A colorless block with approximate orthogonal dimensions 0.258 x 0.403 x 0.434mm 3 was placed and optically centered on the Bruker Duo [Error! Bookmark not defined.] APEXII CCD system at -183°C(90K). Indexing of the unit cell used a random set of reflections collected from three series of 0.5° wide w-scans, 10 seconds per frame, and 30 frames per series that were well distributed in reciprocal space. Five w-scan data frame series were collected [MoKa] with 0.3° wide scans, 20 seconds per frame and 606 frames collected per series at varying φ angles (φ=0°, 72°, 144°, 216°,