For the untargeted LC-HRMS measurements, a quality control procedure was applied. This procedure involved preparing a process blank and a pooled quality control (QC) following the sample preparation procedure. For the process blank sample, material was omitted, while the QC sample consisted of combining approximately 5 mg of each sample (Table .3). During each extraction step of the QC, the supernatant was split by transferring 150 µL into two separate vials.