Figure depicts DPV of the nanosheets in 0.1 M n-Bu4NPF6/CH3CN on a Pt disc electrode (blue curves) against the background of the bare Pt electrode (orange curves). All measurements are initiated at the OCP of the uncoated electrode at -0.2 V and the electrochemical measurement window for this electrolyte is +1.8 V to -2.8 V. In both scan directions, the current already starts to increase/decrease slightly in the vicinity of the OCP. In the oxidative direction, we observe a broad peak at 0.77 V, including a shoulder at 0.37 V. At even more oxidative potentials, the current increases further, however without a distinguishable feature. In the reductive direction, we find a small peak at -1.18 V and a prominent peak at -1.83 V. The intensity of the second peak continuously drops towards more reductive potentials, but with a much flatter flank compared to the onset, suggesting that further reductive processes are buried within this signal.