In summary, the methods developed in this study acts as a preliminary approach for the large-scale standardisation and analysis of experimental synthesis data, representing the first step in creating a closed feedback loop for the automated optimisation of experimental nanomaterials synthesis. By interfacing with automated and high throughput reactionware e.g. through integration of the XDL chemical programming language, methodology development will be significantly accelerated thereby easing the adoption of nanomaterials at larger scales and in new settings.