Ex-situ SAXS/WAXS measurements were conducted using the MOUSE instrument . In a microfocus X-ray tube attached with parallelizing and monochromatising multilayer optics, Xrays of a distinct wavelength of Cu Ka (λ = 0.15406 nm) were generated. An in-vacuum Dectris Pilatus 1M, was used to measure the scattered signal. The sample-to-detector distances allowed for a q-range of 0.015 < q < 40 nm -1 in a combined SAXS/WAXS approach. The synthesized powders were sealed on a sample holder from both sides with Scotch© tape and hold into the beam. The obtained data was corrected according to the procedure in the literature .