A new prefocused halogen lamp was used for generating enough strength of the light beam. The measurements were performed at 22 o C. Since polymer 1C was proven to show a high specific rotation at 22 o C with fw of 20%, five other samples were then examined for optical rotation amplification under the same condition. Within a few initial minutes, the solutions containing these multilayer polymers and oligomers cannot rotate plane-polarized symmetric lights elliptically to either right-or left-handed direction, which is similar to case 1 in Figure . Asymmetric elliptical polarization started to occur in the right-handed direction after their solutions remained in the polarimeter for 7 -12 minutes. Their highest peaks reached a range of 1660 o to 2080 o , which is close to that of polymer 4C. More specifically, optical rotation amplification for 1A and 2B did not occur until the samples were kept inside the polarimeter for 7 and 9 minutes prior to the maximum specific rotation at 1850 o and 1660 o , respectively. Polymers 1C and 2C showed broader periods of optical rotation amplification for over 30 min as compared with the other four cases.