw the picture but it was somewhere here on cruise mates ...
can anyone tell me where i can go to in order to see a picture of the lighthouse from the ship?
i know ... this is like looking for a "needle in a haystack" but if you can help me out, i will gladly send you a check for $55 million dollars .... :)
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330 Wall Street
Kingston, New York, 12401
Commute to Downtown Kingston
Most errands can be accomplished on foot.
Score Details
330 Wall Street has a Walk Score of 81 out of 100. This location is Very Walkable so most errands can be accomplished on foot.
This location is in Kingston. Nearby parks include Senate Park, Dietz Memorial Stadium and Forsyth Park.
Nearby schools include St Joseph School, Winter Bear Montessori School and George Washington School.
The closest grocery stores are Main Street Market, Four Corners Deli and Charles Grocery-Deli.
Nearby coffee shops include Sissy's Cafe, Dominick's Cafe and Dunkin' Donuts. Nearby restaurants include Stockade Tavern, Opa! Gyros Greek Grill and Elephant.
Explore how far you can travel by car, bus, bike and foot from 330 Wall Street.
View all Kingston apartments on a map.
Popular apartment searches include hardwood floor and top floor.
This location is in the city of Kingston, NY. Kingston has an average Walk Score of 56 and has 23,893 residents.Learn More About Kingston


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Deltour Millau City Hotel
No availability found through our partners. Please contact the business directly or check some of our recommended alternatives.
- Free High-Speed Internet
- Swimming pool
- Restaurant
- Wheelchair accessibility
- Free parking
- Pets allowed
Photos of Deltour Millau City Hotel
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Muddle in the middle of Millau
... snow ploughs and the road status was ' delicat' !!
We had been this way before about 7 yrs ago, but had forgotten most of it. We really enjoyed the 'swooping' up and down on a lovely new road surface. We made a quick stop to see the Viaduct de Garabit, built by Eiffel. There is a motorway aire with wonderful views ...
New baby day
... night next to a usually busy road. Some rain en route today but OK now. It was a great drive down into Millau and we saw some eagles flying, below us at first, they are always fantastic to see. A great night's sleep despite heavy rain for an hour or so. Easy to walk into town from here and lovely views. Will come ...
The ride continues Rubber Down & Thunder Thighs
... and 275m long. Each block weighed about 5 Tonnes and it took three years to build. From Annecy we headed to the twisty roads on the map. The region is the Cevennes National Park and the town to stay in is Florac. This is motorcycle heaven. I know this sounds a little hard to believe but we were able to ride paved roads up and down the walls of the Gorges du Tarn. With out a doubt the best paths we have ever been on. We also were able to spend some time with friends ...
... I think they enjoyed the opportunity to chat with someone who wasn't going to take a shot, unless it was about rugby. They offered a photo op the next morning at 8am. Man we were up early for that! And when we got outside the hotel it was apparent that their motos were still at the police station. So we went for breakfast and then met them later at the station for photos and coffee. Again a few laughs and then we headed south west towards St Affrique. The rain ...
Bit hairy to say the least
... are 2 of us that are told) ends up being not so easy. We were hurried out the door as they close for lunch at 12.
So, we were off. First stop fuel. Well, do you think we could find the fuel cap! We were just shown 5 minutes ago. After much searching, we found it, then the next problem getting the fuel to start pumping. We couldn't work out why it wouldn't start, then we worked out that you had to swipe your credit card. So we did that and voila, fuel. Next we ...


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There are many reasons for racing, but how often can you ride for 24hrs straight just for the heck of it. It's a great escape from the everyday grind and a huge sense of accomplishment to finish, whether it be on the podium or DFL.
Results 51 to 51 of 51
Thread: why do it?
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TL Publishing Group
New Release 4/1/15: Torrid Literature Journal - Vol. XIV Chaos
Free Download: Torrid Literature Journal: Vol. XII Tension
New Release!!!
Happy New Year! Our first issue of 2015 is now available for purchase!
New Release January 1st:
Torrid Literature Journal - Vol. XIII Déjà Vu
Order your copy from Amazon today!
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Content copyright TL Publishing Group LLC. All rights reserved.


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|Reviews for The Mind Of The Tetris Piece
| FallenToMusic chapter 1 . 4/1/2013
You just made me almost cry, as well as my friend. That's actually very impressive *applause*
| Vincent chapter 1 . 12/7/2012
wow that's actually beatiful, I'll never be able to play tetris again though
| writetheorange chapter 1 . 11/21/2012
Omg I can't believe I read this! But I did. There really wasn't a plot, but the thoughts were really weird and because it was short, interesting.


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Call: 1-855-695-2464 1-855-695-2464
Click: Dealer Website
View: Similar Cars from this Dealer
Auto Wise23571 Pebble Run Pl Ste 165, Sterling,
CARFAX Dealer Since 2014
Call: 1-855-695-2464
Auto Wise23571 Pebble Run Pl Ste 165, Sterling,
CARFAX Dealer Since 2014
Some of the cars are at a satellite storage place. PLEASE CALL BEFORE COMING - in order to have the car ready for you. Call or text for more info or set up an appointment !
$2,999 *
Features and options are descriptive of what can be expected on the vehicle. Actual options should be verified by the customer and dealer.
Price may exclude state and local fees and taxes and freight or destination charges or processing fees. Please contact the dealer to confirm price and vehicle availability. Current mileage may vary due to test drives and vehicle relocation.
CARFAX Vehicle History is based only on information supplied to CARFAX. CARFAX Vehicle History information on this page is current as of 04/01/15 at 03:08:00 PM (CDT). The CARFAX Vehicle History Report for the vehicle may contain more current information. Other information about the vehicle, including problems, may not have been reported to CARFAX. Use the CARFAX Vehicle History as one important tool, along with a vehicle inspection and test drive, to make a better decision about your next used car. Vehicle descriptions and details on this page may have been provided, in part or entirely, by the seller or its agent. CARFAX does not verify these descriptions and details, and is not responsible for the accuracy of the information. Please refer to the CARFAX Terms of Use for further information.


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Kadetus Hostel
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Polishing Off the Trip
Today is our last day in Krakow before we head home. The weather has warmed a bit and the skies are blue, so with no set plans, we decided to stroll Old Town in search of the last few must-dos before we departed.
We toured the Royal Residence atop Wawel Hill and its stately, medieval rooms. Now that the mist had dissapated, we could …
I Am a Pole (And So Can You!)
Note: Five points to Gryffindor for anyone who recognizes the Stephen Colbert reference.
Our sleeper train from Vienna to Krakow, Poland, was cozy and snug- we had a little second-class bunk with a sink, and we slept under down duvets until the train pulled into the station at 6am. The Krakow train station, like Vienna's and Salzburg's …
Bohemian like you
... of over 100 countries and counting. Never one to call a spade a shovel, Peter kept us entertained with his stories of rubbing shoulders with the greats of English and Australian cricket, along with good natured ribbing of us poor old convicts! Bratislava is largely reminiscent of Wroclaw, cities whose former charms can still be glimpsed amongst soviet abominations. There is evidence of progress with new buildings and infrastructure and ...
A Day At Auschwitz
... murdered here alone. My day started in Auschwitz, which is about an hour and a half outside the city. Walking onto the site gave a very eerie chill, as I gazed out onto the 28 blocks that locked in thousands of victims, most of whom were Jewish. It is important to note that many other people were the victims of the Nazi's too, including Polish citizens (and other nationalities), soldiers, Gypsies, homosexuals, the ...
When in Poland..meet at the head!
... John Paul in Krakow and 400 in all of Poland. That's adoration. On the doors of the castle there are "dragon bones" chained up. Supposedly when/if they fall it means the end of the world is near. Okay Mayans..haha.
Shelby and I decided to go to the top of St. Mary's Church (we went to the top of the highest building/mountain in every place thus far). The stairs to get to the top were scary! They were very small and uneven. I felt like I was going to the top of ...


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3 products
Begin faceted search navigation.
Viewing 1 – 3 of 3 products
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Kate Aspen 24-pk. Big Top Circus Favor Boxes
Regular $19.99
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Regular $15.99
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Regular $24.00
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Sponsored Links
The links below are ads provided by the Google AdWords™ program. Outside companies pay to advertise via these links when specific phrases and words are searched. These ads are provided by Google and are labeled as sponsored links. Clicking on these links will open a new tab displaying that respective company's own website. The website you link to is not affiliated with or sponsored by Kohls.com


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Posts Tagged 'texas'
Cowgirl PoetThough traditional C&W singer-songwriter Ginny Mac has just graduated from college, she's old-school Old West.
Ginny Mac is a throwback of sorts. The slight, shy twentysomething Fort Worthian lives somewhere between her laptop and the vintage Western wear she finds at secondhand stores.
Arggghhht!A local quartet cranks up the rhetorical noise, all the way to 111.
Home to elegant mannerists John Hartley, Nancy Lamb, Leslie Lanzotti, Jo-Ann Mulroy, and twin brothers Daniel and Dennis Blagg, Artspace 111 may be the last place you'd expect to find politically charged art.
WhiskersThough still young, the Catfish Whiskey guys have matured a lot recently, as their new LP may prove.
Five years ago, Catfish Whiskey was all about the party.
Downwind of a WindfallAir pollution settlement will provide seed money for "green" projects.
Generally speaking, when small environmental groups take on gigantic corporations, it usually doesn't end well for the little guy – or the environment, for that matter.
Magical Misery TourJEFF PRINCE
Memento scavengers made hit-and-run stops for two days, stepping out of their cars to survey the pile of rubble in hopes of nabbing a brick, a fixture, a cinder block painted a familiar blue, any reminder of Fort Worth's ...
Magical Misery TourGen-Y'ers didn't invent the scuzzy wonders of Fort Worth's rock scene.
Jeff Prince
Memento scavengers made hit-and-run stops for two days, stepping out of their cars to survey the pile of rubble in hopes of nabbing a brick, a fixture, a cinder block painted a familiar blue, any reminder of Fort Worth's ...
The Crash That Took MeListen Up
Why is everybody so nostalgic all the time?
Eyes on TxDOTActivist Terri Hall has TxDOT's dream of toll roads in her sights.
Peter Gorman
It's looking like a tough year for toll roads in Texas, and no one could be happier about that than Terri Hall, the San Antonio woman whose group is leading the grassroots fight against the controversial pay-to-drive road...
The Big Picture(s)Kultur
A touring photo exhibit perplexes, while the 817′s two major dance companies generate some ka-ching.
Pump It UpDrummer Adonis Rose keeps taking giant steps toward putting the Fort on the jazz map.
When Adonis Rose arrived in Fort Worth a little more than two years ago, he found the jazz scene here a little lacking.


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You are a fan of vindictive alien ? Come to discover the best forums vindictive alien on the internet and share your experience with a community fan of vindictive alien . You can also build a forum vindictive alien and create your online discussion.
Ruthless Galaxy is a great place to discuss science fiction and submit your art and writings to help us build our story!
Psionic Freaks is a community of Practitioners & Explorers of Psychokinesis/Telekinesis, Extrasensory Perception/ESP, Energy Manipulation, Meditation, Paranormal, Occult, Psychic, Magick, UfO/Alien & Much more. We are pushing the limits of the mind,
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Free forum : Original sci-fi universe created by a community that is passionate about science fiction.
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A Fan of Space Adventures brought to you by four dysfunctional flightless alien birds? Then this is the place to go to talk about it!
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Dark Sky Watchers is for all Astronomy, UFO, Alien, NWO Conspiracy Topics
dark, watchers, astronomy, #alien, conspiracy, topics


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Israeli AG Rules They Can't Kill Their Own Soldiers To Prevent Capture
One of the worst conundrums facing modern militaries engaged in asymmetrical warfare is what to do in the event that one of your soldiers was captured. For decades, the Israeli Defense Forces have relied on a still-classified and highly controversial method known as the "Hannibal Protocol." And now a large part of it… »


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Free concert Thursday at Holmes
The 8th Street String Quartet, the "all-star" ensemble of the principal string chairs of the Fargo-Moorhead Symphony Orchestra, will perform a free concert at Detroit Lakes' Historic Holmes Theatre this Thursday, Sept. 9, at 7 p.m.
The quartet includes Symphony Concertmaster Benjamin Sung and Assistant Concertmaster Jane Linde Capistran, violin; Tim Nelson, Principal Viola; and Elise Buffat Nelson, Principal Cello.
Are you a newspaper subscriber but you don't have a Digital Access account yet? https://secure.forumcomm.com/?publisher_ID=40&event=subscriber/lookup.
You will need your subscription account number and phone number. Not sure if you have an account? Email us at firstname.lastname@example.com and we can help you.


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- 7 comments
mcm2014 Dec 16, 2014 at 09:33 UTC - 0 likesBurberry Outlet Online, http://www.burberryfactorys.com/
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macbooster Oct 13, 2014 at 08:12 UTC - 0 likes
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Art Sampler Classes
This is a new series of Art Sampler classes aimed at adults (and older kids with a parent) who are interested in learning the basics of various art techniques. Local artists will teach painting, needle felting, drawing, photography and whatever else we can think of!
The next class, on April 19 from 2 - 5 PM. is 2D Mixed Media Collage by Jennifer Bachelder.
There are class fees associated with each class, and pre-registration is encouraged. Click below to learn more! More
Upcoming Events
March 20 - April 12
A Photographic Essay of Yellow Springs by 8 local Instagram photographers, Amy Hable, Corrine Bayraktaroglu, Talitha Green, Sandi Sharp, Steve Ali, Lori Gravley, Julius Eason and Adrian Cosby.
April 4
Singer/Songwriter Concert featuring David Schumacher, Lorna Hunt, and Nicole Adele
April 11
Arts Alive! featuring Lo Sparks
April 19
Art Sampler Class
Gallery Calendar
111 Corry Street, Yellow Springs
Open Wednesday thru Sunday, 1-4 pm More
Most of the YSAC Permanent Collection now hangs in the hallways of Antioch University Midwest (AUM) at 900 Dayton Street in Yellow Springs. We are proud to partner with AUM to bring you this body of art, representing the artistic heritage of Yellow Springs. The Collection can normally be viewed during AUM's General Operating Hours Monday - Friday from 8:30 am - 5:00 pm and Saturday from 8:30 am - 3:00 pm. AUM also sponsors community arts and cultural programs, such as the Yellow Springs Experience. More
Yellow Springs Artist Directory Now Available!
The wait is over! After nearly a year of gathering information, layout and editing, the print version of the Yellow Springs Artist Directory is available now. The directory contains nearly 300 artists including visual artists, authors, performers, musicians and more! Pick up your copy for just $2 at the Yellow Springs Arts Council Community Gallery.
And remember, everyone who is listed in the Directory gets a free copy. Stop by and get yours today!More


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Just how street is Brooklyn rapper Haffa? Well, let's just say that if he were any more street, his clothes would be covered in tire treads. As evidence, I present So Gully, the first official leak off the Booth newcomer's forthcoming mixtape. Rapper/producer Scram Jones mans the boards on this gritty track, borrowing a vocal sample from 50 Cent's Disco Inferno to serve as the centerpiece of his tense, percussion-synth beat. For his part, Haffa comes with aggressive flows to match Scram's grimy boardwork, peppering his hard-nosed bars with polysyllabic rhymes: "There's a war goin' on outside, no man is safe from / so I keep a bulletproof and a space gun / and I emerge from the jungle where the apes hung…" Does this hood-certified up-and-comer have what it takes to hustle his way to the top of the game? Speculation is welcome, but we won't know for sure till March 12, when The Cookup (presented by Scram) hits the 'net.
Written by richard on 02/22/10
Submit your Rating
Beast Music Records
First DJ Booth Appearance:
"Yes We Can ft. Rhymefest, Haffa, & Saigon" (2009)
Total DJ Booth Features:
1 Songs
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Super 8 Cedar Rapids
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Day 3: West Branch Iowa--Herbert Hoover Museum
... make a considerable fortune in mining in Australia and China, before truly answering the call to become a public servant. He is arguably the biggest proven humanitarian to have served as president. He led hunger relief efforts that saved millions in Europe during and after WWI; and led disaster relief efforts during massive floods which plagued the Mississippi River. I could drone on and on, but I will try to hit some ...
Step back in time. . .
... all using the name Amana and a second word. South Amana, East Amana, West Amana, North Amana, High Amana, and Middle Amana. The residents in the early days received housing, medical care, meals, schooling, etc.Jobs were assigned but no one received a wage.
We enjoyed walking the streets and looking in the shops. We had lunch in the Ox Yoke Inn and enjoyed a fine German dish of ...
It's wise to look ahead......
... 8211; that name regularly appeared in spelling tests as a boy, and I have never before had the chance to use it in anger! Of course we stopped for a picture and to dip our hands in the famously muddy water – but swimming was not really an option. And so we end up in a hotel in Iowa City, Iowa. Our 8th state of the trip. And tonight we're not looking any further ahead than the 24 hour weather forecast.
232 miles today
Windy and rain tonight. . .
... weather forecast is not too good as storms are predicted along our path.
Our destination is Amana Colonies in Amana, IA. This is an historic German town that we stopped briefly on our trip to Alaska in 2012. The town closes up at 5:00 pm so we decided to come back and stay a few nights to check it out. More tomorrow on our venture into town.
I have included a short video of what we see as we head down the road. Enjoy.
Corn Fields and Ground Squirrels
Yesterday, Mike turned 65. He is officially a Senior Citizen. It's hard to believe it was all those years ago, we were just a couple of kids, going to the dance at the Pine Grove Pavilion in Portsmouth. Now, here we are, closing in on the first major destination of our journey, Yellowstone National Park. Tomorrow we pull out and head towards Lincoln, Nebraska. ...


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|What Plays Like A Dunlop Biomimetic 200
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Was $199.95
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The 200 from Dunlop has always garnered respect from advanced level players. Rock solid from the baseline and smooth and precise at net, this one carries on the 200 legend. If you like the 200, these other control-oriented racquets will be a good fit.


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Customer Reviews
For GAP SO PINK
by Gap
This is my signature scent. I hope you never discontinue it. I usually wear it in the summer when it is hot due to the fresh, crisp scent. I like a bit heavier scents in the fall and winter.
Written by Lora on September 24, 2013Read Review details ►
I have worn this fragrance for a long time. I love it, everytime I switch to something new I always go back to So Pink. I have worn more expensive fragrances and never had I received more compliments than I do with So Pink. Guys love it! And ask me all the time where did I get it, and people always say you smell sooo good, or someone smells good. I was in a sandwich shop and the guy behind the counter said someone sure smells good today. LOL! and he was slicing meat all day. LOVE IT!!!
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Excellent Fragrance, Excellent service and delivery even in Canada! Wow i am impressed! Simon from Montréal, Qc
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gap so pink got it for my birthday and used it up love it. been trying to get more the stores didnt have any more for a long time. glad i was able to find it on line. nice scent like grapefruit. will open your sense of smell put a smile on your face.
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i love so pink by gap. i was looking for the perfect scent for the longest time and in the end it came down to chanel's chance eau tendre and gap's so pink. i chose so pink and i'm so glad i did
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so pink is my favorite fragrance makes me feel clean and fresh all the time . women have ask me what perfume im wearing because smells good . I love it have been wearing it for the last 6 yrs and will never get tire of it. I go to san antonio to get it and it's far from where I live. never get rid of this fragrance. thank you Ellie.
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This scent is so nice. This smells like a sweet pink grapfruit.. it's one of my favorites
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Very nice citrus scent. You can especially smell the grapefruit.
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My first parfum and I'm so happy with it, it's great!
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Craft room what it used to look like
minnie_txJuly 15, 2008
There are pictures of what the craft room used to look like on page 4 in the gallery if interested
leather pictures in 3D handcrafted
leather pictures in 3D handcrafted
online shop www.leatherpicyure.co.uk
and market in Gloucester
Leather pictures are news in UK
FlamingO in AR
Holy MOLY! You got rid of a ton of stuff, Minnie! How does your craft room look now? I would love to see it.(Oh, I found the pics on page 5, btw.)
I just painted my craft room and redecorated it a bit. I'm still not sure I like it, all my friends do but I'm thinking lime green paint wasn't the smartest decision I've ever made. It's pretty shocking.


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Your Dog, Your Life
The Scoop
Dog News, Politics
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Doggie Style
Gear and Glam
Wildebeest creates the perfect present for new dog parents.
Dog Breeds
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Health & Care
Behavior & Training
Dogs & Cleaning
Dog of the Day
georgie girl aka gigi
8-year-old Female
Other pets in your family: Tatum Gilda (atb) | Casper Dory | Sadie Jean - ATB 5/2/07 | Madden Marie
Copyright © I-5 Publishing, LLC. All rights reserved.
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Dr. John M. Dawson, MD
Podiatric Medicine
- 1700 Prairie City Rd
Folsom, CA 95630
- 2 Locations
- (916) 351-4800
Dr. Dawson works in Folsom, CA and 1 other location and specializes in Podiatric Medicine. Dr. Dawson is affiliated with Mercy General Hospital, Mercy Hospital Of Folsom and Mercy San Juan Medical Center.
Gender: Not Available
Languages Spoken: English
Podiatric Medicine
Medical School: Not Available
*This physician has multiple office locations. See Office Information for details.