Powder X-ray diffraction (XRD) patterns of the MoS2-based materials were obtained in Bragg-Brentano geometry using a Bruker D8 Advance diffractometer operating with a Cu Kα radiation source (λ = 1.5406 Å) using a 0.02° step size and a dwell time of 1 s. Powder size distribution analysis was performed using a laser diffraction particle size analyzer (Mastersizer 3000, Malvern) to measure the size of non-spherical particles by the dynamic light scattering (DLS) method. A mixture of isopropanol and deionized water (1:1 volumetric ratio) was used as a dispersant. Raman spectroscopy was performed on bulk powder samples using a Renishaw InVia confocal Raman microscope with a 532 nm excitation laser. The laser power was kept at 100 µW to prevent the oxidation of samples. At least three different spots were investigated to check the homogeneity of samples.