Data was collected from the scaled-up reaction (Table , entry 9) and extrapolated to 1 g scale with a 6.5 factor (Table ). A yield of 98% was assumed, which was in line with the ratio between starting material and product. The final fraction was comprised by a mixture of cyclohexanone and cyclohexenone in a 98:2 ratio. A fractional distillation would be the reasonable stage in purification. Nevertheless, data could not be collected as this equipment was not present in our laboratory.