Figure shows that without the NF substrates the XRD diffraction peaks are located at 10.94 QDs. The increased interlayer spacing in the 1T phase of MoS 2 has been attributed to the intercalation of NH 3 /NH 4 + between the S-Mo-S layers during the MoS 2 electrodeposition carried out in a NH 4 -containing electrolyte. The XRD analyses of NiFeCo-Mo(doped)-LDH and MoS 2 @NiFeCo-Mo(doped)-LDH without NF substrate reveal that Mo doping reduces the diffraction peak intensity, increases peak width, and shifts the peals to a higher angle; together these observations imply that Mo doping makes LDHs more amorphous by either decreasing the LDH crystallinity or by increasing layer irregularity.