The cyclic voltammetry plots depicted in Figure reveal the distinct oxidation potential signature of the BTMAPAQ(CO2)2 a flow cell comprising 12 ml of 0.1 M 1,5BTMAPAQ paired with 40 ml of 0.2 M BTMAPFC. Figure presents the measured parameters-voltage, pH, upstream gas ratio, measured partial pressure of CO2, and flow rate at the downstream-during this experiment. While the CO2 sensor and flowmeter provide the total amount of capture and release, they are unable to differentiate the specific mechanism contributing to the overall capture. Hence, in the electrolyte path to the battery, we introduced a reference electrode to measure the real-time potential of the negative electrode against the reference electrode. Utilizing this setup, the cell was intentionally charged in a nitrogen environment, followed by a controlled purge with 0.1 bar CO2 and 0.9 bar of N2 for varying durations (60 minutes in Figure ), followed by a switch back to the nitrogen environment. This experimental procedure with different purge durations (15, 30, and 60 minutes) was intentionally designed to allow us to control the amount of adduct formation during the course of the experiment and examine its relationship with the discharge voltage profiles.