Figure presents the evolution of the d 115spacing values for each of the found particles during a scan in addition to the d-spacing values of the particle measured with SXDM. During charging, phase transitions in the crystal imaged by SXDM occur with a slight delay compared to the whole sample (see Figure ). This could be a sign of the beam reacting with the surrounding electrolyte and slightly inhibiting the charge rate, however the matching evolution of the d-spacing for both cases confirms that X-ray radiation does not significantly affect the lattice of the cathode itself. Another apparent feature is the variation of phase transformation between particles. While most of the crystallites follow the characteristic two-phase evolution of the Bragg reflection (as observed in Ref. ) several particles exhibit a solid solution transformation prior to the rest of the ensemble.