Synthesis of organic molecules for electronics experiments was carried out using Suzuki-Miyaura cross coupling (SMCC) by leveraging recent advances in iterative automated synthesis . Prior SMCC conditions for automated synthesis require more than twelve hours to prepare one molecule . Manual synthesis requires even longer time scales to synthesize a library of small molecules . In this work, we used automated iterative coupling based on a new rapid SMCC method (Supporting Information Section S1-S3) that significantly decreases the reaction time to ten minutes with high yield .