Despite over a hundred years of precedent in the field of electrochemistry and electrode science, deliberate efforts to explore new electrodes for use in synthetic organic chemistry are still rare. This study leverages materials science developments and cross-application to solve a pressing problem for the scale-up of reactions that require delicate or expensive RVC-and GC-based electrodes, respectively. The PC electrodes described herein are commercially available from IKA and KULR to facilitate immediate adoption of this electrode in the synthetic community. It is anticipated that further exploration of PC and related electrode materials may offer unique opportunities for chemical reactivity and such studies are underway.