Bare framework 0.822 Half Cu-sites occupied by water 0.761 All Cu-sites occupied by water 0.706 Half Cu-sites occupied by DMF 0.605 All Cu-sites occupied by DMF 0.446 Among the isotherms showing too high pore volume, we identified one case of a typo in the units of the isotherm graph (mmol/g instead of the more plausible cm 3 (STP)/g), resulting in an experimental pore volume that dramatically exceeded the geometric one (11.34 vs.