In conclusion, we evaluated the versatile, robust, and scalable synthesis of C-O bonds via nickel electrocatalysis. The reaction was initially investigated in batch reactors, addressing critical reproducibility issues of untreated RVC electrodes. The transformation was successfully transferred and optimized using a flow electrochemical reactor. The flow protocol was validated both in terms of robustness and scalability. Overall, we anticipate that this work provides valuable insights on the flexibility of electrochemical organic synthesis and its potential applications in medicinal and process chemistry settings.