To address this issue, inspired by previous works on electrochemical synthesis platforms, we developed a rapid screening electrochemical platform capable of conducting multiple reactions simultaneously, thus enabling both reactivity screening and optimization of synthesis conditions. This platform features a standardized 24-well plate electro-synthesis reactor (Figure ), which includes a water jet-cut anode and cathode connectors, an alignment plate, and a vial locator. Components for the reactor are readily available through commercial vendors and can be easily assembled at low cost in the lab (See Supporting Information Section S2 for detailed design and assembly information). Furthermore, the choice of electrodes can be adjusted to meet specific experimental needs, enhancing the flexibility of our setup. The experimental setup includes 4 mL electrochemical reactors with two pairs of counter electrodes, totaling four electrodes (Figure ), and it allows for increased surface area and improved current distribution, which enhances mass transport. Such improvements facilitate the diffusion of reactants to the electrode surfaces and the efficient removal of products. Additionally, dual-electrode setup ensures that the reaction can continue even if one pair fails or loses connection, thus improving the reliability of the experimental setup.