[Cu4(MeOL)2(CH3L)2], and [Cu4(MeOL)(CH3L)3] using IR spectroscopy and PXRD suggest that the samples retain the same packing as their MeOH solvates, indicating that the samples do not decompose after activation (Fig. ). The 1 H-NMR spectra of digested samples show that the scrambled cage [Cu4(MeOL)3(CH3L)] retains 0.06 MeOH/cage (Fig. ), which we attribute to MeOH coordinated to the paddlewheel. Previously, we had observed that subsequent to activation the homoleptic cage [Cu4(MeOL)4] also retained MeOH, but to a greater degree, with a solvent content of 0.4 molecules of MeOH per molecule of cage.