The production of nanoporous Fe-fumarate (MIL-88A), with crystals 100 nm in size, was facilitated through ultrasound. Iron (III) chloride hexahydrate and fumaric acid were combined in a sealed glass flask and heated to 50 ºC in an ultrasonic bath. The reaction parameters, shape, crystalline nature, and yield of generated products were specifically influenced by the Fe content synthesis time, and the base contents . Without the use of a solution phase surfactant, catalyst, or template, according to Tehrani and co-workers, Zn3(BTC)2 nanorods may be generated under ultrasonic conditions . In a further study, the combinations of the iso structures Ln(BTC)(H2O) were created utilising (BTC)3 as the linker (Ln = Ce, Tb, or Y). Tb substance was previously produced by ordinary heating, however, by using ultrasonication, the reaction temperature and time may be reduced to 20 minutes and 40 ºC, respectively. 23 lm-long highly crystalline particles were produced. Based on N2 sorption investigations , these compounds also displayed exceptional physical properties. NaOH and triethylamine were used in a sonochemical process with pH-adjusted synthesis conditions to create ZIF-8. In brief, 50 mL of DMF, 0.7 mL of triethylamine, 2 mM zinc nitrate hexahydrate, and 2 mM HMeIm were mixed.