Measurements were taken on a Bruker Avance 700 instrument. The 90° pulse was calibrated before each measurement session, and the samples were allowed to relax for 20 s between pulses so quantitative concentrations could be extracted. The chemical shift of the spectrum was referenced to the 𝛼 hydrogens of tetrahydrofuran with a chemical shift of 3.580 ppm. The bound and unbound ligand peaks were fitted and areas integrated using the software MestreNova, and concentrations of both populations were calculated using the ratio of areas between the ligand peaks and the mesitylene peaks. Uncertainty in the integrated areas was estimated at 5%.