The experimental setup for nanoaggregate synthesis and analysis included three peristaltic pumps, a micromixer, a Y mixer, and a flow cuvette. Peristaltic pumps (Vapourtec, SF-10) were chosen over syringe pumps to handle larger volumes of Milli-Q water, block copolymer stock solution, and diluting solvent. The pumps used in this study are generally highly accurate in delivery and show little pulsation in the flow. The block copolymer stock solution and tetrahydrofuran (THF) were combined at the Y mixer to produce a diluted block copolymer stream at the desired concentration. This stream then merged with water at the micromixer, where intense turbulent mixing occurred, leading to the formation of nanoaggregates. These nanoaggregates were subsequently flown into a cuvette that is placed prior into an DLS instrument for real-time analysis.