text:
A method is disclosed for the elimination of hazardous metal wastewater and sludges by recovering the non-ferrous metals zinc, nickel, copper (II), cadmium or chromium (III) present in an aqueous sludge comprising mixed metal hydroxides by selectively precipitating the ferrous metal ions present while maintaining the non-ferrous metal ions in solution, isolating the precipitate and then precipitating the non-ferrous metal ions from solution.
1. A method for treating wastewaters and sludges from a plating process to facilitate reuse of metal values by the recovery of non-ferrous metal hydroxide, said method comprising the following steps (a) through (f) in the order presented:
(a) lowering the pH of an aqueous slurry obtained from a plating process from an alkaline pH to an acid pH, said slurry comprising solid ferrous hydroxide and a solid non-ferrous metal hydroxide wherein the non-ferrous metal is selected from the group consisting of zinc, nickel, copper (ii) cadmium, and chromium (III) to dissolve the non-ferrous metal hydroxide;
(b) converting the ferrous hydroxide to solid ferric hydroxide by aeration of the aqueous acidic slurry;
(c) isolating the solid ferric hydroxide from the slurry leaving a solution comprising non-ferrous metals;
(d) raising the pH of the solution of step (c) to precipitate non-ferrous metal hydroxide;
(e) recovering the precipitated non-ferrous metal hydroxide; and
(f) introducing said non-ferrous metal hydroxide into the plating process.
2. The method of claim 1 wherein the isolated solid ferric hydroxide of step (c) is washed with dilure aqueous acid and the aqueous acid is added to the aqueous slurry of step (a).
3. The method of claim 1 wherein the non-ferrous metal hydroxide comprises a mixture of zinc hydroxide and a second hydroxide of nickle, cooper (II), cadmium or chromium (II); and wherein in step (d) the pH of the slurry is raised to above 12.0 to maintain the zinc hydroxide in solution while precipitating the second metal hydroxide.
4. The method of claim 3 whe the pH of the slurry is raised to about 12-13.5 step (d).
5. The method of claim 4 further comprising lowering the pH of the slurry to precipitate the zinc hydroxide following step (e).
6. The method of claim 5 wherein the pH is lowered to about 7-11 following step (e).
7. The method of claim 1 wherein the non-ferrous metal hydroxide comprises zinc hydroxide.
8. The method of claim 7 wherein the pH is lowered to about 3-7 in step (a).
9. The method of claim 7 wherein the pH is raised to about 7-11 in step (d).
10. The method of claim 1 wherein the non-ferrous metal hydroxide comprises nickel hydroxide.
11. The method of claim 10 wherein the pH is lowered to about 3-7 in step (a).
12. The method of claim 10 wherein the pH is raised to about 8-14 in step (d).
13. The method of claim 1 wherein the non-ferrous metal hydroxide comprises copper (II) hydroxide.
14. The method of claim 13 wherein the pH is lowered to about 3-7.0 in step (a).
15. The method of claim 13 wherein the pH is raised to about 8.0-14.0 in step (d).
16. The method of claim 1 wherein the non-ferrous metal hydroxide comprises cadmium hydroxide.
17. The method of claim 16 wherein the pH is lowered to about 3.0-7.0 in step (a).
18. The method of claim 16 wherein the pH is raised to about 7-14 in step (d).
19. The method of claim 1 wherein the non-ferrous metal hydroxide comprises chromium (III) hydroxide.
20. The method of claim 19 wherein the pH is lowered to about 3-5 in step (a).
21. The method of claim 19 wherein the pH is raised to about 5.75-14 in step (d).
22. A method for treating wastewaters and sludges from a plating process to facilitate reuse of metal values by the recovery of zinc hydroxide, said method comprising the following steps (a) through (f) in the order presented:
(a) lowering the pH of an aqueous slurry obtained from a plating prodess from an alkaline pH to an acid pH, said slurry comprising solid ferrous hydroxide and solid zinc hydroxide, to dissolve the zonc hydroxide;
(b) converting the ferrous hydroxide to solid ferric hydroxide by aeration of the aqueous acidic slurry;
(c) isolating the solid ferric hydroxide from the slurry leaving a solution comprising zinc;
(d) raising the pH of the solution of step (c) to precipitate zinc hydroxide;
(e) recovering the precipitated zinc hydroxide; and
(f) introducing said zonc hydroxide into the plating process.
23. The method of claim 22 wherein the pH of the aqueous slurry in step (a) is about 8-11 prior to lowering.
24. The method of claim 22 wherein the isolated solid ferric hydroxide from step (c) is washed with dilute aqueous acid and the aqueous acid is added to the slurry of step (a).
25. The method of claim 22 further comprising thermally converting the recovered zinc hydroxide to zinc oxide.
26. The method of claim 22 wherein the pH is lowered to about 4-5.5 in step (a).
27. The method of claim 26 in the pH is lowered by combining the slurry with sulfuric acid or hydrochloric acid.
28. The method of claim 26 the pH is raised by combining the slurry with an alkali metal hydroxide.
29. The method of claim 22 wherein the pH is raised to about 8.5-9.5 in step (d).
The present invention provides a process for eliminating hazardous plating wastewaters and waste metal sludges by the recovery of toxic non-ferrous metals therefrom by the use of selective precipitation.
Ferrous metal products are commonly rendered corrosion resistant by the application of electroplated coatings of non-ferrous metals such as zinc, nickel, copper, cadmium and chromium. Electroplate is also employed to provide a decorative finish on many types of metal products. Zinc is the metal which is predominantly employed for electroplating.
Presently, more than 40% of the plating shops in the United States electroplate zinc from a variety of plating baths. These include highly alkaline plating solutions, which often contain cyanide as a complexing agent, and acidic baths containing chloride or sulfate salts and buffers for pH control. Other less commonly-used acidic baths use fluoroborate and pyrophosphate salts. Proprietary organic additives are often used to produce a bright finish.
Each year, zinc plating operations in the United States generate five billion gallons of wastewater contaminated with zinc, which must be removed prior to release of the wastewater into the environment. The majority of zinc platers currently employ conventional wastewater treatment techniques for the removal of zinc. Typically, the pH of the wastewater is adjusted to about 8-11 to precipitate the metallic cations as the corresponding hydroxides, which are gravity concentrated and dewatered to yield a toxic heavy metal sludge.
Even when highly concentrated, this sludge is not reusable in plating baths, since it contains substantial amounts of iron and water hardness factors (calcium and magnesium salts). Therefore, the sludge must be containerized and shipped to environmentally-secure landfill sites. The total cost of such "safe" permanent disposal is very high, and can equal or exceed the value of the chemicals used in the plating process. The number of these hazardous waste disposal sites is declining. Many of the sites will require costly remedial action under state and federal laws which hold the waste generator to be ultimately responsible for clean-up costs. The proposed USEPA Disposal Elimination Schedule will force platers to employ metal recovery methods by banning land disposal of such hazardous electroplating wastes by 1988. See Federal Register (May 13, 1985).
In order to avoid the formation of these intractable chemically-complex metal waste sludges, processes have been developed based on the selective precipitation of metal values from aqueous solutions of dissolved metals. For example, U.S. Pat. No. 3,800,024 discloses a process for the sequential removal of iron, chromium and nickel from spent acidic steel pickling solutions by raising the pH of the solution in two steps. R. F. Pagel, (U.S. Pat. No. 4,025,430), discloses the sequential treatment of an acidic effluent with a controlled amount of lime, followed by precipitation of the metal ions remaining in the overflow with sodium silicate. However, such processes do not address the problems associated with recovering the metal values from alkaline plating wastewaters and waste metal sludges containing mixtures of precipitated metal hydroxides. Furthermore, the presently-available technologies such as ion exchange, reverse osmosis, evaporation and electrolysis cannot economically separate and recover the metal values from these complex wastewaters and sludges.
Therefore, a need exists for a method to remove the metal values from metal-containing wastewaters and sludges to afford effluents which can be safely discharged into the environment. A further need exists for a method to separate non-ferrous metals from the ferrous metal and water hardness factor impurities present in these aqueous metal wastes to yield a reusuable non-ferrous metal-containing product.
The present invention is directed to a method for the recovery of metal values from wastewaters and waste metal sludges which comprise aqueous slurries or dispersions of ferrous metal and non-ferrous metal hydroxides. Such wastewaters and sludges are the product of the conventional treatment of metal-contaminated effluent water, including wastewaters from electroplating, electropolishing, mechanical metal plating, anodizing, acid pickling and cleaning, and the like. Typically, the wastewaters from a given process are combined and treated with alkali metal or alkaline earth metal hydroxides or oxides to yield colloidal metal hydroxide dispersions, or sludges.
According to the present invention, an aqueous slurry comprising solid ferrous hydroxide [Fe(OH)2 ] and a solid non-ferrous metal hydroxide such as zinc, nickel, copper (II), cadmium or chromium (III) hydroxide is treated to oxidize the Fe(OH)2 to ferric hydroxide [Fe(OH)3 ] and pH-adjusted to precipitate the Fe(OH)3 while retaining the non-ferrous metal in solution. The solid Fe(OH)3 is then removed from the slurry and the pH of the liquid phase is adjusted to reprecipitate the non-ferrous metal hydroxide. This solid product is then isolated from an aqueous effluent which has been cleared of metal values to the extent that it can be safely discharged into the environment. Typically, the recovered non-hazardous ferric hydroxide is also disposed of while the non-ferrous metal hydroxide is of sufficient purity to be re-used in the primary metal-treating process without further treatment.
In a preferred embodiment of the invention, essentially pure zinc hydroxide is recovered from mixed metal hydroxide sludges. These sludges can be obtained from waste-waters containing dissolved zinc and iron, such as those generated by alkaline and acidic zinc plating streams, including preplate and postplate operations. The pH of the process wastewater is adjusted to about 8-11 to yield an aqueous slurry comprising solid zinc hydroxide and iron hydroxides. Preferably, this treatment slurry is then concentrated by gravity settling or filtration methods to reduce the volume of the liquid slurry. The pH of the slurry is then lowered to dissolve the zinc hydroxide while the slurry is aerated to oxidize ferrous hydroxide to insoluble ferric hydroxide. The insoluble ferric hydroxide is then removed from the slurry, e.g. by filtration, and the pH of the resultant filtrate is raised to reprecipitate the zinc hydroxide. The recovered solid zinc product can be returned to the plating bath without further treatment. Alternatively, the zinc solids can be thermally converted into zinc oxide, e.g. by heating the hydroxide cake at 300�-500� C. This embodiment of the present process permits the recovery of greater than 90%, preferably about 93-98% of the total zinc present in the starting slurry (the wastewater or sludge) over a wide range of operating temperatures (about 10�-90� C.), employing inexpensive, readily available reagents.
If desired, the steps of the present process can be readily automated, so that the combined plating process wastewater streams are converted into a mixed metal hydroxide sludge, concentrated and further processed to recover the plating metal values in a continuous fashion. Such an automated system can be established and operated with relatively inexpensive, commercially-available equipment.
The amphoteric precipitation properties of zinc salts can also be used to separate zinc from additional non-ferrous metals in the course of the separation of the non-ferrous metal hydroxides from iron hydroxide. For example, a zinc-nickel-iron hydroxide mixture is separable by lowering the pH to dissolve the zinc and nickel hydroxides while aerating to precipitate ferric hydroxide. The pH is then raised to above 12, e.g. to about 12.0-13.5 to precipate nickel hydroxide while retaining the zinc in solution as the zincate ion. After removal of the nickel hydroxide, the pH is lowered to about 7-11 to reprecipitate the zinc hydroxide.
Although for convenience, the precipitated metal solids are referred to herein as "hydroxides", it is believed that they may contain substantial amounts of other compounds such as hydrated oxides, and carbonates.
The aqueous slurries of mixed metal hydroxides which provide the starting materials for the present invention can be formed from dilute aqueous solutions of metal ions such as the acidic or alkaline wastewaters which are derived from a wide variety of metal processing operations. For example, a typical zinc electroplating process employing an alkaline zinc cyanide bath at pH 12-13.5 also includes the following operations; preplate cleaning, preplate pickling, preplate stripping and postplate chromating wastewater. Wastewaters from acidic zinc plating baths (pH 1-6.5) can also be processed by the present method. Furthermore, zinc mechanical plating (peen-plating) also yields wastewater containing dissolved zinc.
If necessary, the wastewaters are pretreated to destroy metal-ion complexing agents and to reduce hexavalent chromium. The pH of the wastewater is then adjusted to about 8-11 with an alkali metal hydroxide or alkaline earth metal hydroxide to precipitate the metal ions as the corresponding hydroxides. See, for example, U.S. Pat. No. 4,338,200. Preferably, the resultant slurry is concentrated prior to further processing, e.g. from about 0.05-1% solids to about 1-7% solids, for instance, by gravity settling in a flow-through tank or a still holding tank. Alternatively, more concentrated sludges which are in the form of semi-solid cakes or pastes can be diluted with water to flowable slurries prior to further processing according to the present invention.
The aqueous slurry comprising a mixture of metal hydroxides is then treated to complete the oxidation of the ferrous hydroxide present to ferric hydroxide and to selectively solubilize the non-ferrous metal hydroxide present, e.g., zinc hydroxide. Preferably, these operations are carried out in the same treatment zone, which may be referred to as the "metal dissolving zone." More preferably, the oxidation and pH lowering steps of the present process are carried out simultaneously, although in some instances it is desirable to accomplish the oxidation step prior to pH adjustment.
For example, an aqueous sludge comprising about 1-7% hydroxide solids can be gravity-flowed into a metal dissolving zone such as a treatment tank where the liquid is agitated, aerated and treated by the addition of an acid to lower the pH to the desired range, e.g. to about 3-7. Agitation and aeration may be accomplished by any convenient means, e.g. by propeller stirring or by low pressure air bubbling, respectively. Acid additions can be controlled by a pH receiver which is operated to maintain a given pH at a monitoring electrode.
Preferably, the pH will be lowered into the desired range by means of the addition of the appropriate amount of an aqueous mineral acid such as sulfuric acid, hydrochloric acid, and the like, while aeration is continued until substantially all of the ferrous oxide present has been converted into ferric oxide. The end-point pH is selected to fall within a range wherein (a) the desired non-ferrous metal hydroxide is soluble and (b) ferric hydroxide is not significantly soluble. These metal dissolving ranges are summarized in Table I, below, for a number of non-ferrous metals.
TABLE I______________________________________ Dissolving Range (pH)Metal Useful Preferred______________________________________Zn+2 3-7 3.2-6.6*Ni+2 3-7 3.2-6.7Cu+2 3-7 3.2-6.4Cd+2 3-7 3.2-6.5Cr+3 3-5 3.2-4.9______________________________________ *Optimal: 4.0-5.5
Following pH stabilization and a sufficient period of aeration and agitation, the solids-laden "dissolved metal" slurry is treated to remove the precipitated ferric hydroxide and any hardness factors precipitated by the addition of sulfuric acid, e.g. CaSO4. The removal can be accomplished by filtration systems such as plate filter presses, gravity belt filters, vacuum belt and drum filters, centrifugal filters and the like. The isolated solids can also be washed with aqueous acid (pH 4-6) to remove any entrained zinc-containing solution. This filtrate can then be returned to the metal dissolving zone for further treatment. In operations such as those involving the treatment of dilute hydroxide slurries, it may be desirable to allow the ferric hydroxide precipitate to concentrate in a settling zone prior to feeding the dissolved metal slurry into the filter.
The pH of the filtrate containing the target dissolved non-ferrous metal ions such as dissolved zinc ions, is then raised to within the range required to reprecipitate the non-ferrous metal, as by the addition of a base such as solid or liquid alkali metal hydroxide, with agitation as required. Preferred alkali hydroxides include sodium or potassium hydroxide. These reprecipitation ranges are summarized in Table II, below, for several non-ferrous metals.
TABLE II______________________________________ Reprecipitation Range (pH)Metal Useful Preferred______________________________________Zn+2 7-11 8.3-10.4*Ni+2 8-14 8.1-13.5Cu+2 8-14 8.25-13.5Cd+2 7-14 7.5-13.5Cr+3 5.75-14 6.0-13.0______________________________________ *8.5-9.5 optimal to avoid Ca+2 /Mg+2 precipitation.
When it is desired to separate zinc from nickel copper, cadmium or chromium, the latter metals can first be reprecipitated at the upper end of the given range (pH=12.0-13.5+). At this pH, zinc will remain in solution and following filtration, can be reprecipitated free of contaminants comprising both ferrous and non-ferrous metals by lowering the pH of the filtrate to about 8-11.
Following an optional settling step, the reprecipitated metal hydroxide can be isolated, e.g. be filtration, and can be reintroduced directly into the parent metal plating or similar process or further treated. For example, the zinc hydroxide and associated hydrated oxides and carbonates can be converted to zinc oxide thermally, i.e., by heating at 300�-500� C.
On the other hand, the dissolved metal concentration of the filtrate has been lowered ro the extent that it can be disposed of without further treatment. In accordance with the present invention, greater than 90% of the zinc in the slurry-starting material can be recovered in the reprecipitated cake, while less than 1 mg/liter remains in the final effluent phase.
The invention will be further described by reference to the following detailed examples.
Four one-gallon (3.8 liter) samples of an alkaline, metal hydroxide slurry were taken from the sludge holding tank of a commercial zinc electroplating operation which employs conventional pH adjustment and gravity settling to remove zinc from its total wastewater flow. The pH of each of the four samples was determined, and the samples were analyzed for total zinc, iron and for total calcium and magnesium concentration. The results of this analysis are summarized on Table III below. All procedures were performed at 21�-25� C., unless otherwise noted.
TABLE III______________________________________Waste Slurry Starting Material Analysis Calcium and Zinc Iron MagnesiumSample No. pH G/L* G/L Mole/L (EDTA)______________________________________1 9.3 4.34 1.16 .02502 8.6 2.16 2.82 .01443 10.2 3.59 1.43 .01974 9.9 3.75 0.95 .0234______________________________________ *grams per liter
Three 1000 ml aliquots of each of the four slurry samples were then employed to make up a set of twelve test samples for treatment according to the present invention as described hereinbelow.
An aqueous solution of 1.0 g of ferrous sulfate (FeSO4.7H2 O) in 10.0 ml water was added to each sample to raise the iron (II) level present. Aqueous 20% sulfuric acid (H2 SO4) was added with stirring in an amount effective to lower the pH of each sample to 4-6, to dissolve the zinc solids present. Each sample was then aerated for 60 min. at 1500 cc/min. to oxidize the iron (II) present to iron (III). The resultant solution was vacuum-filtered and the residue of hydrated iron oxide ("Fe(OH)3 ") was washed with 300 ml of deionized water and collected. The wash was combined with the filtrate.
The pH of each filtrate was adjusted to 7-11 with sodium hydroxide to precipitate the dissolved zinc and the resultant white solids were recovered by filtration in vacuo. The precipitate was washed with 300 ml of water and dried at 110� C. for 2 hours. The solid precipitate was then analyzed for zinc, iron and total water hardness factor ions (Ca+2 /Mg+2). The filtrate was analyzed for total zinc. The data obtained from these twelve runs is summarized on Table IV, below.
TABLE IV__________________________________________________________________________ RECOVERED ZINC SOLIDS ANALYSIS Original pH Used to Calcium & ZincSample No. Dissolve Zinc Reprecipitation Tot. Wt. Zinc Iron Magnesium Zinc Recovered Zinc In Final(Aliquot No.) Solids pH (grams) (grams) (grams) (Moles) (EDTA) wt. % % Filtrate__________________________________________________________________________ (mg/l)1(A) 4.3 7.4 8.05 4.21 .02 .0040 52 97 19.02(A) 4.2 8.1 4.43 2.08 .01 .0034 47 96 3.13(A) 4.4 9.3 8.23 3.49 .02 .0106 42 97 <1.04(A) 4.2 10.8 12.67 3.62 .03 .0150 29 97 <1.01(B) 5.0 7.2 9.38 4.26 <.01 .0048 45 98 27.02(B) 5.2 8.2 4.40 2.11 <.01 .0066 47 98 3.53(B) 5.2 9.8 8.61 3.44 <.01 .0114 40 96 <1.04(B) 5.3 11.0 10.71 3.58 <.01 .0182 33 95 <1.01(C) 5.5 7.4 8.95 4.10 <.01 .0056 46 94 12.62(C) 5.6 8.4 4.58 2.02 <.01 .0054 44 94 1.43(C) 5.9 9.3 7.86 3.35 < .01 .0073 43 93 <1.04(C) 5.5 10.7 10.64 3.62 <.01 .0169 34 97 1.2__________________________________________________________________________
The data summarized on Table IV indicate that in the case of samples 1A, 2A, 3A and 4A, a detectable amount of iron was found in the reprecipitated zinc solids. This is probably due to the difficulty in oxidizing ferrous to ferric ions by aeration at pH values below about 5. Thus, any ferrous ion present after aeration will be coprecipitated with the zinc in the alkalinization step. It is expected that longer aeration times or avoidance of the low end of the "zinc dissolution" pH range will prevent the pass-through of ferrous ions.
In Sample Nos. 4A, 3B, 4B and 4C, the weight percent of zinc in the recovered solid product is significantly lower than in the other samples. This coincided with significantly higher levels of hard water mineral metals found together with zinc in the recovered solid product, and indicates that the pH value used to reprecipitate the zinc should preferably be kept below a pH of about 10 to avoid the undesirable removal of hard water metal ions (Ca+2 /Mg+2) with the zinc solids. Hard water metal ions are probably removed as the insoluble carbonates and hydroxides of calcium and magnesium.
The percentage of the original zinc recovered for all samples was 93-98%. The majority of the unrecovered zinc was found by further analysis to be retained in the iron solids removed by the first filtration. It is expected that higher zinc recovery efficiencies can be attained by washing the waste iron solids with weakly acidified water (pH 4-6) and recycling the wash water in the acidification step.
The data summarized on Table IV demonstrate that the zinc values can be efficiently recovered from wastewater comprising a slurry of mixed metal hydroxides without significant contamination by iron or water hardness factor ions. Furthermore, the zinc levels in the final aqueous phase can be reduced to a level which would permit discharge of the wastewater into the environment without further treatment.
Solutions containing nickel, copper, chromium and cadmium were obtained by sampling electroplating baths containing these metals. The nickel, copper and chromium bath samples were all acid-type electroplating solutions. The nickel and copper samples also contained proprietary organic brightening agents. The cadmium bath was a conventional alkaline cadmium cyanide-based plating solution containing organic brightening agents.
Each bath sample was analyzed for plating metal concentration. A measured volume of each bath sample was then diluted with tap water to yield a 2000 ml test solution containing 10.0 g of the plating metal. This metal concentration corresponds to the concentration of metals typically found in settled hydroxide wastewater slurries (2-7 g/l).
The cadmium test solution was treated portionwise with 10% w/v sodium hypochlorite to oxidize all the cyanide ions present. The reaction end-point was determined by a positive potassium iodide starch paper test for chlorine. The chromium test solution was treated with excess 10% w/v sodium metabisulfite to reduce all the hexavalent chromium to trivalent chromium (Cr+3).
A solution of aqueous ferrous sulfate (25 ml) containing 8% w/w iron was added to each of the test solutions to ensure the presence of iron (II) in the samples.
The pH of each test solution was adjusted to 8-11 to completely precipitate the target non-ferrous metal. Within this range, all of the ferric or ferrous ions precipitate along with the target metal. The pH of all of the acidic samples was adjusted with 10% w/v aqueous sodium hydroxide. The pH of the basic cadmium test solution was lowered with 10% v/v aqueous sulfuric acid. At this point, the composition of each sample corresponded to a typical plating wastewater treatment slurry containing both non-hazardous iron solids and the hazardous "metal of value" solids in the form of insoluble hydroxides.
The pH of each test sample was then adjusted with 10% v/v aqueous sulfuric acid to 3.5-5.5 to redissolve the metal of value. Vigorous aeration and mechanical agitation was used throughout the period of pH adjustment and continued for an additional 90 minutes to complete the oxidation and precipitation of the ferrous ions which would otherwise remain in solution along with the target metal. The acidified and aerated test samples were vacuum-filtered using a Buchner funnel to remove all of the iron solids as ferric hydroxide. The isolated iron waste solids were washed with 500 ml deionized water (pH 3.5-5.0), and the wash water was combined with the filtrate.
The pH of each filtrate was raised to 8-11 by the addition 10% w/v aqueous sodium hydroxide to reprecipitate the dissolved plating metal. The precipitate was isolated by vacuum filtration using a Buchner funnel and the solids were analysed for total plating metal and for iron. The results of these analyses are summarized in Table V, below.
TABLE V______________________________________ Plating Metal SampleComponent Nickel Copper Cadmium Chromium______________________________________Starting metal 10.0 g 10.0 g 10.0 g 10.0 gRecovered metal 9.8 g 9.6 g 9.8 g 9.5 gIron in <0.1 g <0.1 g <0.1 g <0.1 grecovered solids______________________________________
The results summarized in Table V demonstrate that the present metal recovery process is effective to recover the non-ferrous metals nickel, copper, cadmium, and chromium from alkaline slurries containing the corresponding hydroxides. It was observed that the cadmium and nickel solids dissolved much more slowly than the zinc solids. Also, the nickel solids reprecipitated more slowly and over a wider pH range than did the zinc solids. However, these reaction differences would not prevent the economic application of the present recovery process to these plating metals.
The wastewater stream generated by combining the preplate cleaning, preplate stripping, plating bath and postplate chromating wastewaters from an alkaline zinc cyanide plating process was flowed into a conventional wastewater pretreatment tank system. Following destruction of cyanide, reduction of Cr(VI) and pH adjustment to 9.0, the total combined wastewater stream was transferred into a flow through gravity settling tank. The collected settled hydroxide solids were then transferred to a storage tank that holds and further concentrates the solids. The inflow to the storage tank contained 0.2-0.8% solids, while the concentrated slurry which collected in the storage tank bottom contained 1-7% solids. The storage tank overflow return stream contained less than 0.05% solids, and was gravity returned to the flow through settling tank.
The stored slurry was gravity-flowed from the bottom of the storage tank to a zinc dissolve tank. Acid was added to dissolve the zinc-containing solids, and the solution was aerated to complete the oxidation of Fe(II) to Fe(III). Acid additions were controlled by a pH receiver to maintain a pH of 5-6 at a monitor electrode. Mechanical mixing was provided by a prop mixer and aeration was provided by low pressure air through a bubbler pipe.
The solids-laden dispersion was then pumped into a chamber plate type filter press to separate the iron solids from the zinc-containing solution. The solids were automatically water-rinsed at the end of the filtration cycle and the rinse water was returned to the zinc dissolve tank. The non-toxic iron solids were manually back-washed into a sanitary sewer when the filter plates were emptied. The clear filtrate was introduced into a zinc floc tank where the pH was continuously adjusted to 8-9 to precipitate the zinc as zinc hydroxide. The zinc hydroxide slurry was pumped through a filter press to produce a concentrated, reusable zinc hydroxide filter cake. The filtrate contained less than 1 mg/l of zinc and was discarded. The zinc hydroxide filter cake was returned directly into the zinc cyanide plating solution.
The invention has been described with reference to various specific and preferred embodiments and techniques. However, it should be understood that many variations and modifications may be made while remaining within the spirit and scope of the invention.
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text:
Band of Brothers
Magazine article
By Shabi, Rachel
New Statesman (1996) , Vol. 138, No. 4958 , July 20, 2009
Kuwaiti, Salah al---Appreciation
Kuwaiti, Salah al---Family
Kuwaiti, Daoud al---Works
Kuwaiti, Daoud al---Appreciation
Kuwaiti, Daoud al---Family
Jewish Musicians--Works
Jewish Musicians--Appreciation
Jewish Musicians--Family
Middle Eastern Music--Appreciation
Middle Eastern Music--International Aspects
Article excerpt
Shlomo al-Kuwaiti first realised the scale of things on a business trip to London during the early 1990s. Sitting in a hotel lobby with a journalist friend, al-Kuwaiti, from Israel, noticed an important-looking gentleman wearing a galabeya (robe) and surrounded by an entourage of bodyguards and assistants. Informed that this man was a senior minister from Kuwait, the Israeli thought: "My name is 'the Kuwaiti'; maybe I should say something to him."
He approached the Arab minister, who asked him directly: "Are you the son of Salah al-Kuwaiti?" When Shlomo said yes, the minister grabbed him in a firm embrace. "I think there were tears in his eyes," Shlomo recalls.
This exchange between two people from countries at such odds with each other took place because of the legendary Iraqi-Jewish musicians Salah and Daoud al-Kuwaiti. Once heroes of the Gulf, they are now, in those same states, enjoying a posthumous revival.
The brothers were born in the country of their name, moved to Iraq in the late 1920s, and swiftly gained fame for their groundbreaking music. Salah composed thousands of songs that took Arab classical arrangements to a new level, earning the brothers accolades across the Arab world.
Then the brothers migrated to Israel in 1951, like thousands of other Jews whose families had been in Iraq for over 2,000 years.
"When the plane left Baghdad and flew high up in sky, my father knew his career would hit the ground," says Shlomo. Israel was--and arguably still is--dismissive of Arab culture, seen as an oxymoron and definitely not something that should represent the Zionist state.
The brothers ran a kitchen supplies shop in a Tel Aviv suburb. "But they were never traders, they were artists," Shlomo says. "Now I understand it was very sad for [my father], but he never talked to me about it at the time. He didn't want us to be hurt by his suffering."
Salah al-Kuwaiti died in 1986, ten years after his brother Daoud. …


text: I can't take my eyes off you. Screen obsessed by lassedesignen/www.shutterstock.com 27 March 2015 What if our children are the screen-obsessed couch potatoes of the future? Paul Levy, University of Brighton The evidence is growing over the psychological effects of our screen time - when will the tipping point come?


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Moen YB8000OWB Mason Series Mounting Posts, Old World Bronze - Pair (Wholesale Packaging)
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The Moen YB8000OWB Mason Series Mount Posts is a great way to add a touch of elegance to your bathroom decor. The Moen YB8000OWB Mason Series Mount Posts are great for mounting towel racks. The pro-fit installation system is also a very nice feature that eliminates set screws for faster and much more durable mounting. The Moen YB8000OWB Mason Series Mount Posts also includes a template with a built-in level. The Moen YB8000OWB Mason Series Mount Posts has an old world bronze finish and is backed by a limited lifetime warranty. This item is shipped in wholesale packaging and not retail packaging.
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Fuel Tank Location - Above Carb Level?
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Re: Fuel Tank Location - Above Carb Level?
INBOARD Gasoline tanks are required to have and anti-siphon valve
My Cal 29 A4 has no problem sucking fuel through one and it is a massive safety upgrade form hoping the carb float does not stick open
I will post some pictures tonight as I chose a 14 gallon tank in my refit due to nature of my boat use
I should also have a shot of how well my extra 6 gallon can stowed ABOVE DECK form last summers long trip
I am not sure how different the 29 and 30 are but that bump in the stern was almost designed to hold a jerry can safely
I don think you could get a fuel supply below and A4 carb it is so low on the motor
1970 Cal 29 Sea Fever
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1981 J24 Tangent 2930
Northport NY
If a dirty bottom slows you down what do you think it does to your boat
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Google's "Think Quarterly" packages some of its best data-driven marketing insights and offers it as a quarterly business-to-business online publication that, surprisingly, is also coming out in print form for a select group of marketing executives and agencies. The hard copy is intended to get the quarterly noticed, says Lisa Gevelber, Google's chief of global ads marketing.
View Full Article in:New York Times (tiered subscription model), The
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Rotating Surface Scanning Technique for Raman Spectroscopy
Volume 28, Number 3 (June 1974) Page 279-281
Zimmerer, N.; Kiefer, W.
The difficulty in recording Raman spectra of highly absorbing samples has been circumvented recently by the introduction of the rotating Raman sample technique. This technique appears to be a general solution for the study of highly absorbing materials which would decompose because of the localized heating of the focused laser beam if the conventional static excitation method were employed. Because of its simplicity the rotating Raman sample technique is very useful for laser-excited resonance Raman studies where excitation within strong absorption bands of the molecule under investigation is required. However, in some cases—for instance, at very low temperatures—it is complicated or even impossible to rotate the sample and keep it cold at the same time. Some developments have been made in this direction for moderately low temperatures.


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The spectacular and expansive Casa Piena (meaning Full House) may be located on 4.5 acres of land in San Diego, California, but the Italian-inspired estate is as authentic as they come. To say that the 39-room estate was a major "labor of love" for all parties involved during its construction could never be considered an understatement.
The 11 bedroom, 17 bathroom Casa Piena took almost 5 years to complete and brought together some of the world's finest artisans and craftsmen to create one-of-a-kind murals, wood paneling, mosaics and other high-quality handcrafted touches.
"The amazing quality of craftsmanship and attention to detail in the Casa Piena estate is unparalleled in any other property that I have had the opportunity to work on," stated Ed Earl of Priority One Properties. Earl served as the Owners Construction Project Manager for this estate and represented the homeowner in all interactions with the contractor, architect, designers and tradesman during the construction of the estate home and is now performing as the broker.
Hand forged iron gates usher visitors into the palatial estate, which is composed of four separate buildings. The main house, pool cabana, guesthouse and detached garage total 26,862 square feet under roof. Outdoor features include a sunken tennis court, 3,000+ square foot pool with exhilarating water features, a gazebo, terraced areas, an olive orchard and a private jogging trail that surrounds the estate.
The interior of this private estate showcases and array of classic details, such as carved wood moldings, solid walnut doors, elaborate beamed and hand painted ceilings, ancient stone floors, exotic wood-paneled walls, authentic Italian lighting, and imported hand-carved stone fireplaces.
The materials used for Casa Piena come from over 20 distinct countries all over the world, including Egypt, Tunisia, Madagascar, Bali, China, Brazil, Greece, Spain, Italy, France, Germany, England, Canada, and Mexico.
Old-world styling and imported materials are a large focal point of Casa Piena. Not only do they add value and a rich uniqueness to the home, but they bring all of the ease and grace of an Italian countryside villa to the lush green setting of Southern California. A historic opportunity for ownership of the Casa Piena Estate awaits. To learn more about the estate or to schedule a private tour, please visit www.mycasapiena.com
An exquisitely crafted estate that perfectly recreates gracious old world European splendor, this North Atlanta treasure is the ideal home for someone who loves to entertain on a grand scale or is seeking a quiet escape from the city's bustle.
With more than 14,300 square feet, the home has a classical layout and generous room proportions that welcomes both residents and guests, starting with a new motor court outside and a two-story marble rotunda in the grand foyer. Additional public spaces include a Versailles-inspired living room with marble fireplace or, for more casual evenings, a billiard room and lounge on the terrace level. All floors are accessible by an elevator.
Of course, the kitchen is the heart of any home, and this Country French kitchen is no exception. Equipped with double islands, two pantries, and Dacor appliances, it appeals to the home cook and the professional chef, and is complemented by a separate catering kitchen. A breakfast room and a formal dining room offer two options for meals. A newly installed wine cellar and tasting room reflects a connoisseurs' care for vintage wines.
With its elegant public face, the home has an intimate personal side, too. A library/study has a quiet fireside reading and conversation area. On the second floor, four bedroom suites open to a central family gathering area. A separate apartment is on the terrace level and includes a kitchen and living area. The breathtaking master suite is a luxurious retreat that includes a sitting area, his and hers bathrooms, and boutique-style closets and dressing rooms. Keller Williams agent Cynthia Pierce exclaims, "I could die for that closet -- it's the stuff of dreams!"
All rooms on the first floor walk out onto the veranda that overlooks the estate's custom saltwater pool and formal gardens. "The gardens have an old-world, European feel, with charming surprise nooks and retreats." Pierce says. "It's a very happy house."
On two prime gated acres inside Atlanta's Perimeter and contiguous to Buckhead, with six bedrooms, six baths and four half-baths, the estate is listed at $6,400,000. Interested buyers can contact Cynthia Pierce and 770-757-0001.
Sitting in its home park of magnificent moss- draped ancient oak trees and beautiful formal plantings of azaleas and camellias this serenely graceful antebellum manor house commands a mile of its own river frontage on both east and west sides of the Great Pee Dee River in South Carolina, a one thousand acre former rice plantation. It is no exaggeration to call Chicora Wood Plantation one of the most successful rice plantations in South Carolina of its time. In 1850 it was home-base for Gov. Robert F. Allston, who owned a network of 7 plantations along the Pee Dee River. His holdings produced more than 1.5 million pounds of rice in a years time. From 1896 to 1921 the Gov.'s daughter, Elizabeth Allston Pringle, was the last rice planter of Chicora Wood, "surviving in a man's world and in a society in upheaval". Elizabeth Pringle is known for her contribution to literature as the author of "A Woman Rice Planter"- her own account of a woman's role in daily life on a rice plantation; "Chronicles of Chicora Wood"; "Rab and Dab".
Only three families have actually occupied the plantation since it was granted to the original owner by King George second in 1732. The restoration combines all of the authentic structures with every modern amenity and comfort allowing a life style as elegant or as casual as one might desire.
A 10,000 square foot mansion. The foyer greets you with a grand staircase, a large formal drawing room to the right and an exquisite dining room to the left. Each with massive doors, ornate chandeliers and elegant fireplaces with hand-carved decorative mantels. Overlook the formal garden and the peaceful Pee Dee. The drawing room is adjoined to the library sharing a double sided fireplace. The dining room, elegantly embellished, overlooks majestic live oaks adorned with Spanish Moss. The kitchen has a cozy fireplace, abundant cabinet space and opens to a lovely breakfast room. The second floor of the main house includes the master suite, Mrs. Pringles bedroom and two guest bedrooms. A masterfully designed staircase leads to hidden attic access and the home office with the most amazing atop the oaks view to the river. The staircase is a marvel in itself as it offers "nanny windows" to the former nursery. Positioned on either side of the office are two additional bedrooms.
Behind the wall mural in the foyer you will find a passage to the original structure that was built around 1784. Descending stairs lead to an additional living area and bedroom. The second floor includes two charming bedrooms.
The 8 dependencies on the property: the Summer Kitchen, Smokehouse, Driver's House, Carriage House, Rice Threshing Mill, Shipping Barn, Slave Cabin and School House; most with original pieces of furniture or equipment and restored to their time period with the utmost care.
Over 100 acres of impounded former rice fields afford bountiful hunting opportunities. The plantation in its entirety is protected by a conservation easement with The Historic Charleston Foundation. Many of the neighboring plantations up and down river observe this protection as well, assuring that these lands will never be encroached upon by commercial development. Chicora Wood Plantation is listed on the National Register of Historic Places.
Interested buyers can contact Carol Jayroe of Prince George Sotheby's International Realty at 843-240-4492.
Half a mile as the crow flies from the Pacific Ocean, Casa Del Mar, in San Juan Capistrano, is a virtual private resort -- one and a quarter acres of palm fringed, rose scented paradise.
"This is outdoor living at its absolute finest," says Lee Ann Canaday of Re/Max Fine Homes and the Canaday Group, listing agent for the property.
Exceptionally private, the 9,000 square foot Spanish Colonial estate is a fantasy of California living, featuring spectacular ocean and mountain views from trumpet-vine twirled balconies and a central patio with infinity pool, spa, outdoor kitchen, and a fireplace to enjoy the southern California climate.
"In California you don't get a gated estate with an ocean view unless you pay $20 million," says the broker. Here you can lie in bed and watch the waves for $5.99 million. The eight bedroom, eight bath home, features formal living spaces that rival those of its Hollywood neighbors, a gourmet kitchen with crystal chandeliers and a vast Italian marble island. For casual living, there's a family room and a home theater, with theater seating, bar, and kitchenette.
The master retreat is the crown jewel, "a tranquil haven, with a marble fireplace and a balcony showcasing the hillside and ocean views," says Canaday. The bath boasts a Jacuzzi, steam shower, and sauna.
A separate 1,200 square foot, 2-bedroom casita plays luxurious host to guests.
The area is alive with history. San Juan Capistrano itself was built around the eponymous mission, a main attraction in Orange County.
Contemporary pleasures also abound, says Canaday. The city of Laguna Beach is minutes away, as is whale-watching in Dana Point Harbor, golfing on the best greens, dining at world-class restaurants, or taking a spa day at the St. Regis Resort or Ritz Carlton.
And with the freeway and train station close-by, it's a quick hop to the glitter of Los Angeles.
Interested buyers can contact Lee Ann Canaday by visiting www.canadaygroup.com.
Tucked away along the illustrious River Bend Road of Great Falls, Virginia, is a grand estate of true distinction. Newly constructed in 2012 and host to a 16,500-square-foot residence, including a guest apartment, and another 8,000 square feet of spacious outdoor living terraces on all levels around the mosaic-tiled pool, Lions Haven is a remarkable luxury retreat. Featuring six exquisitely unique bedrooms, seven full and three half baths, this stunning property of nearly five landscaped and wooded acres displays a masterful blend of refined architecture and breathtaking interior design.
The formal entertaining areas and family living spaces are all harmoniously designed to be equally opulent and comfortable by GALA Award winning Luxury Living, LLC. The home's exquisite adornments, hand-painted gold leaf wall art, expansive millwork and coffered, domed ceilings, and countless other sumptuous details will impress even the most discriminating guests. Enjoy the walnut-clad Library, Music Room and rich, gracious spaces of the Family Room and Breakfast Salon. The fully outfitted Gourmet Kitchen is a work of art unto itself. Equally luxurious Master Suites on each of the three levels provide relaxing sanctuary. The Lower Level is beautifully designed for use as a "summer house," and features a pub and wine cellar, living room, cinema room, "cigar room," billiards room, fitness room and spa… in addition to the Master suite and convenient walk-out access to the pool deck and outdoor living/dining rooms.
Offered at $7.9 million. Interested buyers can contact Fouad Talout at 703-873-3500.
Few Florida cities boast St. Petersburg's enviable mix of culture, cuisine, nightlife, and history -- along with a seven mile water park that fronts the Tampa Bay's turquoise sparkle, attracting visitors from around the world with renowned, pristine sandy white beaches moments away. Residents jog along the waterfront, walk their dogs, bike or stop to linger at myriad cafes to sip a frothy cappuccino, and enjoy the town's nearly 360 days of sunshine.
Or cheer the Honda Grand Prix on its wild ride through downtown streets each Spring.
Take a look at the Tampa Bay Times Weekend section, says Lori Famiglietti, a luxury marketing specialist with KW Luxury Homes International. "St Petersburg is the biggest small downtown there is; with almost limitless choices of things to do in a weekend, from arts festivals, antiquing, dining, music venues, attending plays to museum hopping."
A bastion of peace and luxury just minutes from downtown is Snell Isle, where quiet streets are lined with massive palms and immaculately manicured gardens surround magnificent Spanish and European-styled homes, most dating to the 1920s.
Of the premier locations on this splendid isle, Brightwaters Boulevard is the most admired. "It's where the who's who choose to live," says Famiglietti. "It's our Palm Beach."
A home to covet is Famiglietti's new listing at 925 Brightwaters Boulevard, a supremely private, Mediterranean-styled villa with a classic red-tiled roof and a grand circular drive that leads to a splashing fountain at the splendidly columned portico.
Set on more than a quarter acre, this botanical paradise of royal palms and tropical blossoms, features an enormous seaside pool, surrounded by travertine decking, and grounds that wander down to a dock and boat lift for deep water fishing.
Listed at $1.6 million, the nearly 4,000 square foot home features expansive living and entertaining spaces and French doors opening to the pool area and breezy covered lanai.
Two of the home's six bedrooms are on the main level, being utilized as a media room and office, and are also perfectly suited for a guest or in-law wing.
Hovering above it all, the fabulous second floor master suite is a world unto itself, with a beautiful private deck offering sweeping water views.
"At a great investment price of only 1.6M to be on Brightwaters Blvd", says Famiglietti, "you could love it here full-time and forever or as a second home to come and play in our cultured paradise!
Interested buyers can contact Famiglietti at 727-539-9111.
South Carolina's Hilton Head Island hosts Wexford Plantation, a premier community centered around an inland lock-controlled harbor, one of only three on the U.S. East Coast. On an island renowned for its white sandy beaches and world-class golf courses, the community is home to a newly renovated Arnold Palmer Signature Course. Also among Wexford Plantation's attributes are its distinctive houses, especially the property at 8 Plumbridge Lane.
More than 8,200 square feet, the main house reflects the area's Lowcountry architecture with two expansive front porches welcoming visitors. The foyer's curving staircase and gorgeous chandelier hint at more gracious grandeur to come. The spacious, well-appointed kitchen opens out into the inviting family room complete with a wet bar. A separate living room and a dining room allow for elegant entertaining.
The rear of the property mirrors the façade's two porches and encourages relaxed entertaining with its negative-edge pool and view of the harbor. The private dock accommodates vessels up to 72 feet.
The property's private spaces include five bedrooms. The master boasts a luxurious bathroom, which has a soaking tub, a vanity and built-in storage. There are five additional full bathrooms and two half bathrooms in the main house. A poolside guest house has its own kitchen, bath and laundry room. The property also includes a 12+-car garage and a wine cellar.
"8 Plumbridge Lane is built with the finest materials and attention to detail," says Stephen Timperman with Charter One Realty & Marketing. "Wexford Plantation's world-class amenities will exceed your expectations. What a wonderful place to call home!"
Besides its 18-hole golf course, Wexford Plantation has other recreational amenities, such as outstanding tennis facilities; harbor; croquet lawns; scenic trails; and clubhouse with a restaurant, cocktail lounge and a pro shop.
The asking price for 8 Plumbridge Lane is $3.995 million. Interested buyers can contact Steve Timperman at 800-345-2392.
*Premier French Estate
*Over 6.3 Acres
*12,213 Square Foot Main House
*943 Square Foot Detached Guest House
*Unobstructed Lake, Golf Course and Mountain Views
*Recently and Extensively Remodeled
*Completely Private
*7 Bedrooms
*8 Bathrooms plus 4 Powder Rooms
*Huge Bonus/Theater Room with Wet Bar
*Paneled Office/Library
*Two Living Rooms
*Double Island Gourmet Kitchen
*Temperature Controlled Wine Room
*Dramatic Two Story Formal Entry
*Smart Home System
*Video Surveillance Security
*Infinity Pool and Spa
*Lush Manicured Lawns
*Garages for 8 Cars
*Prestigious Guard Gated Lake Sherwood
Offered at $11,950,000. For more information, visit www.JordanCohen.com.
The old world meets the new as you enter into the elegance of this grand home through an imported antique oak door into the two-story limestone entry with imported Italian chandelier and custom designed wrought iron spiral staircase. Experience the grandeur of the formal living and dining room as you pass through the space you will be awed by the expansive views of the beautifully landscaped gardens and ocean through the beveled glass French doors.
Close to the Lodge and the Tap Room, this luxurious three-story grand estate with over 8,400 sq. ft. of living space is perfect as a primary residence or as an elegant retreat. The home features six bedrooms, four full baths, two powder rooms, five antique stone fireplaces (four dating to the 1700's), a media/library room, separate quest quarters, private offices, and a stone patio with wrought iron balcony offering views of the Pebble Beach Golf Links and Carmel Beach. In addition, there is a beautiful, private, large stone jacuzzi.
For more information, visit www.1480Padre.com.
A collaboration of the world's finest materials and a setting on 198 acres with over one mile of North River shoreline has created an estate of incomparable beauty. The estate comprises an incredible main house, a fantastic guest cottage, a poolhouse, a detached home office, and versatile hangar space for any hobby enthusiast. A masterpiece of design that has created a home of comfort, distinction, and efficiency. Easy accress to Virginia Beach, Colonial Williamsburg and Washington DC. Perfect for a corporate retreat priced at $5,999,995. Interested buyers can contact Kelly Corbett at 757-570-7860.
The remarkable Texas Hill Country creates a breathtaking backdrop to one of Texas's premier communities – Cordillera Ranch in Boerne, Texas. At Cordillera Ranch, residents enjoy luxurious and resort-style amenities such as premier golf, fine dining, an equestrian center, river club, rod and gun club, a full fitness and spa facility and hundreds of acres of community parks and trails, all within private gates of this gracious 8,000-acre community.
Residents of Cordillera Ranch enjoy close proximity to exemplary schools in the Boerne school district, as well as private school opportunities, and the ability to connect with nature while being just a stone's throw from the conveniences of neighboring San Antonio. Cordillera Ranch offers the opportunity to purchase a Master Golf membership on their famed Jack Nicklaus Signature golf course, consistently named one of Texas top 10 courses.
For someone who enjoys entertaining a luxury, yet relaxed lifestyle, real estate agent Debra Janes of KW Luxury International is marketing an ideal and newly built estate within this alluring ranch community. 207 Riverwood is situated on one of the few acreage parcels that borders the beautiful Guadalupe River. The stunning Old World Mediterranean style architecture blends beautifully with the sleek, soft contemporary flavor of the home's interiors.
Casa de Rio defines luxury and romance. 8,178-square-feet and expansive verandas offer picture-perfect hill country views overlooking tiered pools, 2 Jacuzzis and an outdoor grilling kitchen all easily accessing the river. This unique property offers an exquisitely appointed owner's retreat, epicurean kitchen for two that is open to the grand room, formal dining, wine cellar, a home theatre, 2 game rooms, 5 bedrooms and 5 ½ baths on nearly 3 riverfront acres. All of the perks of this well designed masterpiece make it a perfect fit for the buyer wanting luxury within the highly desirable Texas hill country.
Cordillera Ranch is the up and coming premier addresses in Texas offering everything for the young ... and the young at heart.
Interested buyers can contact Debra Janes at 210-573-4040 for more information.
When you bring up Maine's Sugarloaf mountain on Google Maps there's little to be seen but nature and the highest skiing mountain facility on the East Coast. Tucked in the far northwest region of the state, you will find a four season recreation center. Sugarloaf's Carrabassett Valley is at the heart of a mountain range with the steepest vertical drop on the East Coast for alpine skiers and miles of trail for cross country enthusiasts. It's a sportsperson's paradise in milder months as well, with hiking and biking, fishing, boating and excellent golf. Not surprisingly, it's also the home of the Carrabassett Valley Academy, which has schooled Olympians like Bode Miller, Seth Wescott and Kirsten Clark.
"If your family has ability and loves the out of doors, this is the spot," says Dr. Irwin, who is currently offering the Loaf's most spectacular property -- a storybook log home on a massive scale that is so extraordinary it took a masterful local craftsman over seven years to complete. Hardly child's play. Set on nearly three wooded acres with 290 plus square feet on a babbling brook, with a magnificent deck looking up to Sugarloaf Mountain, the 6800 square foot log home features three master bedroom suites, seven stone, floor to ceiling, fireplaces and two great rooms -- one styled like an English pub with a 40-inch fireplace and a game room. Amenities also include a sauna, a hot tub, and what Dr. Irwin calls a "three-season room," a screened porch in summer that becomes a glassed conservatory in chillier months. This resort within a resort offers access to the perfectly groomed cross country trails outside the front door. This beautiful on mountain home is served by a shuttle bus that passes the house every half hour for the five minute trip to the stellar slopes.
Offered at $2,167,500. Interested buyers can contact Laurent L'Heureux at 813-969-1484.
A rare opportunity to live in the most beautiful estate on Vancouver Island. This 35-acre, 20,000-square-foot oceanfront estate was lovingly designed and built be one of the world's great entrepreneurs as his own personal country estate. The estate is located along 1,200 feet of ocean frontage and 1,300 feet of river frontage. Of museum quality construction, the estate offers the buyer the opportunity to live in a work of art. Designed for grand-scale entertaining with a two-story trophy room so large that an elegant hostess could hold a fin d'siecle ball. Here, entertaining is elevated to the status of fine art. The spa wing includes an indoor pool, gym and second kitchen. The property includes a guesthouse, barns and is a very private, secluded setting, yet close to airports, shopping and the best of golf, fishing, skiing and boating. Price upon request. Interested buyers can contact Marilyn Hoffman at 214-1736 for more information.
It might seem unlikely timing, but four years ago, on the heels of the real estate fracas, Mike McCumber and Tim Savage opened the doors to Gulf Coast International Properties, a boutique luxury real estate firm specializing in high-end, water- and beach-front properties.
The partners, who had known each other for a decade, felt that "traditional real estate companies weren't offering the services or marketing programs people were looking for in the Naples real estate market," Savage says.
Gulf Coast flew in a new direction, with exceptional, personalized care. "More like advisors than selling agents -- a concierge service," McCumber explains. They combined that care with a strong Internet presence, rare at the time in Naples.
"We still invest in print advertising, there'll always be an interest in pretty pictures," says Savage. "But the future of real estate marketing and sales is in the digital space. Getting our properties in front of a guy sitting at a cafe in Toronto, looking at his tablet or smartphone. With print, there is a limited distribution, a shelf-life, a static nature to the information. Through our website, www.gcipnaples.com, and our strategic global online partnerships, like www.Invidiata.com in Oakville, ON, our properties are accessible anywhere at anytime."
Unlike traditional firms, which tend to nurture solo stars, the partners and the company's agents work as a team, in a discreet collaboration that brings agents, buyers and properties together. "We do more large deals in the conference room than through the MLS," says McCumber.
The company's primary focus is Naples, FL, with its beautiful waterways, magnificent beaches, roughly 70 golf courses and a more casual sophistication. It's an area that has long been attractive to well-to-do mid-westerners who prefer the turquoise serenity of boating on the placid Gulf of Mexico to navigating the Atlantic's tumult.
"It's much like Palm Beach, but more low-key," Savage says. "They wear flip flops -- and drive the Ferrari to buy groceries."
Located at the southern tip of Naples lies the uber-luxury community of Port Royal. Here, residents enjoy membership in the Port Royal Club with its world-class fitness center, Hydro-grid tennis courts, large beach-side pool, and charming clubhouse originally built in the late '50s.
Now showing: A magnificent three-story, five bedroom retreat featuring a two-bedroom guesthouse, pool, and exquisite grounds rolling down to 125 feet of pristine, sugar sand beach located in Port Royal.
Enough to lure any Canadian from the bistro down to the sunshine and onto the sands of Naples, Florida.
Interested buyers can click here to learn more about this property.
Long thought of as the ultimate luxury destination, Aspen, Colorado is home to a newly constructed, 18th-century-inspired, Tuscan estate.
Designed and created by Gregory "Skip" Gozzo, a noted builder with a flair for luxury and sophistication, no detail was spared in this 16,000-square-foot estate, which incorporated 40,000 square feet of hand-cut Pican limestone that is gently placed throughout the home. Mahogany flooring and doors, 10-foot tall windows, French doors, 100-year-old hand-hewn timbers, and custom-designed cherry cabinetry woodwork are also found throughout. All light fixtures and chandeliers are custom-designed and hand-made.
Within the estate, you'll find five fireplaces with handset limestone facings with true masonry herringbone pattern. Two large family rooms allow family and guests to have their own privacy and ability to spread out. Overlooking one family room is the large, gourmet and commercial-grade kitchen equipped with all the top appliances. A breakfast room overlooks the outdoor gathering area, which includes a fireplace, dining table for 12 guests, summer kitchen, fire pit, spa and waterfall.
The master bedroom has spectacular views of Owl Creek Valley, which you can see from the walkout balcony. The master bathroom features his and her vanities, an oversized shower, spa bathtub, and a ladies vanity.
Six large guest suites all have walkout patios, bathrooms with tubs and showers, oversized showerheads and walk-in closets. A caretaker bedroom suite has a full kitchen and separate entrance in and out of the estate.
Amenities include a theatre room with 120-inch projection and raised platform seating; a temperature-controlled wine cellar; a large, custom wood-paneled library with 71-inch television and bar; an exercise room with state-of-the-art equipment, steam room and shower; and a 3-car garage.
Even better, this estate is already furnished with 18th and 19th century antique furnishings from around the world. All upholstered furniture is custom-made from the framework up and includes some of the finest fabrics and leathers. All cushions are down-filled, and all bedroom headboards are custom-made from the framework up with silk linens and custom-designed bedding to accent them.
Outdoors, you'll find 5,000 square feet of patios and decks adjacent to hundreds of acres and pastures, which also has a 2-acre flat building envelope perfect for entertaining. A stream in the back of the property runs into a beautifully landscaped pond with a 15-foot waterfall. Enjoy spectacular views of the entire Owl Creek Valley, including straight on views of Mount Daly and Mount Sopris.
For more information and pictures, contact Skip Gozzo at 561-308-4367.


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A Death in Summer
By Benjamin Black
(Pan MacMillan, Paperback, 9780330539906)
Publication Date: July 2011
Other Editions of This Title: Hardcover, Hardcover, Paperback, Hardcover, Compact Disc
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Writing under the name Benjamin Black, John Banville has created a world built around a pathologist in the Dublin city morgue called Quirke. In his new novel, A Death In Summer, Quirke is brought into the case of a powerful owner of a newspaper chain who's found dead. Host Scott Simon speaks with Banville about this latest mystery. More at NPR.org
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FictionPress.com https://www.fictionpress.com FictionPress.com: Snowshinobi Story feed for writer: Snowshinobi 2015-03-29T14:36:16-08:00 tag:fictionpress.com,2015-03-29:/atom/u/834914/ Snowshinobi https://www.fictionpress.com/u/834914/Snowshinobi 2013-09-11T12:44:12-08:00 2013-09-11T12:44:12-08:00 First Flight tag:fictionpress.com,2013-09-11:story.3153048 Author: Snowshinobi
Sci-Fi
English, Rated: T
Romance/Sci-Fi
Chapters: 1, Words: 892, Reviews: 0, Rated: T, Complete
Short story-dialogue thing I wrote for two characters I'm working out, Beto and Swing. They're a pairing :3 so y'know the deal, if you're not a fan of shonen-ai here's your chance to escape, and if you're into it then cool enjoy :) I write 'wordy', editing isn't my forte o o and . . this was written at 4:00am ;. Any critiques or thoughts you have on this would make my day! Snowshinobi https://www.fictionpress.com/u/834914/Snowshinobi 2012-08-18T15:35:31-08:00 2012-08-18T15:35:31-08:00 Who's Winning Now? tag:fictionpress.com,2012-08-18:story.3051455 Author: Snowshinobi
Fantasy
English, Rated: K+
Friendship/General
Chapters: 1, Words: 1,774, Reviews: 0, Rated: K+, Complete
Summary: Honestly, Arrow. What kind of idiot do you take Delta for? You're not the only one who can win arguments, the tables are turning . . . /cover drawn by me, AkiIsAwesome42 on deviantART/ Snowshinobi https://www.fictionpress.com/u/834914/Snowshinobi 2012-06-17T10:45:48-08:00 2012-06-17T10:45:48-08:00 Two Cats and a Tape Recorder tag:fictionpress.com,2012-06-17:story.3033095 Author: Snowshinobi
Humor
English, Rated: K
Humor/General
Chapters: 1, Words: 738, Reviews: 4, Rated: K, Complete
One cat's trash is another cat's opportunity . . . Snowshinobi https://www.fictionpress.com/u/834914/Snowshinobi 2012-04-11T04:24:27-08:00 2012-04-11T04:24:27-08:00 Stardust tag:fictionpress.com,2012-04-11:story.3012566 Author: Snowshinobi
Fantasy
English, Rated: K
Hurt/Comfort/Friendship
Chapters: 1, Words: 1,193, Reviews: 3, Rated: K, Complete
Summary: Friendship is a double-edged blade . . . That sounds pretty ominous, but this is really just a fic about 2 odd characters I made up who are good friends. Songfic using the song 'Boats and Birds' by Gregory And The Hawk . More details inside!


text:
Window on Freedom: Race, Civil Rights, and Foreign Affairs, 1945-1988
The civil rights movement in the United States drew strength from supporters of human rights worldwide. Once U.S. policy makers--influenced by international pressure, the courage of ordinary American citizens, and a desire for global leadership--had signed such documents as the United Nations charter, domestic calls for change could be based squarely on the moral authority of doctrines the United States endorsed abroad. This is one of the many fascinating links between racial politics and international affairs explored in "Window on Freedom. Broad in chronological scope and topical diversity, the ten original essays presented here demonstrate how the roots of U.S. foreign policy have been embedded in social, economic, and cultural factors of domestic as well as foreign origin. They argue persuasively that the campaign to realize full civil rights for racial and ethnic minorities in America is best understood in the context of competitive international relations.
Additional information
Includes content by:Publisher:
- Brenda Gayle Plummer
- Paul Gordon Lauren
- Gerald Horne
- Carol Anderson
- Cary Fraser
- Chapel Hill, NC
- 2003
- United States--Foreign Relations--1945-1989
- United States--Race Relations--Political Aspects
- Racism--Political Aspects--United States--History--20th Century
- African Americans--Civil Rights--History--20th Century
- Minorities--Civil Rights--United States--History--20th Century
- United States--Foreign Relations--Developing Countries
- Developing Countries--Foreign Relations--United States


text:
PopUp Plus Online's New Summer Look Book
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Mason Jar Wedding Ideas
Why You Should Never Wash Your Jeans
18 of the Ugliest Leggings We Can't Believe People Actually Buy
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9 Signs You're in the Right Relationship
15 Ways to Make Your Bridesmaids Feel Special
What Are the Symptoms of Gluten Intolerance?
The Sexiest Celebrity Butts
Make Your Day Easier with These Helpful (and Hot) Products
How Work Flexibility Helps New Moms Return To Work
A Bare Feet Boho Wedding You'll Love


text:
Dec 22, 2013; Los Angeles, CA, USA; Minnesota Timberwolves shooting guard Kevin Martin (23) struggles to control the ball as Los Angeles Clippers point guard Chris Paul (3) defends during the game at Staples Center. Mandatory Credit: Richard Mackson-USA TODAY Sports
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1500 ESPN Twin Cities is giving away the ultimate Chicago Pro Draft experience.
Apollo wants you to enjoy time with your family at Cragun's! Win a 2 night stay at Cragun's on Gull...
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Hendren v. Wells Fargo Bank, N.A. et al
|Christopher Dorr, T.D. Service Financial Corporation, Wells Fargo Bank, N.A. and Wells Fargo Home Mortgage, Inc.
|Darren Hendren
|Case Number:
|July 13, 2012
|Oregon District Court
|Eugene (6) Office
|Presiding Judge:
|Ann L. Aiken
|Nature of Suit:
|Real Property: Foreclosure
|Cause of Action:
|28:1442 Petition for Removal- Breach of Contract
|Jury Demanded By:
Access additional case information on PACER
Use the links below to access additional information about this case on the US Court's PACER system. A subscription to PACER is required.
Access this case on the Oregon District Court's Electronic Court Filings (ECF) System
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text: YouTube Marketing Jobs 1,540 were found based on your criteria Post a job. It's free! Newest Jobs First Oldest Jobs First Most Employer Hours Least Employer Hours Most Dollars Paid Least Dollars Paid Highest Feedback Score Lowest Feedback Score 1 2 3 4 5 … › » Marketing expert and project lead. Must know Strategy in Google+PPC and most platforms. Hourly – 1 to 3 months – 30+ hrs/week – Posted 6 hours, 30 minutes ago I have a very interesting job for the right candidate. This is a contract position for over 3 months perhaps longer. Skills Required! Must know and be able to run multiple forms of Social media marketing. Google Adwords + PPC Campaigns- Facebook Marketing Twitter- Bing and be able to set up and administer email campaigns. This is a daily position where I will need to be communication with you every day. 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Know that social media is more than posting a cute picture it means engaging through adding conversation asking questions posting quiz and to know that its 3/1 3 either pictures, posts, quiz or questions and 1 on social proof of whatever they are promoting. facebook-marketing instagram-marketing internet-marketing marketing-strategy pinterest-marketing social-media-marketing tumblr twitter-marketing youtube-marketing P.T.-F.T. Online Marketing Assistant/Business Partner to Run Online Businesses Hourly – 3 to 6 months – 10-30 hrs/week – Posted 1 day, 12 hours ago I prefer to open this position to a M/F Filipino preferably with a College degree or have Customer Service Skills, backgrounds in Call Center experience, Network Marketing experience, SEO, Social Media Marketing. 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We are seeking someone with experience and expertise in this area and we will welcome your suggestions as to best practices and efficiency. article-writing blog-writing content-writing google-adwords internet-marketing lead-generation seo seo-backlinking social-media-marketing wordpress youtube-marketing


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XFC Opens Flyweight Division Jimmy "The Prowler" Fowler is set to make his XFC debut at the promotion's February 22 event. The Brazilian Jiu-jitsu specialist will be one half of the promotions first ever televised Flyweight matchup, where he will ... Read More »
Category Archives: press releaseFeed Subscription<
UFC on FUEL TV 7 post-fight show quotes
The following quotes are from tonight's UFC POSTFIGHT SHOW ON FUEL TV for UFC ON FUEL TV 7: BARAO VS. MCDONALD, hosted by Jay Glazer, with UFC light heavyweight number-one contender Chael Sonnen and Bantamweight Champion Dominick Cruzoffering analysis. This was the first time FUEL TV used the "Fan CAMeo," letting viewers be featured in the show. Read More »
An inside look at Roger 'The Leperchaun' Carroll
One of the most anticipated fights of the night is a Welterweight matchup between local favorite Roger Carroll and regional challenger Josh Eagans as Xtreme Fighting Championships returns to Charlotte for XFC 22: Crossing the Line on February 22. The ... Read More »
Cris Cyborg to face Ediane Gomes at Invicta FC 5
POUND-FOR-POUND SENSATION TO FACE SUBMISSION ACE EDIANE GOMES AT INVICTA FC 5 AT AMERISTAR CASINO HOTEL KANSAS CITY APRIL 5 WINNER FACES NO. 1 RANKED MARLOES COENEN KANSAS CITY, Mo. (February 15, 2013) –Pound-for-pound great and devastating featherweight (145 pounds) KO ... Read More »
South Florida's Premier Fighting Promotion CFA Brings WMMA to the MIA
Main Event Features UFC vs. Strikeforce Veterans PRESS RELEASE (Miami, FL) – Championship Fighting Alliance (CFA), S. Florida's premier MMA fighting promotion announces CFA 10 featuring UFC vs. Strikefore Veterans and the debut of the first WMMA in tournament in ... Read More »
Suzie Montero seeking Victory at XFC 22 on AXStv Feb. 22nd
Former World Combat League participant Suzie "La China" Montero will return to the cage on February 22 at XFC 22: Crossing the Line in Charlotte, North Carolina. Montero is (1-1) since turning pro, including a debut victory against XFC-vet Kim ... Read More »
Bellator Returns To The University of South Florida March 28th
Bellator Returns To The University of South Florida March 28th With Two Tournament Finals Plus the Return of World's #1 Ranked & Florida's Own Jessica Aguilar Live on Spike TV Newport Beach, CA. (February 15, 2013) – Bellator MMA will ... Read More »
World Series of Fighting 2 Kick-Off Press Conference at MMA World Expo at New York City's Javits Center
Tomorrow/Saturday, Feb. 16 at 1:00 p.m. EST WHO: Former UFC Heavyweight Champion Andrei Arlovski Hard-Hitting KO Artist Anthony Johnson Red-Hot Bantamweight Tyson Nam Two-Time National Muay Thai Champion Marlon Moraes Middleweight Star David Branch &! nbsp; Brazilian JIu-Jitsu Black Belt ... Read More »
After long layoff, Barboza returns to Twin River ready to make a major push in 2013
BARNSTABLE, Mass. (Feb. 14th, 2013) — The only thing worse than the two-year layoff for Jesse Barboza was the fact his last fight ended in a disappointing draw, leaving the former three-time New England Golden Gloves champion with a lot ... Read More »
Meet kickboxing legends from Glory 5 & 6
London, England (February 13) – Elite superstar kickboxers Remy Bonjasky, Gokhan Saki, Liam Harrison, Jordan Watson and Albert Kraus arrive in London this weekend for an exclusive Glory World Series UK debut ahead of next month's GLORY 5 LONDON event ... Read More »
Cage Fury Fighting Championships presents 'CFFX XIX: Sullivan vs. Lane' featuring three championship fights
GFL PRESENTS "REAL FIGHTS" ON COMCAST SPORTSNET CAGE FURY FIGHTING CHAMPIONSHIPS PRESENTS "CFFX XIX – SULLIVAN VS LANE" FEATURING 3 CHAMPIONSHIP FIGHTS ON COMCAST TCN AND CSN SPORTSNET BEGINNING FEBRUARY 18 New York, NY (February 14, 2013) – This weekend GFL ... Read More »


text:
My name is Mariya and I live in Switzerland for 3 years now. I work in food industry company in the area of Marketing trainings. I speak English, Spanish and a bit of German. I don't smoke, I like to take photos in the cities I visit, to learn new food recipes and to cook new Italian dishes.
Hi, I'm Ingo and I'm from Switzerland. I work in IT industry related to tourism and winter ski resorts. I speak German, English and a bit of Italian. I love coffee and pizza and wine and the "dolce vita" . I don't smoke and I like to travel and to discovery cities walking the whole time.


text:
Monday, March 30, 2015
training : web-based trainings : diabetes seminars
Upcoming Live Online Education
Join us for one-hour live online seminars that provide CME/CE credit. Presented by experts, these seminars will discuss what's new, update your knowledge and skills, and describe practical tools to use with your patients with diabetes.
Accredited Sponsors: IHS Clinical Support Center, IHS Nutrition and Dietetics Training Program, and IHS Division of Oral Health.
Join Session
Registration not required. This session will provide a review of current data on pediatric overweight and obesity and the relationship with type 2 diabetes, discussion of evidence based prevention and treatment of overweight and obesity in children, and a review of current public health approaches for intervention.
Upcoming Sessions:
Diabetes Seminar Recordings
Note: The previously recorded sessions in the table below do not offer CME/CE. To find opportunities to earn CME/CE go to the Diabetes Online CME/CE Education.
The most recent Advancements in Diabetes recorded sessions (since November 2014) offer CME/CE and can be found on the Diabetes Online CME/CE Education webpage. The sessions listed in this table are not eligible for CME/CE.
Division of Diabetes Treatment and Prevention | Phone: 1-844-IHS-DDTP (1-844-447-3387) | email@example.com
This website may require you to download plug-ins to view all content.
Accessibility · Disclaimer · FAQs · Website
Privacy Policy · Plain Writing Act · Freedom
of Information Act · HIPAA · No Fear · Glossary · Contact
Indian Health Service (HQ) - The Reyes Building, 801 Thompson Avenue, Ste. 400 - Rockville, MD 20852


text:
Gay Marriage: Historical Context
NPR continues its examination of the debate swirling around gay marriage as NPR's Margot Adler puts the issue into context, exploring the recent history of marriage and how that informs the debate on gay marriage.
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Grand Jury Will Consider Evidence Presented by State in Ferguson Shooting Case
Summary: The state will begin its presentation of evidence against a police officer that shot and killed an eighteen-year-old boy to the grand jury this week. The grand jury will determine if criminal charges will be filed. Prosecutors in St.…>read moreNo Comment August 20, 2014
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A hairstylist uses many tools: shears for cutting, brooms for sweeping, and Barbicide for killing Barbas, demon of fear. Leave it to a professional with this Groupon.
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text:
Voahausa.com - VOA Hausa
The Voice of America, which first went on the air in 1942, is an international multimedia broadcasting service funded by the U.S. government through the Broadcasting Board of Governors. VOA broadcasts approximately 1, 500 hours of news, information, educational, and cultural programming every week to an estimated worldwide audience of 125 million people.
Keywords: Voa Hausa Babban Shafi Najeriya Afirka Sauran Duniya Kiwon Lafiya Sauti Shirye-Shirye Bidiyo Sashen Muryar Amurka Africa America Global West International Media News Radio U.S. United States Voice Of World Nigeria
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The web server used by Voahausa.com is located near the city of Cambridge, USA and is run by Akamai Technologies. This web server runs a few other websites, mostly in the english language.
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