In addition, it was evident that the evolution of the enantiomeric excess of the sublimated part varied more markedly the further the initial value of the scalemic sample moved away from the presumed eutectic ratio of the two enantiomers. Analogously for the intermediate cases of TLA with 20% ee, 30% ee, and 60% ee the high speed at which the sublimation occurred did not allow for a complete enantioenrichment or enantiodepletion of the residue.