One of the identified XFC failure pathways is graphite anode degradation, which includes Li plating, loss of inter-particle connectivity, and delamination of anode from the current collector. Investigating the origins and characteristics of anode degradation spatially in three dimensions (3D) is imperative to understand its role in capacity fade and battery failure. Numerous methods have studied graphite anode degradation in LIBs. These include electrochemical methods, spectroscopic methods, optical imaging/microscopy, scanning electron microscopy, focused ion beam-scanning electron microscopy, transmission electron microscopy, scanning probe microscopy, X-ray micro-computed tomography (µCT), 22 X-ray diffraction (XRD), and Xray diffraction computed tomography. Each of these methods have their own advantages and trade-offs. For example, although X-ray µCT allows non-destructive 3D visualization of the anode microstructure, traditional absorption-based X-ray µCT offers poor absorption contrast for low-Z elements such as Li and C at high X-ray energies (e.g., 40 keV) that are needed to penetrate the full LIB cells. Thus, our objective is the exploration of non-destructive alternative methods for 3D visualization of graphite anode degradation from XFC with sufficient spatial resolution and contrast.