While our methods are generally applicable, our focus is solving the harder challenge of high viscosity and non-Newtonian behaviour of the analyte, which will be our principal consideration, i.e., this material parameter is likely to have an impact on design choices for almost all steps of the workflow. The addition of aqueous titrant to a viscous analyte requires a homogenisation technique that can generate high shear rates and induces convective flow that collect material from the edges of the container. Finally, the complete removal of reactants that have come into contact with parts of the titration platform between unit operations is critical for minimising cross-contamination between samples -highly viscous samples likely require chemo-mechanical techniques for effective cleaning.