X-ray photoelectron spectroscopy (XPS) measurements were acquired on a Kratos Amicus X-ray spectrometer with a dual anode monochromatic Kα excitation source. All binding energies were calibrated against the adventitious carbon C 1s peak at 284.8 eV. Here, we used X-ray photoelectron spectroscopy (XPS) to analyze the chemical states of the constituent elements of hybrid coordination crystals and glasses. After the measurement, the data were fitted and analyzed using the XPSPeak 4.1 software.