In addition to organic synthesis, the slug-flow methodology (SFM) has found application in polymer synthesis and is worth citing to understand SFM's wider utility. A flow platform capable of polymerizing 397 unique copolymer compositions was developed by Reis et al. using a droplet flow reactor. The methodology and highfidelity data enable them to discover >10 copolymer compositions of promising 19 F MRI agents that outperformed state-of-the-art materials. A rapid generation of copolymer libraries was achieved by forming droplet-flow in an automated HTE flow setup . This approach not only assists in overcoming the challenges of viscosity in conventional photopolymerisation reaction, but also generates structure-property relationships for co-polymer libraries. We have generated a segmented flow pattern (Figure ) by alternating the infusion of organic components and degassed water to create 9 different compositions . The organic components consisting of styrene, AIBN (α,α′-Azobisisobutyronitrile), and p-Xylene were infused using a computercontrolled segmented-flow platform. These approaches allow the compartmentalization of reaction mixtures without cross-contamination and enhance experimental throughput significantly.