The Cu26Pd74 oxidation catalyst was synthesized by a dynamic H2 bubble template assisted galvanostatic electrodeposition method using an activated Ni foam as scaffold. The electrodeposition was carried out in a single compartment three-electrode configuration, where a leakless double junction Ag/AgCl electrode (sat. KCl, Metrohm, Switzerland) was used as a reference electrode, an activated Ni foam scaffold was used as the working electrode, and a Pt foil (~6 cm 2 area) was used as the counter electrode. The electrolyte solution contained a total 0.02 M solution of CuSO4•5H2O and Na2PdCl4 salts with a Cu 2+ :Pd 2+ molar ratio of 30:70. The galvanostatic electrodeposition was carried out by applying a current density of -2 A cm -2 for 40 s. The formed bimetallic catalyst was then washed with Milli Q ® water multiple times to remove any residual salt and acid and was subsequently dried under N2 flow.