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Did You Interview With the Top Boss?
by Smart Living
Like us on Facebook
In one scene, she interviews with designer Tori Birch, who was just one of the many special guests on the episode. The interaction was sweet and emphasized how under-prepared Serena is for the working world, but I couldn't help but think it's a bit far fetched to have a major designer meet with potential intern or entry-level applicant. Did you interview with the top boss or company owner when you got your job, or did you meet with a hiring manager?
Photo courtesy of The CW
Read More Savvy PollGossip GirlInterviewBoss
Spectra 5 years
Yep, I interviewed with the Lab Director, my immediate supervisor, and the HR manager.
Advah 5 years
Yep but I'm his PA, so we sort of had to meet.
tiff58 5 years
I work for a Fortune 25 company, and entered in right out of college, so no. :)
mek123 5 years
At my current company it was a 4 step process ending with the owner/CEO.
syako 5 years
No, not for this position.In my first job there was a total of 8 employees, so after my 1st interview with the hiring manager I did interview with the CEO, but that's just because it was such a small company.
syako 5 years
No, not for this position. In my first job there was a total of 8 employees, so after my 1st interview with the hiring manager I did interview with the CEO, but that's just because it was such a small company.
kimmieb124 5 years
I had to have multiple interviews, starting with HR, moving up to the department supervisor, and finally with the big boss. That's pretty much standard where I work.
ilanac13 5 years
i didn't interview with the top boss but then again it wasn't for a position that really merited meeting with him. i think that if it was for a very senior position then i probably would have.
bellaressa 5 years
Yes, I interviewed with president, senior VP and VP.
Link Love
- How to work from home (and still get stuff done) — Real Simple
- How to find free beauty products and health services — All You
- When should you get a vacation rental instead of a hotel? — Wise Bread
- Gardening hacks from gardening experts — LearnVest
- What your desk says about you — DailyWorth
- Avoid impulse spending with this easy trick — Lifehacker
- 5 pieces of career wisdom from women who've made it — HuffPost Women
- How other people do money: kids around the world — The Billfold
- Cost of a Mad Men lifestyle — Bankrate

subset: commoncrawl


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Vendor Manager ? Localization (Part Time; Lehi, UT) Location: Lehi, UT - Remote candidates will be considered Type: Part-Time, contracted position (20 ? 30 hrs per week) Experience: Senior level Functions: Vendor Manager Industries: Translation Services Posted: Ongoing Lingotek2/23/2015 Lehi, UT Save This Job
Headquartered in Alviso, CA, Minerva is a privately owned company developing broadband television software solutions for the telecommunication, cable, satellite and enterprise markets. Job Description Play an integral role in the development and delivery of innovative2/22/2015 Alviso, CA Save This Job
Job Number:003627 Job Title:L3 Support Intern Number of Openings:1 Job Type (Employment Type):Internship Country:United States State/Province:Illinois City:Chicago Job Schedule:Part Time Level of Education:Some College Years of Experience:0 Position Description Who You Are: Do2/21/2015 Chicago, IL Save This Job
About the Job We are currently seeking an entry-level engineer or an economist with basic software knowledge who will be responsible for performing program level analytical work as well as supporting software applications used to manage programs in the area of energy efficiency2/20/2015 Madison, WI Save This Job
We're looking for Management System Software Engineers to work on application and systems management software for a large, distributed Linux-based environment. This engineer will play a central role in the re-imagining, implementation and delivery of a new, distributed management2/18/2015 Sunnyvale, CA Save This Job
JustFab, the premier online fashion styling service and lifestyle brand is looking for a QA Analyst / Test Engineer with hands-on experience testing functionality and validating e-commerce sites and systems meet design specifications and requirements documentation in an agile2/17/2015 El Segundo, CA Save This Job
Summary: MapR is looking for seasoned and passionate DevOps leader (Director of DevOps) to enable world class engineering team to deliver most innovative and open Hadoop platform. You will play hands-on role and manage the team responsible for build & release, installer2/17/2015 San Jose, CA Save This Job
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Job Description All Covered, a company of Konica Minolta Business Solutions USA, Inc. is currently seeking a Director of Service Delivery. Job Summary: The Director of Service Delivery (DSD) has the overall responsibility of all engineering resources within a geographical market.2/14/2015 New York, NY Save This Job
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Description Senior Threat Analyst Location: Sunnyvale Description We are seeking a self-starting, responsible, mature, highly motivated Senior Threat Analyst to join our growing Systems Engineering team. Candidates should be located in or near Sunnyvale, CA. In this role,12/14/2014 Sunnyvale, CA Save This Job


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Walking in the dark
Surfer Enjoying The Sunset In Imperial Beach
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Life in the bubbles!!! (Imperial Beach)
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Phenomenal picture of the IB pier!!! One of the best I've seen.
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For the love of a city.... IB IS OK!!!
IB Pier
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text:
Friday, 03 Jun 2011 06:35 AM
CHILLICOTHE, Ohio — An Ohio woman who just turned 100 years old has taken customer loyalty to the extreme: She's still using a bank savings account that's been around almost as long as she has, since the year before World War I.
June Gregg recently mentioned to a friend that her account is the same one her father opened for her in January 1913, when she wasn't even a year-and-a-half old. The friend told the people at Gregg's small-town bank in southern Ohio.
"That perked my ears up, because I was like, '1913?!'" said Doug Shoemaker, general manager of what's now a Huntington National Bank branch this community, 45 miles south of Columbus. The bank's investigation found out that not only was it the same account, but also that the account number changed only once, when Columbus-based Huntington acquired the plainly-named Savings Bank in the early 1980s, Shoemaker said.
Gregg still has the little blue passbook from when the account was opened with an initial deposit of $6.11. Her father, Gilbert, a farmer who grew corn, wheat and hay, was a Savings Bank customer and wanted his only daughter to learn thrift.
"That's what he always taught us: to stay out of debt and save our money and not buy anything until we had the money to pay for it," Gregg said in an interview.
With the help of the account, Gregg is comfortable in retirement even after so many years, Shoemaker said.
"I get along good because I don't have many wants," said Gregg, who never married and has no children.
The compact, white-haired woman who tends to speak with a chuckle in her voice retired in 1976 after working for the post office for more than a quarter century. Earlier, she operated a general store, using the savings account for the business. Gregg opened the store in 1932, three years after she graduated from high school and received as gifts a $2.50 gold piece and a $5 gold piece, which went into the account.
"I wish I hadn't put those in," she said, aware of gold's value. "It was during the Depression, and my dad told me to put them in the bank."
Gregg said she never considered taking her savings elsewhere because she liked the bank, across the street from the Ross County Courthouse. Greg McBride, senior financial analyst for Bankrate.com, said it used to be far more common for customers and families to develop long-term attachments to banks, but that was before all of today's shopping around and bank name changes.
"It seems less prevalent today because we're seeing such consolidation and so many changes in banking, and incentives for consumers to move," he said.
Though she has a checking account to pay bills, Gregg said she uses the savings account for "personal dealings" and still goes to the bank regularly, though she lives in Bainbridge, 17 miles away.
"I had to give up driving two years ago, so now I just have to go when I get a chance. I try to go once a month if I can," she said. Gregg now relies on friends to get around and walks with a cane.
The bank toasted Gregg on her 100th birthday Thursday with a party complete with balloons and a cake with large candles of the numerals "1-0-0." Bank employees sang "Happy Birthday."
"Certainly I think June takes the cake" for loyalty, Shoemaker said, while noting that there are other customers who've stayed with the bank for 30 or 40 years, sometimes more.
As a gift, the bank will bump up Gregg's interest rate for the next 100 days to around 5 percent, about 5 times the average going rate, Shoemaker said.
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text:
Bush to Scott: Push Vouchers, Sell Fla. Virtual School
Posted: 08/25/2011 - Former Gov. Jeb Bush sent Gov. Rick Scott a list of policy suggestions at the start of his tenure, according to emailed documents obtained by the Associated Press.
Posted: 08/25/2011 - Former Gov. Jeb Bush sent Gov. Rick Scott a list of policy suggestions at the start of his tenure, according to emailed documents obtained by the Associated Press.
Updated: 08/25/2011 - Casey Anthony has returned to Florida to serve a one year probation on stolen check charges. Yet the Florida Department of Corrections is keeping her exact location a secret.
Posted: 08/25/2011 - A former state welfare worker has been charged in a $1.3 million scam for stealing personal information to get food stamps, which she traded for cash.
Updated: 08/25/2011 - A Leon County deputy observed a man reach into a truck, grab a machete and then start walking towards another man who was holding a pipe wrench in the Mahan Drive Publix parking lot.
Updated: 08/27/2011 - Lemon Lane found guilty of murder, victim's family steps in to spare any possibility of the death penalty
Posted: 08/25/2011 - A 21-year-old Crawfordville man was arrested for stalking and exposing his sexual organs to a female victim in the parking lot of Wal-Mart last week.
Posted: 08/25/2011 - The ambassador of Colombia to the United States met with floral workers in South Florida advocating for passage of a free trade agreement.
Posted: 08/25/2011 - A Jacksonville man has pleaded guilty to killing his former mother-in-law.
Posted: 08/25/2011 - Police say a Miami woman faked her own kidnapping to get attention from her boyfriend.
Posted: 08/25/2011 - A man and woman in Central Florida are going to jail for manslaughter after their pet snake killed a toddler. And the man's attorney says it's all because of Florida mom Casey Anthony's acquittal.
Posted: 08/25/2011 - Grand jury indicts two in death of inmate.
Posted: 08/25/2011 - A Tampa Bay area man has been sentenced to 20 years in prison for beating his girlfriend's young daughter to death.
Posted: 08/24/2011 - Madison County Sheriff's Office investigators find a clandestine marijuana grow operation.
Posted: 08/24/2011 - Florida lawmakers will continue in the coming year to look for ways to save money in juvenile justice and prevent incarcerated kids from committing crimes again.
Updated: 08/25/2011 - The board of commissioners in Tallahassee had a full evening in its first assembly back from summer break.
Posted: 08/24/2011 - Thanks Sheriff Harvey for more than three decades of service
Updated: 08/25/2011 - A new state law, passed with only anecdotal evidence and no hard facts, isn't saving the state as much money as expected. In July the state began drug testing welfare recipients and cutting off benefits to people who fail the test.
Posted: 08/24/2011 - Feds are taking action, seizing a government computer in Santa Rosa County where GEO runs the Backwater prison.
Updated: 08/25/2011 - FDLE Deputy Commissioner replaces outgoing DOC head Edwin Buss
Updated: 08/24/2011 - On August 16th, 2011 the Grand Jurors of Gadsden County cleared Investigator Brian Alexander in the July 19th, 2011 police shooting of Carmelo Quijada.
Updated: 08/24/2011 - Goat owner wants bear-hunting legalized in Florida to stop problem
Updated: 08/24/2011 - FSU professor calls east coast quake "once in a lifetime," says chances of a quake you can feel in Florida are slim
Updated: 08/25/2011 - Eyewitness News has confirmed that 75-year old Mary Baker Vann has been located.
Posted: 08/24/2011 - A Quincy printing house has closed its doors--and the economy is to blame. And its left dozens of folks without a job.
Updated: 08/24/2011 - Florida's five water management districts have submitted tentative budgets that would slash their spending by more than $700 million, or 40 percent.


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A tour of some of the most tasteless tattoos in hockey fandom
Oct 15, 2010, 6:36 PM EDT
I've written nearly 2,000 posts for Pro Hockey Talk, followed the sport obsessively for years and basically cannot go a day without at least discussing the NHL in passing. Yet as devoted as I am to hockey, I could never imagine committing to a tattoo for the sport.
(Granted, I'm ink-free, so perhaps I'm just commitment phobic.)
Other hockey fans aren't so shy about wearing their passions on their sleeves. Literally. Marty Vance put together another great post full of horrible hockey-related tattoos today. Fair warning: his post and some of these tattoos might be a little on the "NSFW" (not safe for work) side. Here are some of the highlights … or should I say, some of the lowest of the low.
Note: all of these images came from Vance's post.
Snide remarks: Nothing says commitment (or foolishness) like getting a tattoo on your head. There's a sincere part of me that hopes this is either a Photoshop job or a temporary thing. It brings out my inner-grandparent: "How is he going to get a job?"
Snide remarks: As Vance noted, disparaging another team's logo is a clear sign of an inferiority complex. Few teams have little brother syndrome quite like the Nashville Predators do with the Detroit Red Wings. Although after being in second place for years, now they have baby brother syndrome because the Chicago Blackhawks pushed them to third place (at best). Not sure if there's enough room in the Predators' mouth for a tomahawk, though.
Snide remarks: This tattoo corners the market on obscure hockey moments. It's a reference to Max Talbot making a "shush" gesture to the Philadelphia Flyers in game six of their 2009 playoff series, after losing a fight that nonetheless seemed to rile the Pittsburgh Penguins up on their way to a comeback victory. Seems like a great idea for an avatar on Penguins blogs, but as a permanent part of your body? Dubious.
Snide remarks: Yup, that's right. Hockey sticks form the crucifix for the oddest mix of religious and puck-based devotion I've ever seen. Is this in bad taste or even blasphemous? I don't know, but I'll just go ahead and be stunned.
So, those are some of the worst hockey-related tattoos in the universe. Make sure to read the whole post to see even more ridiculous designs (and check out the previous version) and giggle at Vance's clever commentary. Again, it might be something to read once you get home from work, though.
Oh, and a word to the wise: there's nothing wrong with showing your eternal devotion to your favorite team, but be at least slightly smart about it. Keep it simple (maybe your favorite player's number, a simple puck/stick-based design or just the standard team logo) and easy to cover up for job interviews. Remember, it's cool to be super-unique when it comes to choosing a jersey to wear, but when it comes to tattoos, you're better off avoiding the road less traveled.
- kyleortonsarm - Jun 16, 2011 at 1:10 AM
For some reason I personally know three different people with the Philadelphia Eagles logo tattooed on their bodies. I'm not sure what it is about that terrible football team that demands such devotion.
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Unless otherwise indicated, the material below has not been prepared by Van Eck Associates Corporation or HardAssetsInvestor.com.
Neither assumes any liability for any content on a third-party website or material prepared by a third party.
- Alternative Energy
Jim Rogers May Buy 'A Lot' Of Gold Under $1,000
Jim Rogers: Shale Oil Industry Will Slow; Global Production & Reserves In Decline
Gold Spikes To $1,200 As Dollar Tumbles, But Is The Greenback's Rally Really Over?
Market Wrap: Gold & Oil Skyrocket As Dollar Skids After Fed Decision; NatGas Up Ahead Of Data
Saudis Signal New Oil Strategy As Production Nears Record Highs
***Top stories from the last 15 days
- Written by Brad Zigler |
- August 14, 2008
Computing Inflation In Real Time
- Details
Calls went in the opposite direction, too, as pundits tried to get their names and their quotes in print (or electrons for the digital editions) for their clip files.
It's, in a way, quaint. There's the government, dropping a pearl once a month, and there's the journos who scramble after the bauble, hold it up to the light and try to divine the health of the oyster that spawned it.
The problem is that nobody really puts much stock in the inflation numbers issued by the government anymore. It doesn't much jibe with people's lived experience, judging from the stories I hear. For the most part, hedonic pricing and the carving out of food and energy prices from "core" inflation seem to be weasling techniques meant to downplay the virulence with which prices are rising.
This morning, the BLS clocked the Consumer Price Index (CPI) rising at a 5.6% annual pace, but nobody I know buys into that.
For those who distrust the government's take on inflation, or who just don't want to wait a month for the next indication, I propose a new method: one that allows you to gauge inflation in real time from readily obtainable information.
If inflation's the loss of purchasing power metered by price changes, why not use a monetary constant like gold to take its true measure?
Gold's price is readily available as is the dollar's value against other currencies. You could, for example, keep track of the price of gold in greenbacks and in euros. The difference in the rates of appreciation (or depreciation) can give you the basis for calculating your purchasing power loss (i.e., inflation).
In May 2006, for instance, gold sold for $658 or €515. As of yesterday's morning fix, the metal was worth $817 or €549. That's 24.2% appreciation in the dollar price, but barely a 7% uptick in terms of euros. Annualizing the difference in the rates of return gives you an implied inflation rate of 13.6%.
And that, people tell me, is a much more realistic estimation of the price shocks they've countenanced recently.
Inflation Measured By Gold
(See implied inflation via gold.)
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text:
1,147 Grier City, PA Roofing and Gutter Installers and Suppliers
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Commercial Roofing, Industrial Roofing; Residential Roofing Read More
Warren Thompson & Son provides you with the best in residential and commercial roofing and siding as well as replacement windows and gutters. With over 40 years' experience as a... Read More
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Our special coverage of the closest race for years
Explore the personal stories of Syrian refugees in Lebanon
28 Aug 2013 06:43 GMT | Politics, Middle East, US & Canada, Egypt, Qatar
A fugitive leader of Egypt's Muslim Brotherhood has denied accusations that his group is committing acts of "terrorism", following the coup that toppled the country's president.
Mohammed el-Beltagy's address, which aired on Tuesday, comes as the Brotherhood plans new demonstrations to defy a crippling security crackdown that has put most of its senior and mid-level leadership behind bars.
Among those detained on Monday was 25-year-old US citizen Mohamed Soltan, the son of outspoken Brotherhood figure Salah Soltan, family and security officials said.
El-Beltagy, a former politician with the Brotherhood's Freedom and Justice Party, is wanted himself on accusations of inciting violence and has been hunted by authorities for nearly three weeks.
Live Box 201372884866233
In a videotaped message aired by Al Jazeera Mubasher Misr, el-Beltagy said that authorities were trying to turn a "political crisis" into a security problem by accusing his group of orchestrating a terrorism campaign.
Egypt's media, almost uniformly anti-Brotherhood after the closure of Islamist television stations, have described the crackdown as a "war against terrorism".
"Don't be fooled by these lies and deception that aim to label us with terrorism, violence, [and] killing ... at a time when the hands of the coup regime are drowned in blood," el-Beltagy said.
Arrests and raids
El-Beltagy went into hiding earlier this month after authorities violently broke up protest encampments held by supporters of President Mohammed Morsi, overthrown July 3 by the military after days of mass protests against him.
Hundreds died in the crackdown, including el-Beltagy's daughter.
In retaliation, Morsi supporters attacked police stations, government buildings and churches. Hundreds of Brotherhood members, the group's top leaders and Morsi supporters were arrested, many accused of orchestrating and taking part in violence.
Airport authorities also said on Tuesday that well-known Egyptian cleric Yousef al-Qaradawi, based in Qatar, would be arrested upon entry to the country.
Qaradawi is a Brotherhood ally and has spoken out vehemently against Abdel Fatah El-Sisi, the military chief who led the coup.
The current bout of violence is the worst in Egypt's two and a half years of turbulent transition. More than 1,000 people, mostly Morsi supporters, were killed in the raids and other violence since mid-August. Violence has waned in the past few days.
An official in the Interior Ministry said on Tuesday that 106 security personnel have been killed since August 14 and that more than 900 have been wounded in violence, including soldiers and policemen.
The official spoke on condition of anonymity in line with regulations.
Meanwhile, a stolen ambulance laden with explosives exploded when army troops opened fire at it before it hit a police station in the town of Sheikh Zuweyid near border with Gaza, an intelligence official said.
The remains of the three attackers' bodies were found in the wreckage, he said.
The official spoke anonymously in line with regulations.
Source: Agencies
For the Muslim Brotherhood to survive and thrive, it needs to shore up its traditional base of syndicates and students.
Politics, Egypt
As the world watches the legal proceedings against Mubarak and Morsi, we ask if their trials will be transparent or not.
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Trash is a fast-growing import in the Scandinavian country, which turns it into heat for people's homes.
Environment, Europe, Sweden
Critics say the UK's home secretary is using Muslims as a 'political punchbag' in a bid to shore up right-wing support.
Human Rights, Politics, Racism
2014 was the worst year in more than a decade for polio infections, with at least 306 new cases reported.
Polio, Asia, Pakistan
Recent court ruling finds police unit not guilty of rounding up and executing 42 Muslim men during 1987 communal riots.
Human Rights, India, Asia
Clashes continue in Yemen's coastal city, as bombing by Saudi-led coalition targets Houthis' air-defence capabilities.
War & Conflict
Egypt's president says heads of states at Arab League summit have agreed to begin forming joint unit of 40,000 troops.
War & Conflict, Politics
It is a source of sustenance but also of tension and new political realities are now increasing uncertainty.
Egypt, Sudan, Middle East
A media post-mortem into the UK's surveillance report. Plus, why five years on in Argentina the media looks so familiar.
Media, Edward Snowden, Security
The untold story of how the Lebanese community overcame the odds and found their place in multicultural Australia.
Asia Pacific, Australia, Lebanon
How to keep a telenovela profitable and demanding sponsors happy while inspiring the production team to stay passionate.
Arts & Culture, Mexico, Latin America


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Shepparton girls sweep basketball country finals
Shepparton Junior Gators completed a remarkable few months of representative basketball with victory.DAMEN FRANCIS February 26, 2013 9:20am
Shepparton Junior Gators Under-16 girls side that won the Basketball Victoria Country division two championship in Bendigo on the weekend
The spectacular success of Shepparton Junior Gators' under-18 girls team this season represents the epitome of true teamwork, coach Chris Judd says.
The Junior Gators completed a remarkable few months of representative basketball with victory in the division one grand final at the Basketball Victoria Country Junior Championships on Sunday.
Judd said it was the team's ability to work hard and seize the moment that proved the difference all weekend.
''The team worked particularly well with each other and and for each other,'' Judd said.
''Against Southern Peninsula they threw everything at us, man-to-man, a press and a zone and we just broke through all of it.
''All seven players made their contributions, even Lauren Murray and Janie (Burn) in limited minutes.''
A little bit of luck didn't hurt either.
''At the end of (grand final) game Shelby (Britten), Mikaela (Owen), Sarah (Down) and Rhianna (Barton) had four fouls each and Ash (Lancaster) had fouled out, so a few more fouls and we would have been in serious trouble,'' Judd said.
On day one, Shepparton had to get past talented opponents Warnambool and Southern Peninsula just to reach division one.
Overtime was required against Ballarat in the quarter-final and only via a Britten trey with 0.6 seconds on the clock to level scores.
Wangaratta proved no match in the semi-final, before the final against Traralgon, which ended 44-40.
The association's success continued in the under-16 girls competition, with victory in the division two final.
Shepparton crushed Sale in its opening game, but came up short against powerhouse associations Geelong and Southern Peninsula on day one.
The results left the Gators third in pool C and earned them a spot in the division two quarter-final, where they beat Swan Hill, before accounting for Warragul and Maffra in the semi-final and grand final respectively.
Prior to the weekend coach Tony Long said he would be satisfied with a division one appearance or victory in division two and he stuck by that.
''The girls played really well, they pushed Geelong and Southern Peninsula all the way, they were just not quite good enough to get over the line,'' Long said.
''The grand final was tough, because Maffra had played one less game, but the girls hung tough and it was a top effort.''
Genna Ogier was the stand-out player for the team, of which most will move on to under-18s next season.
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In awe of Rumma
More heroics from Ramadan Yze secured Central Park-St Brendan's a ninth Haisman Shield in 11 seasons yesterday.
Lakers crash out of finals
The Yarrawonga Mulwala Cricket Club A Grade team lost its semi-final clash against Bruck on the weekend, bringing to an end their 2014-2015 season.
VIP guest at Guides
On March 5, Member for Northern Victoria Wendy Lovell visited the Tatura Guides, to speak about leadership and also of her experiences when she was a Guide.
Echuca Cup star jockey in critical condition after fall
Jockey Jack Hill was airlifted to a Melbourne hospital on Friday after falling from The Muckle Toon during Race 4 at Donald.
Team time trial arrives
The 28th Fleche Opperman 24-hour team time-trial finished in Rochester last Sunday as exhausted cyclists rolled into town shortly after sunrise.
KLTC's winning weekend
Two teams, two premierships for Kyabram
Taking a stand against cyber-bullying
A new project developed by Mitchell Shire Youth Council members.
Piano concert in Deniliquin tonight
Leading concert artist Daniel de Borah will perform in Deniliquin tonight as part of the South West Music 2015 concert series.
Support school's anti-bulling day
Heathcote Primary School students are asking the community to show their support for student efforts to stamp out bullying.
Putting the fun in funraiser
Cobram District Health Ladies Auxiliary continue fundraising for the hospital.
Piano concert in Deniliquin tonight
Leading concert artist Daniel de Borah will perform in Deniliquin tonight as part of the South West Music 2015 concert series.
'Disappointed' by government on procurement
Peter Kelly has ended his reign as general manager of SPC with one major battle unfinished: convincing governments to purchase Australian-made food.
Our Paul Kelly
Benalla GP Paul Kelly receives an award in recognition of his 37 years as a doctor in rural Victoria.
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Town Square
Berlin Wall sections unveiled at library
Original post made on Nov 18, 2013
Read the full story here Web Link posted Saturday, November 16, 2013, 11:14 PM
Comments (1)
a resident of Bailey Park
on Nov 18, 2013 at 10:52 am
The only other sections of the Berlin Wall in Norcal are in Monterrey. There are only 60-something in the US.
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Continuation of Office Cap Discussion
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Welcome to a free stock market game from MarketWatch.
With VSE you can:
- Trade stocks in Real-time using your virtual portfolio
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News & Tools
- StubHub files antitrust suit against Ticketmaster
- [DJIA] Dow at session highs after adding 270 points
- China's curiously pain-free banking
- Pending home sales in February climb to 20-month high
- Greek market drops as deal talks flounder; Europe stocks up
- If the Fed doesn't hike rates, it will be due to one of these charts
- Apple's Tim Cook calls 'religious freedom' law dangerous
- The market in a minute: A short but critical week
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Stocks to WatchDuPont, Nike, KB Home are stocks to watch
Among the companies whose shares are expected to see active trade in Friday's session are DuPont, Nike, and KB Home.
The StockpickersIliad to forge ahead with T-Mobile bid
Collapse of Sprint offer may strengthen Paris telecoms operator's hand.
The Ratings GameKraft-Heinz deal seen as expensive
In Kraft, 3G Capital Partners is buying a business that has missed Wall Street's consensus on sales in eight of the last 10 quarters and is losing market share in key categories.


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City of Wilmington considering spending $3.5 million or more to buy downtown propertySubmitted by WWAY on Fri, 11/08/2013 - 12:31am.READ MORE:
Two days after the municipal election, the City of Wilmington announced it is negotiating with Chuck Schoninger and Riverfront Holdings II, LLC to possibly buy land on the northern downtown riverfront for a "passive waterfront park." The proposed park would be between 6 and 7 acres and would cost the city between $3.5-$4 million, according to a city spokeswoman. Full story...»
YOU MAKE THE CALL: Was traffic stop of city employee handled properly?Submitted by WWAY on Thu, 08/22/2013 - 11:59pm.READ MORE:
Often in newsrooms there are stories that lead to debate: Is it news or not? Will viewers want to see it, or should they see it all? Tonight, we ask you to be the judge. Full story...»
Hundreds of jobs possibly coming to WilmingtonSubmitted by Sarah Murphy on Wed, 08/14/2013 - 5:21pm.READ MORE:
Wilmington's economy could see a boost in the near future. Wilmington Business Development says it is in the early stages of courting a major company to the Port City. Full story...»
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Jonathan Adler is known for a design aesthetic that combines bold colors, modernistic forms and groovy retro patterns. One of the country's leading interior designers, Jonathan Adler has also been the lead designer for Bravo's "Top Design" series and creates lighting for Robert Abbey.
The Claridge Mini Teardrop Accent Lamp is available with the following:
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احلي كس في زبر بنت بنوت Those Its been a tough road for racers lately, so I`m super excited for Erica Enders getting back to the Pro Stock arena.
This move was similar to that taken by ADV Films several years before with several of the major torrent sites. سكسي تركي in whatever way you want, knowing that if the news have changed or if you saved your Newsfeed settings since the last time the script was called, it will return the number of news items you specified with the format you specified.
A show getting green-lit depends entirely on the show`s ability to find a sponsor.6 seconds at more than 330 mph, slightly slower than a Top Fuel dragster.
احلي كس في زبر بنت بنوت Think about one piston in a gasoline engine. Which is why I`m really excited that the other Erica racing is not only driving a Mustang this year too, but has gone with a Black/Pink color scheme for her DragStar Pro Stock ride. سكس فديو مبشر The National Cosplay Championship will also be officially launched in Melbourne on 27 March at the Supanova pop culture expo. Cosplay or Costume Play is a pop culture phenomenon in which aficionados gather in groups, dressed in elaborate - usually handmade - costumes inspired by characters or themes from their favourite anime {Japanese animation}, manga {Japanese comic books}, graphic novels and video games.
One of the biggest things I`ve missed is my signature Black & Pink racecar paint jobs.Can consumer-generated media {CGM} work as a monetizeable business model for video like it has for text? What are the challenges with incorporating video into public Wikis? And, can traditional news companies use the wiki model for incorporating CGM video and build back their own news communities, or are the challenges too great?However, traffic and consumer activity doesn�t equate profit. Those Its been a tough road for racers lately, so I`m super excited for Erica Enders getting back to the Pro Stock arena.


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The Plan: Gospel Coalition Booklets -eBooks
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Product Information
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Vendor: Crossway Books & Bibles
Publication Date: 2011
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Series: Gospel Coalition Booklets
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Publisher's Description
From eternity past God has had a perfect plan for the world. The Fall and entrance of sin into the world did not surprise him, nor did it detract from his plan. All things have been sovereignly worked to this end. What exactly is this plan, and where do we learn about it?
In this new booklet from the Gospel Coalition, Colin Smith demonstrates that Gods plan is shown in the Bible and centers around his promise to bring sinners to eternal life, through Christ, for his glory. The Old Testament tells the story of the making of the promise, which is fulfilled in the life, death, and resurrection of Jesus Christ. Gods people, the church, spread the good news of this promise to the world, and the Holy Spirit is given to believers as the seal of the promise.
The Plan offers a thoughtful explanation for point 5 of the Gospel Coalitions confessional statement. The Gospel Coalition is an evangelical renewal movement dedicated to a scripture-based reformation of ministry practices.
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PHOENIX – Having an off night offensively, Maya Moore still found a way to help her team win.
Moore was 3 of 12 from the field before she made a three-pointer, stole an inbounds pass and made a layup in the final minute to lift the Minnesota Lynx to their sixth straight victory, an 82-77 victory over the Phoenix Mercury on Sunday.
"I'm always trying to find a way to stay involved and help my team win," Moore said. "I never give up, I don't like to give up on my team and I could have easily just let it get to my head and gotten frustrated. But our team has done such a good job of picking each other up."
Moore finished with 14 points on 5-for-14 shooting, Rebecca Brunson had 18 points and 13 rebounds, and Seimone Augustus scored 15 points for the Lynx, who have won eight of their last nine. Minnesota made 4 of 6 free throws in the final 19 seconds to secure the victory, its ninth straight against Phoenix.
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Diana Taurasi had 26 points, six rebounds and six assists for the Mercury, which led much of the game.
Other games
At Shock 90, Dream 63
Glory Johnson collected 24 points and 10 rebounds and Liz Cambage added 23 points and 15 rebounds as Tulsa extended its winning streak to a season-high three with the victory over Atlanta.
The Dream lost its fourth straight game after having won six in a row.
Fever 65, at Mystics 52
Tamika Catchings had 23 points and 10 rebounds as Indiana swept a home-and-home series from Washington.


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17 Aug 2009
Verdi: Luisa Miller
On a good night an opera performance can come across with visceral excitement without a classy production, top-name singers, or the benefit of being of one of the more familiar titles.
Nixon in China is a three-act opera with a libretto by Alice Goodman and music by John Adams that was first seen at the Houston Grand Opera on October 22, 1987. It was the first of a notable line of operas by the composer.
It is thanks to Céline Ricci, mezzo-soprano and director of Ars Minerva, that we have been able to again hear Daniele Castrovillari's exquisite melodies because she is the musician who has brought his 1662 opera La Cleopatra to life.
Lyric Opera of Chicago, in association with the Royal Opera House, Covent Garden, has staged a production of Richard Wagner's Tannhäuser with an estimable cast.
Puccini and his fellow verismo-ists are commonly associated with explosions of unbridled human passion and raw, violent pain, but in this revival (by Justin Way) of Moshe Leiser's and Patrice Caurier's 2003 production of Madame Butterfly, directorial understatement together with ravishing scenic beauty are shown to be more potent ways of enabling the sung voice to reveal the emotional depths of human tragedy.
Rarely, very rarely does a Tosca come around that you can get excited about. Sure, sometimes there is good singing, less often good conducting but rarely is there a mise en scène that goes beyond stock opera vocabulary.
The Nash Ensemble's 50th Anniversary Celebrations at the Wigmore Hall were crowned by a recital that typifies the Nash's visionary mission. Above, the dearly-loved founder, Amelia Freeman, a quietly revolutionary figure in her own way, who has immeasurably enriched the cultural life of this country.
On March 7, 2015, Arizona Opera presented Dan Rigazzi's production of Die Zauberflöte in Tucson. Inspired by the works of René Magritte, designer John Pollard filled the stage with various sizes of picture frames, windows, and portals from which he leads us into Mozart and Schikaneder's dream world.
There are some concert programmes which are not just wonderful in their execution but also delight and satisfy because of the 'rightness' of their composition. This Wigmore Hall recital by soprano Carolyn Sampson and three period-instrument experts of arias and instrumental pieces by Henry Purcell was one such occasion.
It has been a cold and gray winter in the south of France (where I live) made splendid by some really good opera, followed just now by splendid sunshine at Trafalgar Square and two exquisite productions at English National Opera.
At long last, Rise and Fall of the City of Mahagonny has come to the Royal Opera House. Kurt Weill's teacher, Busoni, remains scandalously ignored, but a season which includes house firsts both of this opera and Szymanowsi's King Roger, cannot be all bad.
RILM Abstracts of Music Literature is an international database for musicological and ethnomusicological research, providing abstracts and indexing for users all over the world. As such, RILM's style guide (How to Write About Music: The RILM Manual of Style) differs fairly significantly from those of more generalized style guides such as MLA or APA.
Unsuk Chin's Alice in Wonderland returned to the Barbican, London, shape-shifted like one of Alice's adventures. The BBC Symphony Orchestra was assembled en masse, almost teetering off stage, creating a sense of tension. "Eat me, Drink me". Was Lewis Carroll on hallucinogens or just good at channeling the crazy world of the subconscious?
Dominic Cooke's 2005 staging of The Magic Flute and Richard Jones's 1998 production of Hansel and Gretel have been brought together for Welsh National Opera's spring tour under the unifying moniker, Spellbound.
Carolyn Sampson has long avoided the harsh glare of stardom but become a favourite singer for "those in the know" — and if you are not one of those it is about time you were.
Gaetano Donizetti and Malcolm Arnold might seem odd operatic bedfellows, but this double bill by the Guildhall School of Music and Drama offered a pair of works characterised by 'madness, misunderstandings and mistaken identity' which proved witty, sparkling and imaginatively realised.
Saturday, February 28, 2015, was the first night for Los Angeles Opera's revival of its 2009 presentation of The Barber of Seville, a production by Emilio Sagi, which comes originally from Teatro Real in Madrid in cooperation with Lisbon's Teatro San Carlos. Sagi and onsite director, Trevor Ross, made comedy the focus of their production and provided myriad sight gags which kept the audience laughing.
Commenting on her recent, highly acclaimed CD release of late-nineteenth-century song, Chansons Perpétuelles (Naive: V5355), Canadian contralto Marie-Nicole Lemieux remarked 'it's that intimate side that interests me I wanted to emphasise the genuinely embodied, physical side of the sensuality [in Fauré]'.
An evening of strange-bedfellow one-acts in high-concept stagings, mindbogglingly delightful.
On February 19, 2015, Pacific Symphony presented its annual performance of a semi-staged opera. This year's presentation at the Segerstrom Center for the Arts in Costa Mesa, California, featured Georges Bizet's Carmen. Director Dean Anthony used the front of the stage and a few solid set pieces by Scenic Designer Matt Scarpino to depict the opera's various scenes.
Although the English National Opera has been decidedly sparing with its Wagner for quite some time now, its recent track record, leaving aside a disastrous Ring, has perhaps been better than that at Covent Garden.
On a good night an opera performance can come across with visceral excitement without a classy production, top-name singers, or the benefit of being of one of the more familiar titles.
Such is the case with this Luisa Miller, staged at the Teatro la Fenice in 2006 and released by Naxos. The singers, in modern dress, perform on abstract sets dominated, for no clear reason, by photographic reproductions on flat columns. The title role is taken by Darina Takova, a hard-working singer but not a star. Her tenor, Giuseppe Sabbatini, has had some big nights in opera houses (and days in the recording studio) in his career, without ever quite establishing himself in the top rank. The rest of the cast even fewer may know of. The opera itself is not Verdi's most consistently inspired score, though he was approaching his artistic maturity and the music always serves its dramatic purpose - as melodramatic as that may be in Salvatore Cammarano's adaptation of a Friedrich von Schiller play. But it all comes together, under director Arnaud Bernard and conductor Maurizo Benini's leadership (on stage and in the pit, respectively). It may not be pretty, but it's an exciting, engaging Luisa Miller.
What director Bernard wanted from Alessandro Camera's sets remains unclear - perhaps he simply asked for a prop-less space and had only the budget for the rudimentary backdrops that Camera provides. At least the Count's home has more of a frame of reference, with the cool lighting (unceredited in the Naxos booklet) outlining a formal space, rather like an underpopulated hospital lobby. The first scene establishes Bernard's style. As the chorus tries to awake the sleeping Luisa, she lies prone on the stage, with the chorus hovering over her. The vague ominousness of the image foreshadows the cruel and sad events to come, as Luisa is forced to lie and renounce her lover Rodolfo to save her father, because the Count wants his son to marry one Federica. To enforce his nefarious plan, the Count employs Wurm, portaryed with relish by the tall, glowering Arutjun Kotchinian (sene last season in San Diego Opera's Rigoletto as Sparafucile). Kotchinian has the look, sure, but most importantly, he has the voice - a palpably dark and heavy bass. The La Fenice audience shows him its appreciation at final curtain.
They also warmly applaud Luisa's father, handsomely sung by Damiano Salerno. All the darker voices impress: Ursula Ferri makes the most of her moments as Federica, and Alexander Vinogradov schemes impressively as the Count.
The leads get big hands too, of course. Rodolfo may be on the heavy side for Sabbatini, but at this point in his career he has the experience and colors to succeed. His act two aria, probably the score's best known number, goes very well. Takova needs some time to warm up, and she has some challenging music in the first act. After that, she takes command. The drama of the last two acts suits her strong voice, and though she may not look like the youngest daughter the miller could have had, she gets to the heart of the role.
Maurizo Benini supplies tension and drive in the pit, and the Naxos sound - perhaps because the performance is spread over two discs - is remarkably clear and dynamic.
Some may object to the updating, and admittedly, the production can fairly be called drab. But the performance succeeds nonetheless, and as Luisa Miller doesn't come around all that often, opera fans trying looking for some distraction this summer should check out this Naxos set.
Chris Mullins


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February 11, 2013
Gap's results improve with its fashion sense, WSJ reports
Finally, Gap (GPS) is retaking lost ground, reports the Wall Street Journal. The company's latest fiscal year showed upward improvement, the result of an improved fashion sense that involved colorful jeans and sleek, "Mad Men"-style suits. Gap reported an 8% increase in January sales, excluding newly opened stores, and completed the 12 months ended February 2 with $15.7B in net sales, up 6.4% from $14.7B a year earlier. Over the past year, the company's shares are up almost 50%.
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Sales director jobs
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Utilities Sales Director IT Services
- London, Birmingham, Manchester
- £100,000- £120,000 plus substantial bonus
Major new leadership opening in premier high growth IT services and outsourcing player.
Utilities Sales Director BPO
- London, Birmingham, Manchester
- £100,000- £120,000 plus substantial bonus
Key influential leadership role in well-established global IT Services and outsourcing player.
Sales Director (Public Sector)
- London (Central), London (Greater) (GB)
- Circa £100,000 basic (£200,000 OTE)
Sales Director required for a charity subsidiary created to generate significant new revenues by selling existing assets to wider customer base
Sales Director
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An opportunity to spearhead new business acquisition in a fast growing, ambitious marketing services organisation.
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Our client is a global provider of IT software services to a wide variety of business markets. Due to continued expansion they wish to appoint a Sa...
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- £80,000 - £90,000 per annum + full executive package
UK Sales Director - Rail (New Equipment & Maintenance) has arisen within a leading manufacturer of systems for rail rolling stock applications.
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Our client is a nationally operating premium branded high-street retailer with significant Private Equity backing and an ambition for growth.


text:
In the production of organochlorosilanes by reaction of silicon with an alkyl- and/or arylchloride in the presence of a copper catalyst and, optionally, promoter elements, the improvement wherein the silicon has been atomized with an inert gas, has a particle size of less than about 1000 μm, by weight has an Al content of about 0.05 to 0.38%, a Ca content of about 0.02 to 0.2% and an Fe content of about 0.25 to 0.55%.
1. In the production of organochlorosilanes by reaction of silicon with an alkyl- and/or arylchloride in the presence of a copper catalyst and, optionally, promoter elements, the improvement wherein the silicon has been atomized with an inert gas has a particle size of less than about 1000 μm, by weight has an Al content of about 0.05 to 0.38%, a Ca content of about 0.02 to 0.2% and an Fe content of about 0.25 to 0.55%.
2. A process according to claim 1, wherein the atomized silicon is a Si/Cu alloy atomized with an inert gas.
3. A process according to claim 2, wherein the inert gas is nitrogen.
4. A process according to claim 1, wherein the silicon before atomization contains promoter elements.
This invention relates to a new process for the production of organochlorosilanes by reaction of silicon atomized with inert gas with an alkyl- or arylchloride in the presence of a copper catalyst and promoter elements, More particularly, the invention relates to a process for the production of methylchlorosilanes.
The basic process for the production of methylchlorosilanes is the direct reaction of finely divided, ground silicon with methylchloride in the presence of metallic copper or, occasionally, silver as catalyst. The reaction is known to the expert as "Rochow's synthesis" and is described in U.S. Pat. No. 2,380,995.
A mixture of the following silanes (Me=CH3) is mainly obtained in this process: Me2 SiCl2, Me4 Si, Me3 SiCl, MeSiCl3, SiCl4, HSiCl3 3, MeHSiCl2 and MeHSiCl. In addition to the monomeric methylchlorosilanes mentioned, higher-boiling compounds, such as for example methylchlorodisilanes, methylchlorotrisilanes, disiloxanes and silmethylenes, are also formed in relatively small quantities. In general, it is the monomeric compounds which are industrially used, dimethyldichlorosilane being of particular interest. Accordingly, it is desirable to obtain this preferred reaction product with the highest possible selectivity, a measure of selectivity being inter alia the ratio of MeSiCl3 to Me2 SiCl2 (the so-called tri:di ratio), the value of which should be as small as possible.
On an industrial scale, particular emphasis is placed on the production of methylchlorosilanes by reaction of methylchloride with silicon in a fluidized-bed reactor, methylchloride used in excess serving both as reactant and as fluidizing medium.
Since the first investigations about 40 years ago, there have been several publications describing processes for carrying out the reaction, for improving selectivity, for the production of suitable catalysts and catalyst/promoter systems. A first comprehensive review can be found, for example, in "Organohalosilanes: Precursors to Silicones", Voorhoeve, Elsevier Publishing Company, Amsterdam/New York/London, 1967.
The most recent works have concentrated mainly on the specific use of trace elements, so-called promoters, in the catalyst system, cf. for example DE-A-3 425 424, EP-A-138 678, EP-A-138 679, DE-A-3 501 085, EP-A-191 502, EP-A-194 214, EP-A-195 728, EP-A-223 447.
Comparatively few publications relate to the silicon and, when they do, are concerned with purity requirements and physical parameters, such as particle size distribution. For example, U.S. Pat. No. 3,133,109 states that particle sizes in the range from 20 to 200 μm are suitable for the optimal operation of a fluidized-bed reactor. In U.S. Pat. No. 4,500,724, silicon smaller than 700 μm is regarded as suitable, the mean particle size being said to be in the range from 20 to 300 μm and preferably in the range from 100 to 150 μm. The limits mentioned above count generally as state-of-the-art and experts know that the particular optimum is closely related to the particular reactor system used.
Now, the present invention relates to a process for the production of organochlorosilanes, characterized in that silicon which has been produced by atomizing with an inert gas or a suitable alloy of silicon which has been produced by atomizing with an inert gas is used, having thus been brought into a finely divided form in which it may directly be used for the production of organochlorosilanes.
The silicon atomized with an inert gas has a particle size of from 0.1 to 1000 μm, a specific BET surface of from 0.001 to 1 m2 /g and a chemical composition of (in % by weight) 0.05-1% Fe; 0.01-1% Al; 0.0001-1% Ca; 0-8% Cu; 0-1% Zn; 0-1% Sn; 0-0.5% B; 0-0.5% P; 0-0.5% Na; 0-0.5% Li; 0-0.5% K; 0-0.5% Mg; 0-0.5% Sr; 0-0.5% Ba; 0-0.5% Be, remainder silicon (or optionally other impurities in small amounts).
The silicon preferably contains 0.05-0.38% Al, 0.02-0.20% Ca and 0.25-0.55% Fe.
The atomizing of metals is a standard process for the production of metal powders and has long been applied, for example, to such metals as copper or its alloys.
In most cases, metal powders produced in this way are further processed by standard powder-metallurgical techniques into shapes having particular properties; cf. Ullmanns Encyclopadie der technischen Chemie, 4th Edition, Vol. 19, page 566, Verlag Chemie, Weinheim, 1980.
In the atomizing technique, extremely short solidification and cooling times for the silicon are essential. It is also crucially important that the Si powder be atomized with an inert gas, for example nitrogen.
The fact that starting material thus produced shows considerably higher reaction velocity in the synthesis of organochlorosilanes is completely surprising and new.
For the synthesis of methylchlorosilane, the process according to the invention is carried out by reacting atomized silicon having a purity of greater than 98.5% and a particle size below 1000μ and preferably below 500 μm with methylchloride in the presence of a mechanically prepared mixture of copper catalyst and promoter elements. The process according to the invention is preferably carried out in a fluidized-bed reactor because by far the most favorable yields of desired product are obtained in this way and processing advantages, for example high heat transfer, can also be utilized.
In another preferred embodiment of the process, a silicon/copper alloy which has also been obtained by atomizing in an inert gas is reacted with methylchloride.
So-called promoter elements, providing they are used in metallic form, may of course also be added to the alloy to be atomized or may even be mechanically mixed with the atomized silicon/copper alloy.
In the latter case, a fluidized-bed reactor is again preferably used to carry out the reaction.
The silicon used in the process according to the invention has a purity of more than 98.5% Si and preferably more than 99% Si. It is particularly important that the Pb content of the silicon should not exceed 10 ppm. Since the reaction is preferably carried out in a fluidized-bed reactor in the process according to the invention, considerable significance is attributed to the physical properties of the silicon, such as for example its particle size distribution, in addition to its chemical properties. The silicon particles should generally be smaller than 1000μ and are preferably smaller than 500 μm, a particle size distribution of 30 to 300 μm for a mean particle size of 100 to 150 μm being particularly preferred.
The above-mentioned range for the preferred particle size distribution also applies to a suitable atomized silicon/copper alloy.
In the preferred embodiment of the process according to the invention for the production of methylchlorosilanes, 0.5 to 8 parts and preferably 1 to 3 parts catalyst/promoter mixture can be used to 100 parts silicon metal. However, this range may be varied within wide limits because the reaction is normally carried out continuously, rather than discontinuously, in a fluidized-bed reactor.
If an atomized alloy is used in accordance with the invention, its composition is selected as follows:
Si: 90 to 99% by weight
Cu: 0.5 to 8% by weight
An atomized alloy and atomized silicon may of course both contain the typical impurities known to the expert, such as Fe, Al, Ca, Ti, etc., within the limits indicated above.
According to the invention, suitable promoter elements may be added to the melt to be atomized. Promoter elements are known to the expert, cf. the literature cited hereinabove where the elements zinc, tin and phosphorus are mentioned in particular.
The process according to the invention is carried out at a temperature in the range from 250� to 350� C. and preferably at a temperature in the range from 280� to 330� C.
It is advisable to carry out the process under a pressure above atmospheric pressure because the volume/time yield is increased in this way.
An excess pressure of up to 10 bar is advisable, an excess pressure of up to 5 bar being best.
These conditions provide for optimal selectivity in regard to the formation of dimethyldichlorosilane. In addition, it is possible in this way to obtain an optimally controllable reaction velocity.
The gaseous methylchloride is used in a large excess in the reaction because it is passed continuously through and fluidizes the catalyst mass of silicon metal particles and the catalyst/promoter mixture or through the atomized alloy.
The expert knows that it is not essential to use fluidized-bed reactors, particularly on a laboratory scale; instead it is common practice to use reactors in which the catalyst mass is vibrated during the reaction or is kept in motion by means of a helical stirrer to avoid local overheating and to guarantee safe conduct of the reaction.
As the numerous publications cited above show, attempts have hitherto been made to improve not only the selectivity, but also the yield of dimethyldichlorosilane via the catalyst/promoter system. However, it was found that the reaction velocity is also very sensitive to promoters and inhibitors. Thus, the invention according to DE-OS 3 425 424, page 10, is also concerned with the considerable increase in the rate of formation of dimethyldichlorosilane.
All the more surprising was the fact that the method by which the silicon is size-reduced (atomizing as opposed to grinding) should play such a key part. This effect is surprising and new.
The process according to the invention may of course also be used for the production of other organochlorosilanes. Any changes which may have to be made to the process parameters are familiar to the expert.
The invention is illustrated by the following Examples.
All the following experiments were carried out in a stirred-bed reactor of glass (internal diameter 30 mm) equipped with a helical stirrer. The same quantity of silicon or silicon/copper alloy having the same particle size distribution of 71 to 160 μm was used in every experiment. Methylchloride was passed through the catalyst mass from below through a glass frit under a pressure of 2 bar. The quantity of methyl chloride was kept constant and, in every case, amounted to approximately 1.5 l/h at 2 bar. After heating up and initiation of the reaction, a stationary experimental phase was established at 300� C. and the quantity of crude silane mixture formed per unit time was determined under the conditions thus established. The values shown are all mean values of four individual measurements under constant boundary conditions of 2 bar, 1.5 l/h methyl chloride and 300� C.
The catalyst mass consisted of 40 g silicon, 3.2 g copper catalyst and 0.05 g ZnO and was homogenized before use. The same catalyst was used in every case. Samples A and B are commercial silicon powders of different origin produced in the usual way by grinding. Sample C is a silicon powder produced by atomizing with nitrogen.
The following production rates in g/h crude silane mixture are obtained under comparable reaction conditions (2 bar, 1.5 l/h MeCl and 300� C.):
A: 5.7 g/h
B: 5.2 g/h
C 8.3 g/h (over a period of about 8 hours),
which corresponds to an increase in the production rate of approximately 45 and 56% through the use of atomized material.
An alloy produced by atomizing and having the following composition:
Fe: 0.34; Al: 0.40; Cu: 5.75; Zn: 0.14
(plus other non-analyzed impurities)
was reacted in the reactor described in Example 1 under the same conditions (2 bar, 1.5 l/h methyl chloride, 300� C.). In two experiments, the production rates of 8.13 g/h and 9.4 g/h were again distinctly above the otherwise typical production rates of 5 to 6 g/h.
Example 3 is intended to show that the rapid cooling is crucially important to the production rate.
Sample C of Example 1 is compared under the reaction conditions described above with a sample D of the same atomized material which has been subjected to a heat treatment before use in the direct synthesis. To this end, the sample--fused in vacuo in an ampoule--was heated for 2 hours at 1000� C. and then slowly cooled again over a period of another 6 to 8 hours.
Under the reaction conditions mentioned above, the following production rates are obtained for the reaction with methyl chloride (cf. Example 1):
Sample C (unheated): 8.3 g/h
Sample D (heated): 2.35 g/h
The composition of the catalyst mass was of course the same.
The Example shows a reduction in the production rate for crude silanes to around 28% compared with the original sample C, which is attributable solely to the heat treatment.
It will be appreciated that the instant specification and claims are set forth by way of illustration and not limitation, and that various modifications and changes may be made without departing from the spirit and scope of the present invention.
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Kyabram jumper leaps to gold
Kyabram's Riley Ironside won gold at the Victorian Little Athletics championshipsApril 2, 2014 4:36am
Kyabram's Riley Ironside has completed a stellar athletics season with a gold medal at the Victorian Little Athletics Track and Field Championships.
Representing Kyabram Little Athletics, Riley finished first in the under-12 boys high jump with a 1.62
The jump also gave him a new personal best, beating his previous high mark by 10
It was a close competition and Riley cleared the bar on his final attempt to win gold, with his nearest competitor unable to match him with his last jump.
Riley had a busy weekend of competition as he also qualified for championships in the 70
He produced a great run to finish fifth in the 70
In highly competitive fields he finished 10th in the 100
His weekend performances completed a season where he broke nine Kyabram Little Athletics club records.
Three other Kyabram athletes also qualified for the Victorian championships.
Kalab Ford ran a new personal best time of 1:08.19 to finish 17th in the under-12 boys 400
Thomas Burnett finished 12th in the under-12 boys shot put and 19th in the discus and Madeline Hall finished 22nd in the under-13 girls shot put.
Kyabram little Athletics will have its annual meeting on Tuesday, April 29 starting at 7
Thankyou for your comment.Your comment will appear once it has been approved by MMG staff.
Group calls for more lighting at Shepparton's Victoria Park Lake
Safety fears and shorter daylight hours prompt Victoria Park Lake user group to campaign for extra lighting.
Lakers crash out of finals
The Yarrawonga Mulwala Cricket Club A Grade team lost its semi-final clash against Bruck on the weekend, bringing to an end their 2014-2015 season.
VIP guest at Guides
On March 5, Member for Northern Victoria Wendy Lovell visited the Tatura Guides, to speak about leadership and also of her experiences when she was a Guide.
Echuca Primary School students shave it off
Twelve Echuca Primary School students took part in the World's Greatest Shave today.
Team time trial arrives
The 28th Fleche Opperman 24-hour team time-trial finished in Rochester last Sunday as exhausted cyclists rolled into town shortly after sunrise.
KLTC's winning weekend
Two teams, two premierships for Kyabram
Taking a stand against cyber-bullying
A new project developed by Mitchell Shire Youth Council members.
Piano concert in Deniliquin tonight
Leading concert artist Daniel de Borah will perform in Deniliquin tonight as part of the South West Music 2015 concert series.
Support school's anti-bulling day
Heathcote Primary School students are asking the community to show their support for student efforts to stamp out bullying.
Students take on Borneo
A group of Cobram Secondary College will travel to Borneo later this year to participate in the World Challenge.
Piano concert in Deniliquin tonight
Leading concert artist Daniel de Borah will perform in Deniliquin tonight as part of the South West Music 2015 concert series.
Poll Dorset breeders meet
The biannual Poll Dorset Conference at Moama last week heard breed associations worldwide are being challenged to innovate and remain relevant to their members and customers.
Our Paul Kelly
Benalla GP Paul Kelly receives an award in recognition of his 37 years as a doctor in rural Victoria.
Discover unbelievable local deals from local businesses every week in the Goulburn and Murray Valley area with Leapon.com.au!
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Clarion Hotel Stockholm
Ringvagen 98
Stockholm, 11120
Phone: (46) 8 462 10 00
Fax: (46) 8 462 10 99
Stockholm Tourist Center
Stockholm is a charming, old city with the infrastructure of a metropolis. Explore the cultural, political and economical capital of Sweden, which is popularly known as the "Venice of the North". For more information about tourist spots, tours and local festivals or any sort of assistance, you can contact the Stockholm Tourist Center. Please visit the official website for more information. Their open hours are seasonal.
Vasagatan 14
Stockholm, 111 20
+46 8 508 28 508
Earn valuable points toward free nights.


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gimme a number then the trax
Rank what you thought were the best tracks from the album. Personally i think too manny people are sleep…
Ok I made this thread a few days back but I didn't get my point across properly so the thread kinda beca…
@Marshawn_Lynch_With_a_E Thanks for the inspiration!
Here's a Drake x Kendrick example.
Do you think white rappers are appropriating, gentrifying or paying homage to black culture?
As we all …
I'm only on Problems on Ludaversal while I've already listened to the other two a few times but at this …
Just heard the leak and just beautiful imo.
Just hope you guys don't sleep on these good albums being r…
This underrated piece of art went platinum under two month with minimal promotion and NO radio play. I'm…
Critically acclaimed classics (3 that are widely accepted)
Amazing Commercial Success
Extreme Longevity …
Somethin important to me. I ain't sure if I got my own yet
JOIN, STARTS IN 20 MIN….. get in
IMO Outkast has a very slight edge
It's called Scales 925 (possible drug ref.). Here are the pics from the sneaks of the spot. It's slated …
which one is the RAWEST rapper alive
Here's the tracklist:
Boosie Badazz — Empire (Feat. Lee Banks Juicy Badazz Quick Tone)
Boosie Badazz —…
i tried to explain this a few weeks ago but i think it got misinterpretted…
The D.G.A.F era is a movement, maybe something just short of a revolution, its when an artist says fuck you to critics and bitch bloggers like us and disregards flow or whatever technique we deem for someone to be a "good rapper" in exchange for something that simply "sounds good and makes peeps happy" or just to get a message across…
Its pretty much the younger generation looking at the unofficial rules and expectations that many perceive (especially the older generation) for someone to be a good rapper, and putting a big fat middle finger in the air to all of it……who gives a fuck what type of rhymes or "flow" the guy has, if it sounds good thats all that matters right?
Artists included under this include
Lil B
Tyler the Creator
The use of the word SWAG seems prevalent in this era, (a word that the older generation are starting to despise) Its been defended by the likes of Lil B (who also believes that many critics are stuck in the past) and is pretty much the symbol of this era…
This is the stuff that older critics call the "death of hiphop" but the fact is, theres a huge difference between talking and doing…and right now these kind of rappers are the ones that are "doing" these guys are smart and have the majority of veteran rappers behind them. Also the rise of the internet has seen these rappers often release their albums independently….
It's really early to start calling "revolution"
And also, Lil B and Tyler have all the critics on their dick. Don't believe me? I'm Gay and Goblin are both sitting at a 73/100 on Metacritic (four points higher than Eminem's Recovery).
I don't think this is anything new, and i wouldn't call it a movement ether… To me its more of a phase in an artists career. If this subject was brought up like 15 years ago the list would be Eminem, Tupac, Biggie, and Wu-Tang on the list. The D.G.A.F is a way for an artist to brake away from what is established to create something new…
Oh! That's because Recovery is shit.
It's not new that you're a Eminem heter
He is definitively an eminem heter. Of course he ain't a hater
Tyler says swag as a joke. He actually stopped saying it for the fact that his fans started saying it so much that it annoyed him. Also the DGAF generation has nothing to do with them not caring how they rap. Its more related to how the don't give a fuck about who or what they are rapping about. They will call out anybody, and no topic is off-limits. You were completely wrong with your idea.
Actually topic wise it's been like that for a while bro…I'm not talking bout that I'm talking bout the older generation looking at the new era and saying how much they despise new hip hop…when frankly we couldn't give two flying shits…who cares about flow rhymes or density if it sounds good? It's about being unrestricted and being able to enjoy music FOR music…and not approaching t with a critics eye…
@Jonnywang by "critics" I mean more the general public bro…I shoulda clarified that shit
Abiel is a no nonsense DoomHead, don't worry about it MD
The DGAF "Revolution" can be traced back to NWA, but it was mentioned, and started by Tupac. On 2Pacalypse Now with the track I Don't Give a Fuck
All the "old" rappers give props to Tyler the Creator, and as for Lil B, hes terrible and its not old rappers giving him crap, its 95% of the population. Hes strong point is not rapping, and anyone with ears knows that. That's like saying old pop starts don't like Rebecca Black, it's because she sucks…
I don't like Relapse/Recovery, does that make me an Em hater? Nah. I actually like his old shit, so chill out. I know you guys think its heresy to NOT love everything Em releases.
Jk lol
I don't like Relapse. I don't even have it
acutually your lil b statement is quite wrong, hes acutally one of the smartest rappers out there today alot of the "95% of the population" are actually realising this…Lupe Fiasco called his album one of the best of the year, theres a difference between his BASEDGOD stuff and his Lil B stuff, but you have put him in a box and probs wont realise it…
hold up @SteveS23 i never said old rappers didnt like Tyler…i said that he has the support of veteran rappers
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[Genius](http://genius.com) is my favorite site, [Kanye West's "Power"](http://genius.com/kanye-west-power-lyrics) is my favorite song and [From whippin' the bacon rolls to outside whippin' the bacon Rolls](1256) is my favorite line
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