The prompts used for each task are detailed in the Supporting Information (Figure ). For the synthesis conditions extraction task, the LLMs were instructed to extract synthesis parameters for MOF products, including temperature, concentration, reagent quantities, and solvents. Importantly, the LLMs were explicitly instructed to exclude any characterization data, such as analytical measurements, ensuring the focus remained solely on synthesis-related details. This exclusion criterion was a key part of our evaluation to maintain the relevance of extracted information.