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Find records of Tamara Azadianfar
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Tamara Azadianfar (1937 - 2011) was born on January 3, 1937. She was born into the Azadianfar family.
There are no known spouses or children on file for Tamara. Tamara died on January 18, 2011 at 74 years of age.
Tamara Azadianfar's last known residence is at Tujunga, Los Angeles County, California.
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Possible Relatives
- Charles Cloutier
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- Francois Cloutier
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- Genevieve Moreau Cloutier
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- Genevieve Cloutier Verreau
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- Louise Cloutier Cauchon
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- Jean Busque
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- Paul Verreau
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- Antoine Dorval
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- Antoine Ignace Nadeau
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- Genevieve Crepeau Dorval
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- Romaine C Raine
- ·
- Joseph Berube
- ·
- Pierre Berube
- ·
- Augustin Goupille
- ·
- Joseph-Marie Cloutier
- ·
- Agnes N
- ·
- Genevieve-Eleonore Cloutier Belisle
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- Marie-Joseph Cloutier Boucher
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- Marie-Charlotte Lessard Cloutier
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- Jacques Cloutier
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Photos: Dirk takes ball to head; physical play; Mavs overcome slow start to top Pelicans again
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subset: commoncrawl


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1. Wedding Band Equipment Why it's hidden: The cost of the wedding band includes fees for ...
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Web Services Penetration Testing Part 7: More Fuzzing with Burp
In the previous article, we discussed how to integrate Burp Suite Free Edition with SoapUI to fuzz different parameters of a soap request, how to configure Burp, and how to use different features like Burp Repeater and Intruder. I assume that whoever is going through this article have that […]
Hack I-Bank Pro
In this article we are going to see some major vulnerabilities typical of a remote banking application. We found an interesting vulnerable machine created by PHDays team. We hosted the vulnerable machine in Virtual box and logged in with these credentials: Username:root Password:phd2012. We identified the IP for that […]
Information Gathering: Mantra Browser Walkthrough, Part 2
In a previous post, I covered the basics on the popular penetration testing Web browser Mantra. That post contains information on how to download Mantra, as well as installation and basic configuration. The Mantra browser comes with a nice GUI and most of the security and penetration testing related […]
Manually Web Application Penetration Testing: Fuzzing
When we test a web application, we do not test a single page, but a lot of pages of a single web application. Each page may have more than one variable, so technically you will be engaging with a ton of variables during your web application test. So when […]
NSA BIOS Backdoor a.k.a. God Mode Malware Part 1: DEITYBOUNCE
This article is the first part of a series on NSA BIOS backdoor internals. Before we begin, I'd like to point out why these malwares are classified as "god mode." First, most of the malware uses an internal (NSA) codename in the realms of "gods," such as DEITYBOUNCE, GODSURGE, […]
Web Services Penetration Testing, Part 6: Fuzzing Parameters with Burp
In the previous article we discussed in what cases we might face challenges performing manual web services penetration testing and how SoapUI will help in those circumstances. Now, what are the logical and business logic test cases when testing a web services, how do we test them, and what […]
Session Randomness Analysis with Burp Suite Sequencer
1. Introduction
Users of web applications are identified by session IDs. An attacker can impersonate users when generated sessions are predictable. This article introduces Burp Suite Sequencer and shows how it can be used to analyze session randomness.
2. Burp Suite Sequencer
The sequencer is part of Burp Suite, which is […]
Big Data and Incident Detection- A Promising Future, but Mind the PResent
By Matthew Neely, SecureState Director of Strategic Initiatives
The Hype
Recently there's been a lot of talk in the media and at security conferences about using big data tools to detect incidents. As an information security geek, the prospect of using big data tools like Hadoop and NoSQL to plow through piles of IDS alerts […]
From CSRF to Unauthorized Remote Admin Access
1. Introduction
The intention of this article is to show how dangerous a cross-site request forgery (CSRF) vulnerability can be. It will be presented for the D-Link DIR-600 router (Hardware Version: Bx; Firmware Version: 2.16, which was the latest version at the moment of writing this article).
The CSRF vulnerability […]
Advanced Exploits Using XSS SHELL
Before understanding what XSS Shell is, let us recall a few basics of XSS (Cross Site Scripting).
XSS is one of the most common vulnerabilities that exist in many web applications today. XSS is a technique through which the attacker tries to compromise the web application by executing a malicious […]
Manual Web Application Penetration Testing: Introduction
In this series of articles, I am going to demonstrate how you can manually exploit the vulnerability of a web application, compared to using any automation tool, in order to find vulnerabilities in the application. Almost all companies worldwide focus on manual testing of web application rather than running […]
R00t This Box
Here's a challenge, root this box. We found a vulnerable machine named Hackademic RTB1. The main challlenge is to root the box with admin privileges and capture the flag.
First, we hosted the vulnerable image in VMware with bridged mode network settings. Our target is ready, but we don't know […]
IT Security 101: Prevent Weak Passwords
Passwords have been part of IT since long before the age of the desktop PC. However, now more than ever, systems administrators need to re-examine their password security policies to remain effective against modern programs and computers that can crack weak passwords in minutes.
Basic eight-character passwords can now be […]
Attacking LAN hosts with ARP spoofing
1. Introduction
This article introduces the OSI model of internet communication, and describes ARP spoofing. It's used to attack hosts in a Local Area Network (LAN). Passive and active sniffing are described. Finally, the mitigation of ARP spoofing is briefly discussed.
2. The OSI model
This model describes the structure of internet […]
Vulnerability Assessment with Nexpose
Nexpose is one of the leading vulnerability assessment tools. The Nexpose community edition is a free program and the other editions are paid ones. In this article, we will use the free Nexpose community edition, which has the ability to scan 32 hosts. The user interface is clean and […]
Adobe CQ Pentesting Guide – Part 1
This post deals with the step-by-step security testing guidelines for Adobe CQ installation.
Adobe CQ is Adobe's new Web Experience Management software portfolio which provides easy-to-use web apps for creating, managing and delivering online experiences to its users. It also supports integration with other Adobe products. CQ provides a unified […]
Wireless Attacks Unleashed
As we all know, wireless networks are spread at each and every part of the world, starting from personal home to corporate business environments, schools/universities, cafes, etc. The major merit of wireless networking is to eliminate the big and untidy cables, which acquires space and unspoils the look of […]
Vulnerability Scanning with Metasploit: Part II
In the previous article, we learned how to perform a network vulnerability assessment by using the OpenVAS plug-in. In this continuation, we will see how to perform a web application vulnerability assessment by using the wmap plug-in.
WMAP is a feature-rich web vulnerability scanner that was originally created from a […]
The Mechanics of Metasploit
Metasploit is exquisitely prevalent amongst penetration testers and especially hackers because it makes it very easy to develop and launch exploits for software vulnerabilities. This paper exclusively demonstrates how to configure and practice Metasploit, which is a penetration testing platform for developing and launching exploits. This research paper primarily […]
Deadly Consequences of XSS
Cross-site scripting (XSS) is a very popular term, not just among web application security guys, but also among developers, where popping an alert box with a message in it is a HUGE hit.
Among the locations where XSS is generally found in a web application, the most common is a […]


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Select () or exclude () categories to narrow your recipe search.
As you select categories, the number of matching recipes will update.
Find exactly what you're looking for with the web's most powerful recipe filtering tool.
1/1 Photo of Rice Flour Banana Bread (Wheat Free)
Prep Time:
Cook Time:
10 mins
55 mins
I always seem to have rice flour on hand (for Vietnamese and Thai food), and am always looking for ways to use it up. This recipe is from the incomparable Beatrice Ojakangas' "Great Whole Grain Breads" (Simon & Schuster, 1984,1993). The recipe calls for small loaf pans, probably to reduce the baking time. Might be possible to use a large pan, but I haven't tried.
Units: US | Metric
Serving Size: 1 (91 g)
Servings Per Recipe: 10
Every recipe, menu, tip and how-to is right here, at your service.


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Gary D'Amato offers news and insights on Wisconsin golf, new technology, courses and instruction
Golf Channel's Tilghman apologizes
Kelly Tilghman and the Golf Channel handled a difficult situation about as well as it could be handled Thursday.
Back In the booth after a two-week suspension without pay for joking on-air that Tiger Woods' peers should "lynch him in a back alley," Tilghman apologized at the top of first-round coverage of the Buick Invitational. The telecast began with Tilghman introducing herself and saying that during coverage of the season-opening Mercedes-Benz Championship, "I used an inappropriate word that was offensive to many. ... I am terribly sorry for any hurt that I've caused. I would like to express my deepest apology."
The Golf Channel then picked up coverage at Torrey Pines with Woods in the middle of his back nine. He went on to shoot a 5-under-par 67 on the South Course and was tied for third place, one stroke behind co-leaders Troy Matteson and Brad Adamonis.
Neither Tilghman, the first female TV anchor for men's tournaments in golf history, nor analyst Nick Faldo again referred to Tilghman's poor choice of words during the Mercedes-Benz Championship. In an unfortunate attempt at humor during the second round, Tilghman responded to Faldo's suggestion that the other players "gang up" on the dominant Woods in order to beat him by saying they should "lynch him in a back alley." She apologized directly to Woods and two days later to viewers.
The Golf Channel suspended Tilghman for two weeks, hours after the Rev. Al Sharpton called for her to be fired in an interview on CNN.
Woods said earlier this week that Tilghman made a mistake but that she meant no harm and he had accepted her apology.
Comments »
Read and share your thoughts on this story.


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Hi everyone! I'm sorry that I have been MIA. I had been really depressed and I was isolating myself. It was just a really hard time. But now I'm back, and I'm excited about all of the new changes at iVillage. I really like the new look of the message boards.
I have some news, too. I'm off the Pill, so I guess my husband and I are officially trying to conceive. I'm very excited, but also very scared. I'm sure that it will take a while for me to get pregnant since I've been on the Pill for years. I've been posting in the Trying to Conceive forum, too.
I really hope that you lovely ladies are well, and I look forward to catching back up with you!!


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The Time To Shine Has Come
RESCHEDULED: I DECLINE TO SHARE STAGE WITH JAKE E LEE (Ex-OZZY OSBOURNE GUITARIST)!
We are pleased to announce that I DECLINE will be opening for Former OZZY OSBOURNE GUITARIST JAKE E LEE AND RED DRAGON CARTEL at REGGIE'S 2105 South State Street Chicago, IL 60616 on SATURDAY, JUNE 28TH, 2014.
Jake recorded, wrote and toured with Ozzy. They released "Bark at the Moon", which eventually went multi-platinum, and quickly quieted critics who said Rhoads could never be replaced. The "Ultimate Sin" album followed, which was another huge success for Ozzy. Osbourne, at the time was going through his well-documented drug and alcohol periods, and during a rehearsal fired Jake in the middle of one of his rages. Contrary to common belief, however, Ozzy and Jake remain good friends to this day. Ozzy has recently talked to Jake about a possible reunion, although Jake has repeatedly turned him down.
Joining us will be LOVEBLAST and IRON FINGER. Hope to see you there!
Check out the RED DRAGON CARTEL'S LATEST VIDEO below:
I DECLINE drummer John Doyle recently penned a score for Sci-Fi Podcast "No Deodorant in Outer Space", a podcast reviewing literature and movies in classic and contemporary science fiction, fantasy and related genres. The show is hosted by author RYAN SEAN O'REILLY , DAVID "WILK" WILKINSON, and JAMES "BEAM" RAUCH. Visit the site online and Suscribe to the Podcast on iTunes for free
We need your help!! If you're on Facebook, Post a link to OUR FACEBOOK PAGE on your Wall and we'll hook you up with a free download of the live version of "The Administration" performed at Reggie's. Just sign up for our newsletter, like us on Facebook, or get a friend to join our newsletter or like us on Facebook and let us know you did and we'll hook you up!
Well, that's about it for this newsbriefing.
As always, Raise those Horns Up!
- Dole


text:
Ray Kurzweil Says He's Breathing Intelligence into Google Search
Inventor and futurist Ray Kurzweil says work is under way at Google to apply his theory of intelligence to understanding online information.
Discover one of our 28 local entrepreneurial communities »
Be the first to know as we launch in new countries and markets around the globe.
Interested in bringing MIT Technology Review to your local market?
Inventor and futurist Ray Kurzweil says work is under way at Google to apply his theory of intelligence to understanding online information.
The Supreme Court's decision was tailored narrowly, but it may provide openings for lawyers to argue that other forms of mass Internet streaming violate copyright.
Smart watches that take voice commands, issue timely reminders, and even let you order pizza from your wrist go on sale from Google today.
A new line of smartphones designed by Google could spread Internet access more widely in poor regions of the world.
A new kind of search engine will make it possible to search inside the apps on your phone.
Could heat-tracking be the key to interacting with wearable computers?
Many leading apps consume too much data to be viable in parts of the world where data is expensive, says Facebook.
If a device could capture every moment in life for your easy recall later, would you want it to? There are plenty of things I'd rather forget.
As electronics get more personal, some fixtures of earlier eras of computing may feel inappropriate.
Software meant to help people interpret emotions will soon be available in several apps.


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Notes from the November Scrumtisch
The November Berlin Scrumtisch took place on Thursday with the presence of 10 agile42 coaches
Web community manager of agile42, trying to post relevant, informational, fun bits of content on the blog and social networks
It's been a thrilling special event for Berlin Scrumtisch (the Scrum User Group officially approved by the Scrum Alliance). Since a number of European coaches of agile42 were in town for their scheduled European Coach Camp, the Scrumtisch has featured a Meet the Coach night where Certified Scrum Coaches and Certified Scrum Trainers have taken lead on the topics proposed by the audience. The gathering took place at the American Diner Berlin in Friedrichshain, and you can see the sixties-inspired place from the photos!
Users picked topics from the big board and (self-)organized in groups to discuss them ...


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See all Staples Coupons.
Laptops, Computers, and Tablets at Staples
$100 off in-storeSHOP NOW
Posted 3 hr 1 min ago
In-store only, Staples takes $100 off select laptops, desktops, or tablets of $499 or more via coupon code "46137". Need a tablet? Use coupon code "79545" to cut $100 off tablets regularly $399 or more. Some exclusions apply, including iPad Air 2, iPad mini 3, and clearance. Deals ends November 25.


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Join Date: May 2006
Location: BC
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"So let us be loving, hopeful and optimistic. And we'll change the world." - Jack Layton
Flowers, fairies, gardens, and rainbows-- Seasons of Joy: 10 weeks of crafts, handwork, painting, coloring, circle time, fairy tales, and more!
Check out the blog for family fun, homeschooling, books, simple living, and 6 fabulous children, including twin toddlers
|A 4 mo old shouldn't be going 8-10 hours without eating, right????
Cristeen ~ Always remembering our warrior ~ Our is 3, how'd that happen?!?!
We welcomed another warrior in May 2012!!
2012 Decluttering challenge - 575/2012
Katie - Married to Mike 06/02/01, Mom to Sydney Anne born 11/21/09 and Alice Maeryn & Oliver Thomas born 04/24/13
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|Amazon Price
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Audio CD, Audiobook, CD, Unabridged
"Please retry"
Product Details
Would you like to update product info or give feedback on images?.
Very well written book and easy to read and follow.
Kotter's ideas of establishing a sense of urgency and creating a guiding coalition brought great insight to the part of the change process known as readiness.
Each Manager Has to read this book, its mandatory for business people i highly recommend it.
Very helpful; met my needs, however repetitive; could have been a shorter book.Published 21 days ago by Roger Thompson
A truly insight must read for anyone leading an organization through a transition or anyone planning organizational transformation.Published 27 days ago by Inspired
Still a good treatise on organizational change despite its age. Not many business books stand the test of time, but this one does. Read morePublished 1 month ago by Lineman
Exactly how described. Great book and it is just what I ordered.Published 1 month ago by Cute kitty :)


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I don't know about you but I LOVE Yankee Candle! Reader Stacey let us know that Yankee Candle is having a $1 Sale right now for Veteran's Day Weekend!
You can choose from Sampler Votive Candles, Tarts Wax Melts, Treasure Tarts Wax Melts, or Car Jars for this price! Regular price on them is $1.99-$2.99 each, so be sure to grab what you want now while the price is low!
**Be sure to join our Black Friday Deals and HOT Online Holiday Savings Group so you won't miss any of the awesome deals we find during the holiday season!**
Thanks so much for sending over this sweet deal for us Stacey!
Have you checked out the rest of our Coupon Deals? Also be sure to follow us on Facebook to stay up to date. You can also follow us on Twitter, Pinterest and G+!
Social media not your thing? No worries you can sign up for our daily email and have the deals sent right to your inbox!


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Alpha MOS Environment
based in TOULOUSE, FRANCE
Pioneer of electronic noses, Alpha MOS brings its expertise and know-how to the environmental sector. Our mission is to help industries achieve their Environmental Performance objectives : Reducing the impact of environmental releases. Optimizing consumption of resources: water, energy, additives, etc. Improving performance of odor treatment systems and reducing ...
Odotech Inc.
based in Montreal, QUEBEC (CANADA)
Odowatch: Automated electronic-nose-based wireless odor monitoring system. Odor Emission Monitoring. Odor Impact Prediction. ODOTECH designs and manufactures odor measuring and monitoring systems. Nuisance odors generated by a facility can now be monitored 24/7 by the OdoWatch automated wireless electronic noses network. Odotech offers a wide range of services to its ...
IDES Canada Inc.
based in Markham,, ONTARIO (CANADA)
Scentroid is the word leader in odour measurement equipment and services to over 37 countries around the world. Our unique instruments are used in universities, government agencies, laboratories, environmental consultants, waste water treatment plants, land fills, petrochemical plants, and many other industries that deal with odour nuisance.The Scentroid line of ...
based in Daejeon, SOUTH KOREA
Science Lab Center Co., Ltd is specialized in odor monitoring system. Our products branded `OdorCatch` are Output signal analysis of gas sensor, Odor measurement / monitoring systemand Environment friendly photocatalyst. Our Core technology of OdorCatch system as follows, 1. `Output signal analysis technology` of gas sensor, domestic patent registration. - Technology of ...
DelAgua Group
based in Marlborough, UNITED KINGDOM
The DelAgua kit was first introduced to overcome the problem of lack of access to testing laboratories. It is now used all over the World by both Government and Non-Government Organisations as the Portable Water testing kit of choice.DelAgua also supplies all manner of water testing & laboratory equipment at heavily discounted prices to companies and individuals all over ...
Analytical Technology, Inc. (ATI)
based in Delph, UNITED KINGDOM
Manufacturers of toxic and combustible gas detectors along with a complete line of water quality monitors. At ATI, we specialize in the application of electrochemistry to air and water monitoring problems. Our sensors are at work 24 hours a day, 365 days a year, year after year, helping safeguard the workplace against the dangers of toxic gas emissions and improving the ...
Bowker & Associates, Inc.
based in Portland, MAINE (USA)
Bowker & Associates, Inc. specializes in the assessment and control of odor emissions from waste handling facilities and industrial processes. Services include odor emission inventories, performance testing, evaluation and design of odor control systems, value engineering and independent peer reviews of odor control projects, and expert witness testimony.
PCA Technologies
based in Parabiago - MIlano, ITALY
PCA Technologies Ltd. offers innovative solutions for Environmental Monitoring and Civil / Military Security.We employ a line of cutting edge instruments equipped with intelligent sensors (the electronic nose) for quality control, odor monitoring and recognition, and for preventing risks from toxic gases, CWA and explosives.PCA Technologies is partner dealer of Airsense ...
Enviroware s.r.l.
based in Concorezzo, ITALY
Founded in 1997, Enviroware provides advanced consulting services in atmospheric impact assessment, industrial risk evaluation, development of modelling tools and development of environmental software. The expertise of Enviroware guarantees to the Clients the achievement of their objectives, with complete satisfaction. The company can develop modelling tools specifically ...
based in Mannheim, GERMANY
Welcome to AB-GM (Andreas Stefan Bartsch - Gefahrstoffmessungen) your independent expert advisory agency for detecting, examining, assessing and evaluating damage caused by mold fungus, moisture and/or water, asbestos exposure and the adverse effects of odors, as well as for measuring the levels of pollutants, hazardous substances and mold fungus contained in the air in ...


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Last Friday, the Pickens High School Dragons football team hosted the arch region rival from up 515, the Gilmer High School Bobcats, in what was one of the most hyped and most important games in the rivalry. The winner would lock up the number two seed in 7-AAAA and host the three seed from 8-AAAA in the first round of the state playoffs. The Dragons warmed up in their normal green jersey's but when they returned from the locker room they would emerge in all black for the blackout Dragon Nation held, as a surprise to everyone. To top it all off, it was Senior Night, and the Dragons used a second half shut out to take a 42-19 win and lock up a "winner take all" Region 7-AAAA championship game at Cartersville.
[Full Story »]


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A 9:1 Balun is listed on dxzone.com since 2009-03-07 Hits ... Making a simple current balun; QRO baluns; Broadband Baluns. What did A 9:1 Balun look like in the past?Test this site now
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text:
Hawaii hometown backs Te'o after girlfriend hoax
The father of another high-achieving athlete who lives in the area said he felt for Te'o's parents, and for Te'o himself.
"Of course you're going to love them no matter what and support them. There are times when you fall down, but you get to rebound. And that's where Manti personally needs our support, probably," said Benny Kai, a Kahuku resident and father of former U.S. Olympic soccer player Natasha Kai. "I support him in everything he does."
Makala Paakaula, 38, a high school administrator, said Te'o should be lauded for uniting Notre Dame during his senior year when he could have left for the NFL, she said.
"It's amazing how he brought together the whole school to become one ohana, one family, where they all belonged, where they all had a purpose," Paakaula said.
Phi Smotherman, 46, said people in Laie are sorry a guy like Manti became a victim of hoax. He said the town should throw a parade for him when he comes home in recognition of his career at Notre Dame and all the awards he received.
"I hope he does great, goes to the NFL and finds a real girlfriend that he can marry and actually touch," Smotherman said.
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- 7628OKC Thunder: Russell Westbrook will start against the Knicks; Kevin Durant still out
- 7471Oklahoma football: A closer look at the Sooners' bowl options


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Hello community! I had a rejected file on Videohive "cannot be resubmitted as it did not meet our minimum requirements for quality and/or marketplace policies." I would like to hear someone opinion about this project. Thank you! Link HERE
Hello, vidosworld. It seems like 'Real Movie Trailer III' is really similar to your other projects of this kind. It doesn't bring anything new to the table. It basically looks just like a texture change. Maybe it's just me, but the scenes don't look as dynamic as they should be for that kind of a project. When the text flies into the camera it should be better to have some smooth keyframes. It's not easy to make a 2nd or 3rd version of some project. I've been hard rejected due to similarity. Always strive to have something new in your next project.
Thx Protest! I will strive to make it better!
"Do, or do not. There is no strive" as Yoda once said. Or something similar.
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text:
Big Daddy
By: xtube_sponsor
Video Details
Date: 1 year ago
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2 years ago
http://www.xtube.com knows ?
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2 years ago
Nice Daddy !!!
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2 years ago
http://www.xtube.com's go elsewhere, m'dears. Not worth our time or attention.
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Bar Accessories
Magical Mixology Flask$29.99Price: $29.99
When youre delighted with your drink and want to take it on the go, reach for this unicorn flask! A diagram of a unicorns structure - from 'giggles' to 'wishes' - decorates the face of this stainless steel flask, making it the perfect playful place to pour your potent potables. ...
Spirited Cheers Flask$29.99Price: $29.99
Kudos to your great taste in choosing this stainless steel hip flask that arrives with a care card inside a cute canvas satchel. Featuring a wraparound wooden panel that depicts a rope-tied admiralty anchor, this made-to-be-concealed container reads ""Down the Hatch,"" delivering a fun, seafaring feel. Bestow this anchor-bedecked flask ...
Taste of Luxury Flask$39.99Price: $39.99
Cheers to the fancy sipping that's in your future with this stately flask. Plated in 14-karat gold, and boasting a liquid-tight lid and six-ounce capacity, this shining beauty is your golden ticket to enjoying libations looking luxe!
Sip Back and Listen Flask$29.99Price: $29.99
Take your sophisticated palate on the trail with this USA-made stainless steel flask! Featuring a vintage-inspired design that pays homage to an infamous spritely beverage, this canteen sees that you sip around the campfire in style.
Bear Bottle Opener$14.99Price: $14.99
Whether you're having a hopping party or just enjoying a brew for two, this wild wall-mounted bottle opener is sure to come in handy. Affixed on the wall of your den next to a few potted plants and some wood-paneled speakers, this mottled red-brown and black, cast iron bear will ...
Hoot Wants a Cold One? Bottle Opener$9.99Price: $9.99
A refreshing summer ale opened by this owl bottle opener is a surefire smile-inspiring combination! A must-have for bird lovers and beer aficionados alike, this little kitchen gadget is made of sturdy, weathered cast iron with owlet features, a heart-shaped center, and a flat base for easy stand-up display.
Head of the Game Bottle Opener$17.99Price: $17.99
After a swim in the waves and a brief beach volleyball match, your visiting pals are sure to be parched! So why not tout your nautical taste and fierce hosting skills by docking the cooler of drinks below this skull bottle opener? Cast from sturdy metal with a weathered finish, ...
Topped with Tentacles Wine Stopper$14.99Price: $14.99
Save the rest of that Pinot Grigio for another fun evening with this octopus wine stopper. Made from shiny silver metal, this sea creature-adorned gadget has a rubber center for a seal that keeps your vino fresh for next time!
Zip, Sip, Hooray Bottle Opener$17.99Price: $17.99
Celebrate the weekend in the most whimsical way - by reaching for this this zipper-shaped bottle opener to enjoy your bev of choice! The magnetic back and sturdy silver metal of this opener makes it easy to grab off the fridge, pop the cap off a cold one, and toast ...
Whale of an Ale Bottle Opener$17.99Price: $17.99
Open up to an ocean of fun with this quirky bottle opener. Constructed from smooth, heavy-duty pewter, this shiny silver whale features an underside opener to easily remove the cap from your beverage of choice - while making quite a splash with guests!
Wrench Your Thirst Bottle Opener$12.99Price: $12.99
Whether youve just finished renovating your kitchen or repairing your classic convertible, reward your hard work with a cool refreshment after popping off the cap with this handy bottle opener! Cast from iron with a rough, weathered brown finish, this tough wrench is all torque and no play when it ...
Innovative Enjoyment Bottle Opener$14.99Price: $14.99
This wooden bottle opener is for the gal whose normal is unique. Its curved black nail, whose head hooks on the edge of your bottles cap for creative removal, was designed for the ever-imaginative guy. And, the vibrant coral tip of this unique manual appliance is perfect to add a ...
To Fetch a Whale of Water Pitcher$34.99Price: $34.99
Luckily, you neednt go up a hill to delight in the quirky charm of this ceramic pitcher! Colored in muted hues of ivory, slate, and espresso, this vintage-inspired vessel dispenses beverages from a whimsical whales mouth. With a curled tail serving as a convenient handle for your pouring pleasure, this ...


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Crystal Perido wrote: AMY SMITH
123 Main Street • Atlanta, Georgia • 30339
Home: (555) 555-1234, Cell: (555) 555-1235 asmith@sample~resume.com
Objective: Seek the Position of Fashion Model
SUMMARY: Remarkably gifted Fashion Model with over six years experience in displaying and promoting clothes and other goods on television, in magazines and on a catwalk at fashion shows.
Summary of Qualifications
Exceptional performance skills.
Sound knowledge of body posture, movement and facial expressions.
Remarkable knowledge of body and face care.
Thorough knowledge of make-up, hairstyles and fashion.
Exceptional ability to memorize routines.
Strong knowledge of sales techniques.
Uncommon confidence, patience and punctuality.
Remarkable ability to adapt and be able to accept criticism.
Possession of huge professionalism and concentration on duty.
Exceptionally attractive skin and personality.
Great coordination, flexible body, clear speech, tidy appearance, and immensely fit and healthy.
Professional Experience
Crystal Fashion Inc., Minneapolis, MN
2000 - Present
Fashion Model
Model garments, such as dresses, coats, underclothing, swimwear, and suits, for garment designers, BUYERS (profess. & kin.), sales personnel, and customers.
Dress in sample or completed garments displayed or photographed.
Stand, turn, and walk to demonstrate features, such as garment quality, style, and design, to observers at fashion shows, private showings, and retail establishments.
Inform prospective purchasers as to model, number, and price of garments and department where garment can be purchased.
Select own accessories.
Sit for make-up and hair stylists.
Discuss the required poses, movements and the part to be played.
Rehearse the movement or part.
Maintain a nutritional diet.
Model clothes, make-up, jewellery or other products in fashion shows or for magazines or television.
Learn scripts and dialogue for television auditions.
Associate Degree in Fine Arts
University of New York (2000)
Are you insane???!!!!!
OP, do NOT follow this person's advice!!!! Unless you want people (casting directors, agency bookers, other industry people) to roll on floor laughing their hearts out when you approach them.
Snapshots and/or comp cards and/or a portfolio with relevant images for the market you're in are what you need - not a resume!


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Just A Dream
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Environmental protection
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When he has a dream about a future Earth devastated by pollution, Walter begins to understand the importance of taking care of the environment.
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- Reuters
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Pacific Rim 2 will be a "different adventure" to the first movie but Charlie Day and Burn Gorman will be returning for the sequel. Read More »
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Shia LaBeouf is complying with treatment ordered as part of a plea deal stemming from a bizarre episode during the Broadway show Cabaret. Read More »
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Nicole is the cover girl for the 2014 edition of SA Swimsuit! Check out some smoking hot pics of here here.
DurbanTakata South Africa (Pty) Ltd
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Start learning with our library of video tutorials taught by experts. Get started
Make models with 3D objects, edit polygonal meshes, create surfaces and models with 2D shapes and splines, and more.
Practice designing stairs for commercial and residential buildings, as well as winding stairs, custom railings, and ramps.
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A HUGE thank you to Pilot Scott Johnson!
A HUGE thank you to Pilot Scott Johnson! His very first Pilots N Paws mission helped a stray coonhound momma and her 9 puppies get from Chicago to their rescue in Minneapolis, MN. She was found as a stray in rural WV where a local rescue group was contacted about her. She was VERY pregnant and INJURED – probably from being caught in a wildlife trap. She was taken in by the rescue groups (BARC) that works to rescue dogs from the Boone Co WV Dog Pound but they also help at risk strays in the community. Long story short is that she was in foster care for one day then the pups were born. 5 days later she had tail amputation surgery as well as a few toes removed. She recovered well and is a very good mommy!
Their transport to rescue journey began last Wed with a ground transport from Portsmouth, OH to Chicago where they were temp fostered by another rescue contact and taken to the airport to meet their flight to their final destination!
Scott went out of his way to accommodate transporting this family by removing the back seat and adding weights to balance the plane. He even bought a large crate to house them! There were a few bumps in the road with weather but pilot Scott adjusted things and completed the mission!
Best Regards,
Eva Kordusky
BARC Secretary


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Great quirky little hotel near to the Paris Centre. Located in a quiet street but very close to a busy cafe/restaurant area, it fitted our needs very well. We had absolutely no issue with our stay, but having read some of the other less complimentary reviews can appreciate why the more fussy travellers amongst us have left some of their... More
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- TripAdvisor is proud to partner with Expedia, Hotels.com, Travelocity, TripOnline SA and Tingo so you can book your Hotel Mogador reservations with confidence. We help millions of travelers each month to find the perfect hotel for both vacation and business trips, always with the best discounts and special offers.
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- Mogador Hotel Paris


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Sounds Like: Kings Of Leon, Sublime, The Doors, Gotye - somebody that i used to know, Ben Folds
Manager: NC Local Music
Bio: The Resonance Cascade is a new gem to the Raleigh music scene. Be on the look out for upcoming events and surprise events coming to venues near you! More music to come!
<iframe src="https://www.facebook.com/video/embed?video_id=10101206340485909" width="1280" height="720" frameborder="0"></ifr... See Full BioMore Info
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Leapers UTG Dragon's Claw Bipod w/ Clamp on Barrel
Leapers UTG Dragon's Claw Bipods are made of high tech durable construction with a clever ... adjustment wheel for a wide range of Riflescope barrel sizes. The Bipod by Leapers is user friendly ... Features of Leapers UTG Dragon's Claw Bipods High Tech Durable Aluminum Construction Clever...
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Mac gets second chocolate shop
Apr 6, 2012 | 2 Comments
By Molly Walker
Of the News-Register
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It would have been 'nice' to have read the Chocolatier extolling the virtue in not producing her chocolate from cocoa beans that had been harvested by the tiny hands of slave children, but, she did not.
There in lays the rub, as far as human standards go.
I am actually quite surprised that you hadn't asked that question.
• DA Brad Berry: All three officers fired weapons (34043)
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Posts tagged super-turrican
VC Monday Madness: Super Turrican 2
Super Turrican 2 (SNES, 1 player, 800 Wii Points) Wii Fanboy says: download it! With there being only the one Virtual Console game this week, it had better be a good one, right? Well, Super Turrican 2 is a pretty solid title, but with the other great entries in the genre available on the...
This Week in Review: A Smashing Start
Welcome to This Week in Review (formerly This Week in DLC), where we round up all the hands-on impressions and game reviews (including Metareviews) from the Joystiq Network. This week's megaton title should come as no surprise whatsoever. Nintendo Wii First impressions: Super Smash Bros. Brawl ...
VC Monday Madness video wrap-up 3/3/06
We appreciate the fact that we actually have a good game to play this week, but only one release? Come on, Nintendo! You spoiled us with your week after week of releasing multiple titles, only to have us completely let down today? For shame, considering that most also expected the first entry in a...
Virtual Console Monday: Super Turrican stands alone
Keeping expectations in check is the key to having a wholly satisfying life, so we probably shouldn't have grown accustomed to the three-game cornucopia that once characterized Nintendo's weekly Virtual Console release schedule. Now that the standard has dropped to two-per-week and, occasionally...
VC Monday Madness: Super Turrican
Well, it was a long wait. And what kind of thanks do we get for being patient little boys and girls and having to actually turn on our Wii to find out what Virtual Console games are available this week? Super Turrican. Yup, that's it, only one release this week: Super Turrican (SNES, 1 player,...
VC Friday: Pew pew pew
It's been hard not to feel totally pampered by recent PAL Virtual Console updates, with the likes of Phantasy Star II and Street Gangs keeping us up late. This week's releases -- both of which are shooters -- can't quite match that kind of awesomeness, but they're still worth considering. Super...
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Posted on Nov 20th 2014 4:30PM
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Persona Q review: When worlds collide
Posted on Nov 20th 2014 12:00PM


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Walk 4 Water Update
The annual Walk 4 Water event was held Wednesday, August 20 at Sunshine Park in Andover. Hundreds of participants joined the walk to increase awareness and raise funds to build a well to provide clean water for a community in Angola.
We raised over $9,000 to build the well! THANK YOU for your participation and support!
If you would still like to donate to the Walk 4 Water campaign, it's not too late. Visit www.walk-4-water.org.


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WordPress Hosting Review
Alex Denning of WPShout has put together a comprehensive, independent review of the best hosts for WordPress-powered sites. An excellent resource for those looking for awesome WordPress hosting.
Alex Denning of WPShout has put together a comprehensive, independent review of the best hosts for WordPress-powered sites. An excellent resource for those looking for awesome WordPress hosting.
For some projects, it's nice to output clean, well-formatted markup. Using theme template files enables great control over most of your (X)HTML formatting, but not so much for automated functionality involving stuff like widgets and custom menus. One of my current projects requires clean, semantic HTML markup for all web pages, but also takes advantage of WordPress' custom-menu functionality to make things easy. In this DiW article, we'll see how to enjoy both: WordPress custom menus and clean, well-formatted HTML markup.
One of my clients was hacked with the so-called "Cannot redeclare" hack. It seems closely related to the nefarious TimThumb hack, so if you've been hit by either of these hacks, you should check for the other. Apparently these hacks affect shared servers, so if you host multiple WordPress sites, chances are high that they're all infected.
Everyone loves a good comment. Readers benefit from the shared information and authors appreciate the conversation and feedback. But you gotta keep the spam out. Akismet and other anti-spam plugins do an excellent job of automating the process, but it's a good idea to watch out for false positives: legitimate comments marked as spam. Rescuing ham comments from the spam pile promotes healthy comment threads and improves the quality and reputation of your site. In this DiW post, we explain how WordPress & Akismet deal with spam, discuss anti-spam strategy, and share some ham-saving tips and tricks.
Recently I worked on a project where a single RSS feed was imported and displayed in multiple columns on the web page. Certain pages display feed items in two columns, others in groups of three or more. This technique uses WordPress' built-in
fetch_feed functionality to parse external feeds, and a slice of PHP magic to display them in multiple columns. It's flexible too, enabling any number of columns and feed items from anywhere in your theme/template files. For example, you could display any of the following:
We get quite a few requests for 1-to-1 WordPress support, but unfortunately don't have the resources to help everyone directly. We frequently see emails like this:
Hey I'm sure everyone's heard by now, but I wanted to post about Smashing Magazine's new exclusive WordPress section! We're aiming for quality, in-depth articles, tutorials, and reviews on all things WordPress, and we've got some great stuff already in the works. Drop by and check it out! :)
WordPress does an excellent job of keeping track of what's happening with the loop, but once you start customizing parameters and setting up multiple loops, it's a good idea to explicitly reset them using one of three WordPress template tags. In this DiW post, we'll explore these techniques to get a better understanding of when and how to use them in your WordPress themes.
WordPress makes it easy to publish content in any number of categories, with any number of tags, and with any type of custom post format. So for example, in addition to full articles, you could also offer screencasts, links, side posts, tweets, and all sorts of other peripheral content. Complementary material may work great for visitors surfing around your site, but including all of that extra stuff in your RSS feed dilutes the potency of your main articles. The idea here is that your visitors will subscribe to the more focused content.
Nice little infographic showing the usage of WordPress among the worlds top 100,000 sites. Amazing to see that people out there are still running WordPress as old as version 1.5!
WordPress provides a variety of ways to redirect logged-in users. In this DiW post, we explain each of these methods along with some useful tips and tricks along the way. These techniques enable you to redirect logged-in users to internal pages, external pages, and even return them to the current page.
It's TRUE!!! :) We've partnered with Designer Themes, where you can get a free DiW PDF/eBook with purchase of any of their awesome Pro themes (all GPL!).


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There are provided internally cross-linked, stables polymeric materials, in the form of substantially spherical particles, each particle consisting essentially of a single macromolecule. They have the unusual property of being soluble or dispersible in a liquid medium without significantly increasing the viscosity of the medium, rendering them potentially useful in imaging applications such as ink jet printers. They can be prepared by dissolving polymeric material in a solvent system to form a solution of the polymeric material at a concentration therein of less than the critical concentration for the polymer, causing the polymeric material to contract into an approximately spheroidal conformation in solution, cross-linking the polymeric material in solution in said spheroidal conformation so assumed, and recovering stable, cross-linked approximately spheroidal polymeric particles from the solution.
1. A method of making metal particles, comprising:
(a) providing internally cross-linked single-polymer molecules;
(b) contacting the single-polymer molecules with a metal salt to incorporate the metal salt into the single-polymer molecules; and
(c) causing the metal salt incorporated in the single-polymer molecules to form metal particles.
2. The method of
3. the method of
4. The method of
5. The method of
6. The method of
7. The method of
8. The method of
9. The method of
10. The method of
11. A particle comprising a metal particle and at least a portion of an internally cross-linked single-polymer molecule.
12. The particle of
13. The particle of
14. The particle of
15. The particle of
16. The particle of
17. The particle of
a) providing internally cross-linked single-polymer molecules;
b) contacting the single-polymer molecules with a metal salt to incorporate the metal salt into the single-polymer molecules; and
c) causing the metal salt incorporated in the single-polymer molecules to form metal particles.
This application is a continuation of application Ser. No. 10/275,978, filed on May 23, 2003 now U.S. Pat. No. 7,189,279, which is incorporated herein in its entirety by reference thereto, which claims priority to PCT/CA01/00757 filed on May 28, 2001 (which is incorporated by reference herein in its entirety), which claims priority to Canadian patent application 2,309,575 filed on May 26, 2000 (which is incorporated by reference herein in its entirety).
This invention relates to polymers, and methods for producing polymers of novel structure. More particularly, it relates to a process for cross-linking polymers to produce cross-linked polymers stabilized into particularly useful, dense structures. It also relates to novel polymeric materials having unusual properties.
It is known that cross-linking of polymers substantially alters the physical properties of the polymers. Cross-linking can change a thermoplastic polymer to a thermoset polymer, can alter its solubility, density and other physical characteristics. Normally, cross-linking of a polymer is an irreversible process, so that the shape, configuration and density of a cross-linked polymer remain substantially permanent once the cross-linking process is complete.
A variety of different methods of polymer cross-linking are known. One method is reaction with chemical cross-linking reagents. This is particularly applicable where the starting polymer is unsaturated (polybutadiene, polyisoprene, styrene-butadiene copolymers, EPDM etc.), so that the groups of unsaturation take part in the cross-linking. Other methods involve creation of reactive sites such as free radicals on the polymer chains, e.g. by hydrogen abstraction using a free radical-generating initiator, by irradiation with γ-rays, X-rays, etc. Cross-linking can take place with the polymer in solution in a suitable solvent, in suspension or in bulk. Cross-linking is normally a random process, which may involve links between different polymer chains and links between points on the same polymer chain, and permits only limited control over its course and extent. In solution and suspension, non-cross-linked polymers tend to adopt an extended, coiled conformation, which is altered in a generally uncontrollable manner during cross-linking. There is a need for stable, solid particulate polymers of predetermined shape, size and density, for use for example in ink-jet printers, photocopiers and other imaging applications, where the achievement of fine definition and resolution of images depends upon the particle size and uniformity of the particles comprising the imaging medium, and on the viscosity of the imaging medium.
The present invention provides a process whereby polymers in solution are diluted so as effectively to disentangle and isolate the individual macromolecules from one another in the solution, and then caused to contract from the normal, random coil conformation to adopt an approximately spheroidal configuration. Then the macromolecules are stabilized in this conformation, e.g. by applying cross-linking conditions to the solution, so that the dissolved polymer is internally stabilized in its newly assumed, spheroidal configuration, to form independent particles stabilized in that conformation. In essence, the particles are single macromolecules, independent of other, surrounding macromolecules.
By means of the present invention, dense, spherical particles of polymers can be made, having a high degree of uniformity as to particle size, shape and density. The particle size is largely a function of molecular weight of the polymer, a parameter which is controllable by known methods, during polymerization. Polymers of very narrow molecular weight distribution can be made by known methods of polymerization, and these will lead to stabilized polymer particles of substantially uniform particle size, following the method of the present invention. A solution of the polymer is first prepared using a solvent or mixture of solvents in which the polymer fully dissolves, and at a concentration below the critical concentration, and caused to contract into a spheroidal conformation. Then the polymer is stabilized, e.g. by cross-linking. Polymer particles of very small size, average diameter in the range 0.1-10 nanometers (nanoparticles), can be made in this way.
The resulting polymeric materials are internally cross-linked macromolecules, i.e. substantially all of the cross-links are between groups on the same polymer chain as opposed to cross-links between groups on different polymer chains to bond the polymer chains together in a network. These internally cross-linked polymers according to the invention have solution properties which are quite different from those of the same polymeric material either before cross-linking or after cross-linking in bulk. Conventional high molecular weight polymers (100,000 and higher) have high viscosity in solution, resulting at least in part from entanglement of and interaction between individual macromolecules. If such a polymer is cross-linked in the bulk phase, the resulting polymer will not dissolve in any solvent, but may swell when contacted with solvents. Internally cross-linked materials of the invention, in contrast, even with molecular weights in excess of 1,000,000 can be dispersed in a wide variety of solvents and non-solvents, but scarcely affect the viscosity of the solution or dispersion at all. This remarkable property makes these new compositions of the invention of potential utility not only in imaging compositions as described above, but also in drug delivery applications.
Thus according to one aspect of the present invention, there is provided a process for preparing polymeric material in the form of stable nanoparticles having substantially spherical particulate form, which comprises:
dissolving a polymeric material in a solvent system to form a solution of the polymeric material at a concentration therein of less than the critical concentration for the polymeric material;
causing the macromolecules of said polymeric material to contract into an approximately spheroidal conformation in solution;
and stabilizing the polymeric material in solution in said spheroidal conformation so assumed by creating intra-molecular bonds.
Stable, intra-molecularly bonded, approximately spheroidal polymeric nanoparticles can be recovered from the solution, if desired, by standard methods.
The term �intra-molecularly bonded� as used herein indicates the presence of internal cross-links or other bonds linking parts of the same macromolecule to itself, to the substantial exclusion of bonds linking different macromolecules together (�inter-molecular bonds�).
According to another aspect, the invention provides internally cross-linked particulate independent macromolecules having substantially spheroidal particle shapes, said particles having the ability to be dispersed in a liquid medium without significantly changing the viscosity of the medium.
The process of the present invention is applicable to a wide variety of polymeric materials, natural and synthetic. The polymeric materials can be homopolymers or copolymers of two or more monomers, including block copolymers and graft copolymers. It is necessary that the chosen polymeric material be soluble to a substantial extent in at least one solvent system, so as to enable it to adopt a contracted spheroidal conformation in solution, as described below.
The chosen polymeric material is first dissolved in an appropriate solvent system. This may be water, an organic solvent or a mixture of two or more such solvents. The polymeric material is dissolved such that, in solution individual macromolecules thereof remain distinct, separated and non-entangled with one another. This can be achieved by arranging that the concentration of polymer in solution is below the �critical concentration,� which is the concentration at which the individual polymer chains in the solution interpenetrate. The separated, non-interpenetrating macromolecules in solution can be condensed e.g. by changing the solution characteristics, and stabilized by internal cross-linking, to a particle size which, assuming spherical shape, can be calculated from the molecular weight of the polymer. The ability of the macromolecules to achieve a condensed particle size largely in accordance with theoretical calculations, assuming spheroidal shape, acts as a check or test that the polymer in solution, prior to condensation and cross-linking, was indeed in the form of independent, separated, non-interpenetrated macromolecules for the initial stages of the process of the present invention. A person skilled in the art can readily conduct such calculations from a knowledge of the chemistry and molecular weight of the polymer under consideration, and simple experiments to determine particle size after stabilization as described. Comparison of this with theoretical calculation and prediction can determine the critical concentration for the specific polymer solution.
Either as it dissolves (for example in the case of sodium styrene sulfonate-vinyl naphthalene copolymers and similar copolymers), or by reduction of the solvent power of the solution, for example by adding to it a precipitating non-solvent, or a salt which changes the ionization conditions of the solution, the polymer is caused to condense and to contract to dense spheroidal structures. Then it is internally stabilized preferably by cross inking, using a system which is compatible with the chosen polymer and the chosen solvent system, for example by exposure to γ-radiation. When each polymer molecule contains three or more internal cross-links, it can no longer expand to form its normal random coil configuration in solution. Instead, it retains its spheroidal confirmation, the density of which increases with the degree of cross-linking. In the case of some polymers, e.g. those having mutually reactive chemical groups such as polypeptides, stabilization may occur by reaction of these groups with one another as the polymer is caused to condense and contract, e.g. by formation of disulphide bridges, without application of a specific cross-linking step.
A wide variety of polymers and copolymers can be used in the present invention, provided only that a suitable solvent system is available for them, and that the random coils can be condensed to denser spheroidal particles prior to cross-linking. Preferred polymers have ionic charges (polyelectrolytes) so that, in the preferred aqueous solvent systems, the macromolecules are mutually repellant and less likely to agglomerate prior to cross-linking.
Examples of useful polymers in the present invention include polymers and copolymers derived from such monomers as styrene, vinyl naphthalene, styrene sulphonate, vinylnaphthalene sulphonate, acrylic acid, methacrylic acid, methylacrylate, acrylamide, methacrylamide, acrylates, methacrylates, acrylonitrile, N-loweralkyl acrylamides and the like.
One preferred embodiment of the invention involves the use of polymers having a critical solution temperature, i.e. a temperature below which they are soluble in water, and above which they are insoluble in water. Using the process of the present invention, such polymers can be dissolved in water, caused to assume a condensed, spheroidal conformation and internally cross-linked as described. They can then be used for delivery and controlled release of other organic compounds such as drugs. The drug can be dispersed in a suspension of the cross-linked polymer at a temperature above the critical solution temperature, at which the drug will be absorbed by the polymer in its collapsed-particulate form. When the temperature is reduced below the critical solution temperature, the polymer particle swells and slowly releases the drug. Polymers having critical solution temperatures include polymers of N-isopropylacrylamide (NIPAM), the critical solution temperature of which can be adjusted by copolymerization with other monomers.
Upon dilution of the solution, stage 2, below the critical concentration, the polymer macromolecules 10 are spaced apart from one another, but still in their random coil configuration. Upon reducing the solvent power of the solvent system, e.g. by introducing a non-solvent or a salt, the macromolecules condense, stage 3, into generally spherical conformation 12, and can now be cross-linked, eg. by application of ionizing radiation, at stage 4, whereupon internal cross-linking, as opposed to inter-macromolecular cross-linking occurs, effectively locking the macromolecules into the configurations assumed in stage 3. Then the cross-linked, approximately spherical macromolecule particles can be recovered e.g. by freeze drying, for use in applications referred to above.
When the macromolecule particles are re-dissolved e.g. in water, they have very little, if any, effect on the viscosity of the solvent (in any event less than a 10% resulting increase in the viscosity). This is due to the fact that the macromolecules do not agglomerate to any significant extent, nor do they expand or mutually interact to any significant extent. This unusual property renders the nanoparticles useful in a number of specialty applications. The nanoparticle macromolecules having critical solution temperature as described above are, for example, especially useful as drug carriers, where drugs are associated with the polymers in solution and delivered to very small veins and capillaries of the body, e.g. certain areas of the brain, which are so small that they cannot be penetrated by drug solutions of other than very low viscosity.
Whilst water is the preferred solvent for use in the present invention, other polar solvents can also be used if desired, alone or in mixtures with each other and in admixture with water. The best choice of solvent depends to a large extent on the choice of polymer. Polar solvents such as lower alkanols, ketones, amines, dimethylsulfoxide and the like are suitable alternatives to water, when working with a polymer of limited solubility in water.
Another aspect of the present invention comprises the use of internally cross-linked macromolecules as described above in the preparation of nanoparticles of metals, i.e. metal particles which are substantially spherical in shape, and which have an average diameter in the range 0.1-10 nanometers, preferably from 0.1-8 nanometers and more preferably from 0.1-5 nanometers. Such nanoparticles of metals comprise another aspect of the invention. This process aspect uses internally cross-linked polymers as described above, in which the polymer is a polyelectrolye such as polyacrylic acid or a salt thereof e.g. sodium polyacrylate. For example, by dissolving them in water containing a large excess of ferrous ions, the sodium ions can be replaced by ferrous ions. After removal of the sodium ions, the particles can be heated in air or oxygen to above 200-300� C. The polymer content is largely removed by pyrolysis, leaving extremely small particles of iron oxide with very large surface area and important electrical and catalytic properties. If the process is carried out in a reducing atmosphere, high surface metal particles can be obtained. Other metal salts such as silver salts (silver nitrate for example), copper salts and gold salts can be used to produce finely divided metal particles useful in imaging and, because of their very high surface area, in catalysis. Palladium, platinum, titanium and molybdenum are examples of metals which can be prepared in nanoparticle form according to the present invention, for use in catalysis. Substantially any metal which is stable in its metallic form and which has a water soluble salt can be used in this way. The metal salt can be dialyzed against the sodium polyacrylate (or similar polymeric salt) particles of the invention, to remove the alkali metal and replace it with the other metal. Then the product is reduced, e.g. by application of laser radiation, and solid metal nanoparticles e.g. silver particles, in some cases surrounded by a fine layer of residual polymer which has a stabilizing effect, are obtained.
In another modification, ionic groups on internally cross-linked polymers of the present invention, for example the sodium acrylate groups in the particles made in examples 1, 2 and 8 below, can easily be converted to other useful functional groups. Sodium acrylate groups for example can be converted converted to the corresponding acid chloride by treatment with thionyl chloride. Dye molecules containing reactive hydroxyl or amino groups can then be permanently bound to both the surface and the interior of the particles giving rise to products useful in imaging applications such as in ink-jet printing.
The invention is further described with reference to the following specific illustrative examples.
The sodium salt of poly(acrylic) acid (Polysciences Inc. Cat#18755), of molecular weight of 1,300,000, was used in a cross-linking process according to the invention. 97 mg of polymer was dissolved in 100 ml of distilled water. After solution was complete the pH was 8.2, and 98 mg of sodium chloride was slowly added to cause the polymer particles to contract. 5 cc. of the solution was flushed with nitrogen, sealed in a glass vial, and irradiated with 10 megarad of Co60 γ radiation. After radiation the vial was opened and the solution dialysed against water for 5 days to remove the salt, and the polymer particles recovered by freeze drying under vacuum. The particles were studied by atomic force microscopy (A.F.M) (film cast onto mica, to produce tapping mode AFM height image) and shown to be perfectly spherical, with diameters of 6 to 10 nanometers (see
The procedure was repeated with a polyacrylic acid (sodium salt) of molecular weight about 700,000, and the A.F.M. picture of this product is presented as
The procedure of Example 1 was repeated except that before addition of the sodium chloride the pH of the solution was reduced to 3.2 by addition of small amounts of 0.1 N hydrochloric acid. After addition of sodium chloride and cross-linking with 10 megarad of γ-rays, nanoparticles of the same size (6-10 nanometers) were observed as in Example 1 by A.F.M.
Copolymers of sodium styrene sulfonate and vinyl naphthalene containing about equal quantities of each comonomer are known to form hypercoiled pseudomicellar conformations in water, i.e. they do not form expanded random coils, but are collapsed into much smaller spherical structures with much higher coil density due to the hydrophobic interactions between the naphthalene groups and water. These particles are negatively charged due to the ionization of the styrene sulfonate groups in water. The polymers can also be internally cross-linked by the following procedure. A polymer containing 50% by weight sodium styrene sulfonate and 50% of vinyl naphthalene was prepared in benzene solution AlBN as catalyst. After isolation and purification by dialysis against pure water it had a molecular weight Mw of 200,000.
100 mg of this polymer was dissolved in 100 ml distilled water and after purging with oxygen-free nitrogen was irradiated with a dose of 0.40 megarad of Cobalt60 γ-rays. A.F.M. analysis of the resulting particles showed spherical particles with an average diameter of 7.5 nanometers. The A.F.M. picture of the particles is presented as
Internal cross-linking can be carried out by other means besides γ radiation. In some cases, irradiation of the aqueous dispersion with high intensity U.V. laser light will cause internal cross-linking. A simpler procedure is to prepare a copolymer with a small number of double bonds which can be connected by vinyl polymerization. In this example a copolymer of 50% styrene sulfonate and 48% vinyl naphthalene and 2% divinyl benzene was prepared as in Example 3. 100 mg of this polymer was dissolved in 100 ml of water to which was slowly added with stirring 1.0 cc of benzene containing 4 mg styrene and 1 mg of AIBN (azobis-iso-butyryl nitrile). After purging with nitrogen 2 cc of this mixture was heated to 70� C. for 5 hours with stirring. After isolation and purification by dialysis spherical nanoparticles were observed by A.F.M.
An additional 2 cc of the solution prepared in Example 4 was shaken with a small amount of styrene monomer and allowed to separate. Excess styrene was removed and the polymer was internally cross-linked by exposure of the solution to near ultraviolet light (λ=313 nm from the American Ultraviolet Irradiation System for 1 hour. After isolation and purification cross-linked nanoparticles with the viscosity properties of the γ irradiated materials from Example 1 and 2 were produced.
Poly N-isopropyl acrylamide (NIPAM) is an important polymer which is often used in drug delivery systems. It has a lower critical solution temperature (LCST) of 31� C. It is soluble in water below this temperature but precipitates sharply above this. This temperature can be lowered by copolymerization with hydrophobic monomers such as acrylonitrile and raised by hydrophilic monomers such as acrylamide. These co-polymers can be internally cross-linked by any of the procedures described above. In a specific example 100 mg of polyNIPAM with a molecular weight of 200,000 g/mole was dissolved in 100 ml water at 20� C. and was cross-linked with 10 megarads of γ radiation. After isolation and purification, the internally cross-linked 5-10 nm nanoparticles can be used for the controlled delivery of other organic compounds. For example the drug can be absorbed by the collapsed particle in a water dispersion above LCST. After removal of the unabsorbed drug, the dispersion will remain stable until the temperature of the water is reduced below LCST, at which point the particle swells and slowly releases the drug. Since the size of the internally cross-linked nanoparticle is extremely small (�10 nm) it can access almost any part of the human body including the smallest blood capillaries which makes it of interest in a variety of medical therapies. The delivery polymers can also be made sensitive to pH instead of temperature.
Polymers such as NIPAM, polyacrylamide and polyethylene oxide, which do not contain ionized groups, are difficult to keep separate in water solution while the cross-linking process is taking place. This reduces the yield and purify of the desired internally cross-linked nanoparticles. Cleaner products and higher conversions can be achieved by including an ionizable comonomer. A copolymer of 2% acrylic acid and 98% NIPAM was prepared. At a pH of about 8-9 in water most of the acrylic acid units will be ionized, thus giving a strong negative charge to each polymer molecule. At high dilution, this prevents the agglomeration of individual chains to form larger particles. 100 mg of this polymer was internally cross-linked by the procedure of Example 6. A.F.M. studies of the internally cross-linked particles showed a much lower concentration of larger agglomerated particles than those prepared in Example 6.
A solution of sodium polyacrylate was prepared as in Example 1, and after the addition of sodium chloride, 4 mg of 4,4′-diazidostilbene-2,2′ sodium sulfite dissolved in 1 cc benzene was added slowly with continuous stirring. After flushing with nitrogen, the ampoule was sealed and irradiated for 1 hour with 313 nm U.V. light in the American Ultraviolet Irradiation system. After irradiation the product was isolated by freeze drying and purified by dialysis as in Example 1. A.F.M. measurements showed particles similar to those found in Example 1.
Nanoparticles of polyacrylic acid sodium salt prepared according to Example 1 were dialysed against dilute hydrochloric acid to remove the sodium ions, and then treated with excess silver nitrate in aqueous solution to form the silver salt of the acrylic acid groups in the polymer particles. Irradiation of these particles in aqueous dispersion with γ-radiation (10 Mrad) gave a dark orange solution. The UV-visible spectrum shown in
After isolation of the particles and drying of them, spherical particles of diameter about 5 nm were observed by AFM. An electron microscope examination (TEM),
The average diameter of the reduced silver particles was 3.5�0.53 nm. The diameter of the exterior, including the hazy region, was 5.2�0.8 nm. The particle size distribution is shown on
Similar results were obtained by irradiation of the original salt particles with an intense laser pulse from a picosecond quadrupled Nd:YAG laser or XeF excimer laser, and by a chemical reducing agent such as sodium in liquid ammonia.
Similar experiments with iron and copper salts gave similar results, with aqueous solutions giving rise to various colours, depending upon the size of the particles.
Further evidence of encapsulated particles is shown on
Larger particles of polyacrylic acid salts and other polymers for the preparation of metal particles by the process of the invention can be made by emulsion polymerization in the absence of surfactant, by the method of O'Callaghan et.al, Journal of Applied Plymer Science, Vol 58, 2047-2055 (1995). This paper describes a method of making monodisperse polymer latices with sizes of 40 nm and higher.
By following the procedure of this paper, there was prepared a copolymer of butyl acrylate (30%) with acrylic acid (70%), cross-linked with 3% divinylbenzene. The average size of these particles was 230�20 nm. Treatment with silver nitrate as in Example 9 followed by laser irradiation with the Nd:YAG laser while stirring the aqueous dispersion gave silver containing nanoparticles about 200 nm in diameter.
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NASCAR - Danica Patrick and Kurt Busch looking to defy historyDavid Newton
Kurt Busch could win the Indy 500. Danica Patrick could win the Coca-Cola 600. Which is more likely? It might be a tougher equation than you think, David Newton writes.Story | Conversation | May 24, 2014
Roger Penske says he won't renege on Indy 500 offer for Tony Stew...David Newton
Team owner Roger Penske wasn't happy with Tony Stewart's comments about one of his drivers Sunday, but not enough to rescind his offer to one day put the three-time Sprint Cup champion in the Indianapolis 500.Story | Conversation | March 26, 2013
Tony Stewart hasn't shut door on Roger Penske Indy offerDavid Newton
Tony Stewart is open to running the Indianapolis 500 for Roger Penske, sometime after this season.Story | Conversation | January 21, 2013
Danica Patrick confirms she won't run in 2013 Indianapolis 500David Newton
Danica Patrick confirmed on Thursday that she will not participate in the 2013 Indianapolis 500, but she didn't rule out future ones.Story | Conversation | January 10, 2013
NASCAR - Sam Hornish Jr. looking for old Brickyard magicDavid Newton
Sam Hornish Jr. will be introduced as the 2006 Indy 500 winner Sunday. It would be helpful to his career if he can truly compete for the title of 2012 Brickyard 400 winner.Story | Conversation | July 28, 2012
Danica Patrick to race Coca-Cola 600, skip Indianapolis 500David Newton
Danica Patrick has added the Coca-Cola 600 at Charlotte Motor Speedway to her 2012 Sprint Cup schedule, eliminating any possibility she will run in the Indianapolis 500.Story | Conversation | January 23, 2012
NASCAR's Dale Earnhardt Jr. almost upstaged the Indianapolis 500David Newton
About the only way the Coca-Cola 600 could have upstaged the 100th anniversary of the Indy 500 was for Dale Earnhardt Jr. to celebrate in Victory Lane. Too bad Junior ran out of gas.Story | Conversation | May 29, 2011
Sam Hornish Jr. is happy in NASCAR but realizes he can't rest on ...David Newton
Sam Hornish Jr. is still trying to make his way as a NASCAR driver. That sits just fine with the 2006 Indy 500 winner, and so does the reality that that win means little -- on the track -- to his competitors.Story | Conversation | May 29, 2010
An Indy 500 weekend double by Danica Patrick would be a boon for ...David Newton
CONCORD, N.C. -- Marcus Smith was finishing a chicken quesadilla at the Speedway Club atop Lowe's Motor Speedway on Tuesday afternoon when the conversation turned to Danica Patrick. The president of LMS was asked what it would mean to NASCAR if the ...Blog | Conversation | October 06, 2009
Brickyard winners not just paying lip service with traditional po...David Newton
It's all about the milk at the Indy 500. The Allstate 400? It's all about the kiss. With apologies to Snow White, the most meaningful smooch happens this time every year at Indianapolis Motor Speedway, writes David Newton.Story | Conversation | July 23, 2008
Grand-Am Series finding a niche in so-called country club circuit...David Newton
Series boss Roger Edmondson calls it the "best road racing on the planet." Former Indy 500 rookie of the year Scott Pruett says it is some of the best racing, period. Welcome to Grand American Road Racing, NASCAR style.Story | Conversation | April 30, 2008
Montoya nearly pulls off impossible at the BrickyardDavid Newton
Juan Pablo Montoya made headlines by winning the 2000 Indy 500. Seven years later, he almost won again at the historic track -- but this time in a stock car, writes David Newton.Story | Conversation | July 29, 2007
NASCAR - Jimmie Johnson roars to life - Coca-Cola 600David Newton
Jimmie Johnson winning the Coca-Cola 600 to end a season-long victory drought was not the most compelling storyline Sunday. But it was the most predictable, writes David Newton.Story | Conversation | May 25, 2014
NASCAR - Best drivers in the world? It's relative - Indianapolis ...David Newton
Jimmie Johnson is a five-time Sprint Cup champion. So it stands to reason the surefire Hall of Famer would hold his own in, say, the Indianapolis 500, right? It's not that simple.Story | Conversation | May 24, 2013
NASCAR - Danica Patrick and Brooklyn Decker share spotlight at Co...David Newton
CONCORD, N.C. -- The Indianapolis 500 was drawing to an end on Sunday and Danica Patrick was standing in Victory Lane at Charlotte Motor Speedway with supermodel/actress Brooklyn Decker. If Patrick's mind was on the IndyCar Series she left after las...Blog | Conversation | May 27, 2012
NASCAR - Dream weekend for Roger Penske?David Newton
Memorial Day weekend could prove to be a dream weekend for Roger Penske, who's sure to be the busiest man on motor racing's busiest day.Story | Conversation | May 26, 2012


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