The liquid reaction mixture was analyzed by nuclear magnetic resonance (NMR) to identify the organic compounds present. The recorded 1 H-NMR spectra before and after electrolysis, shown in Figure , indicate that the cyclohexanone peaks almost disappeared after the reaction, while new peaks aligned with pure cyclohexanone oxime emerged, confirming the successful conversion of cyclohexanone into cyclohexanone oxime. The 13 C-NMR spectrum obtained for the reaction mixture after electrolysis also supported the formation of cyclohexanone oxime (Figure ).