NMR spectroscopy was used to study β-alanine acrylamide (BAA), a monomer that was created by a simple reaction between β-alanine and acryloyl chloride. Acryloyl β-alanine monomer's production was verified by 1H NMR (Figure .1), which revealed a double bond peak in the monomer at 5.0-6.0 ppm. The production of acryloyl β-alanine monomer is confirmed by the IR peaks at 1644 cm-1 (C=C) and 1463 cm-1 (C-N). The synthesis of the monomer is confirmed by the NMR stack plot between β-alanine and acryloyl β-alanine monomer in (Figure .2). The monomeric double bond was absent in β-alanine but in acryloyl β-alanine the peak 5.0-6.0 ppm was confirmed the double bond peak. The Zn-mediated polymerization of acryloyl βalanine was confirmed by NMR 1.05, 1.30 (CH3 of EBiB initiator, signal a,b) 3.40, 2.51 (CH2 of β-alanine, signal e,f), 2.08 (-CH2 of PBAAM repeating unit). With a pKa of about 3.5, polyβ alanine is a special kind of polypeptide that may react to changes in physiological pH by being protonated and deprotonated within physiological ranges, which changes the polypeptide's hydrophilicity. Furthermore, direct polymerization of amino acid-based monomers with specialized functional moieties often suffers from inherent limits since monomer functionality is incompatible with polymerization conditions. One effective way to get around these problems and create the appropriate polymeric materials with multifunctional compositions was to modify reactive macromolecular scaffolds using a process called post-polymerization modification (PPM). In order to achieve PPM, monomers containing chemo-selective pendant groups-which can be activated under postpolymerization conditions after being inert to polymerization conditions-must be directly or copolymerized.