Transmission electron microscopy (TEM) analysis was performed using a Talos F200i microscope (Thermo Fisher Scientific) operating at 80 kV. Samples were prepared through sonication in ethanol and deposition on a lacey carbon-coated copper TEM grid by dropcasting. Powder X-ray diffraction (XRD) patterns of the MoS2 materials were obtained by using a Bruker D8 Advance diffractometer operating in Bragg-Brentano geometry with a Cu Kα radiation source (λ = 1.5406 Å). Raman spectroscopy measurements were obtained by using a Renishaw InVia confocal Raman microscope with a 532 nm laser at a low power of 100 µW. Sorption isotherms of N2 at 77 K were recorded with the use of ASAP 2460 (Micromeritics, USA). The materials were degassed in a flow of helium at 100 °C for 12 h. Prior the N2 sorption, the samples were degassed in vacuum for 6 h. Brunauer-Emmett Teller (BET) model was utilized to evaluate the specific surface area (SSA) using 0.01 to 0.05 P/P0 range. The elemental composition of prepared samples was evaluated by using Thermo Fisher Scientific FlashSmart Elemental Analyzer. The elemental content of C, H, N, S was estimated in the column filled with copper and copper (II) oxide during incineration at 950 °C. Separate pyrolysis of samples at 1060 °C in a column filled with nickel coated carbon was used to estimate the content of O.