In this work, we applied the Synthetic Conditions Finder (SyCoFinder), which is the web-application based on the methodology developed by Moosavi et al., to find the optimal synthesis conditions for Al-PMOF (H 2 TCPP[AlOH] 2 (DMF 3 (H 2 O) 2 )), first synthesized by Fateeva et al. Unlike HKUST-1, our knowledge of alternative synthesis conditions of Al-PMOF is very limited. To the best of our knowledge, to date only one synthesis condition, a hydrothermal reaction, has been reported. Unfortunately, this synthesis gives a relatively low yield (ca. 40%) with the reaction time of 16 hours. Recently, there has been a renewed interest in this MOF as Boyd et al. discovered that this material can efficiently capture CO 2 from wet flue gasses. However, the low yield and relatively long reaction time of the current reaction is at present a bottleneck to scale-up the synthesis. It is therefore important to investigate whether the yield and time of the reaction can be further optimized. In addition, it will give us some insights whether the approach developed by Moosavi et al. can be extended to other MOF systems.