Figure shows the diffraction patterns of the recycled Li3InCl6 after separation from different electrode materials and subsequent recrystallization. All diffraction patterns (see Figure ) and the determined lattice parameters (see Table ) confirm the successful recovery of crystalline Li3InCl6. Rietveld analysis reveals deviations in the lattice parameters compared to those of the pristine sample. The relative change in cell volume, in relation to the volume of the pristine sample, is given in Figure . It was observed that the cell volumes increased for all recycled electrolytes, except for the recycled Li3InCl6, after separation from NCA. These variations in lattice parameters may be attributed to ion-exchange processes, which result in alternations in the Li-In-Cl ratio.