By employing this streamlined flow process, compound 40 was obtained with an 86% yield after isolation through column chromatography. It is noteworthy that the use of flow conditions allowed for a reduction in both the nickel (5 mol%) and photocatalyst loading (2 mol%), while still yielding comparable results to the batch process. Importantly, this flow approach facilitated easy scalability of the transformation to a 25 mmol scale without the need for reoptimization of the reaction conditions.