Electrochemical exfoliation is a widely used method for synthesizing graphene oxide (GO) due to its efficiency and scalability. The application of voltage leads to the intercalation of anions into graphite, causing exfoliation and oxidation. Research has shown that adjusting anodic voltages significantly influences the yield and quality of GO. For instance, Pei et al. demonstrated the effectiveness of water electrolytic oxidation in producing high-quality GO within seconds . Additionally, Chen et al. reported a photosynergetic electrochemical approach that improves GO synthesis by utilizing light to enhance the electrochemical process . Carbon-based fibers derived from electrochemical synthesis are also showing promise for advanced energy storage applications . The use of carbon-based materials as electrodes in supercapacitors has been extensively studied, with excellent results in terms of capacitance and conductivity .