Powder X-ray diffraction (PXRD) measurements were performed on a Bruker D8 Discovery equipped with a Cu K α source using a Bragg-Brentano geometry. In the incident beam, a focusing Goeble mirror and a 2.5 • axial Soller Slit are installed. In the diffraction beam, Q region. The SCT acquisition protocol consists of 5 scans with a constant step size of 0.025