To further showcase the synthetic potential of our method, we investigated the scalability of our continuous-flow procedure (Scheme 4). It is worth noting that during the scope investigation, we observed that the stainless-steel sacrificial anode could be reused over 50 times without noticeable degradation in electrode performance (Table ). Leveraging this robustness, a scale-up experiment was conducted to produce over 4 mmol of 2b during a 49-hour uninterrupted run, achieving an isolated yield nearly identical to that obtained on a 0.2 mmol scale. This indicates that anode surface degradation and potential cathode passivation over extended operation times remain minimal (Scheme 4A). Additionally, after a brief re-optimization of the protocol for the cyclopropanation of 6b (Table ), we enhanced throughput per reactor from 112 to 448 µmol•h -1 by connecting five electrochemical flow reactors in series. This setup enabled the isolation of 2.47 g of 2b without significant yield loss, highlighting the advantages of continuous-flow technology for scaling up electrochemical processes (Scheme 4B).