Single Crystal X-ray Diffraction experiments were conducted at Colorado State University using a Bruker D8 Advance Quest equipped with an Incoatec Microfocus Source (I µS) of 3.0 and II microfocus X-ray sources. Crystals (measuring 50 µm on a side) were isolated in a paratone oil and mounted on a goniometer base B3-R, MicroRT, using micromounts of 100 µm. An Oxford Cryostream system gradually cooled the crystals to 100 K to ensure stability and temperature control. Smaller data sets collected at 300 K and 150 K revealed that the crystals were twinned during growth and not during cooling. The experiment employed monochromatic Mo Kα radiation (λ = 0.71073 Å), with data processing carried out using the Bruker APEX4 suite of programs. Briefly, the data from non-merohedral twins were "detwinned", frames scaled, merged, and corrected from absorption via TWINABS. The crystal structure was initially solved using charge flipping implemented in Olex2 and refined using SHELXT using reflections assigned to the primary twin domain and refined against multiple twin domains via SHELXL in Olex2 employing the de-twinned reflections (e.g., HKLF5).