To address the final aspect of reproducibility, our platform proves validity in both electrode fabrication and electrochemical measurements. The use of screen-printing to create miniaturized, defined areas of measurements not only saves materials but also facilitates automated ex-situ analysis. This is attributed to the precisely arranged grid of measurement positions established by the screen-printed mask on the substrate. Further enhancements in future studies can be achieved by integrating XRF measurement results into the platform, allowing for the identification of mask defects and the selection of points with minimal deviation, thus reducing issues related to electrode thickness variation. Such variations can also effect the distance between the WE and RE, potentially leading to deviations in measurements . These challenges can be further minimized by directly coating onto the substrate holder and avoid the use of a bendable foil for electrode fabrication. The consistency of our high-throughput electrochemical protocols, along with their correlation with XPS results that aligned with findings in the literature, further underscore the reproducibility and fidelity of our system. Auto-MISCHBARES enables in-depth investigation into the synthesis of SEI/CEI, especially for post-lithium battery materials, an area that still holds vast potential for exploration.