Similar to previous experiments, the photochemistry was conducted in the Signify Eagle Reactor, utilizing PFA tubing with a 0.8 mm I.D. However, for this campaign, chip-on-board blue LEDs with a tunable light intensity ranging from 0 to 188 W were employed to match the absorption maximum of the Ru(bpy)3 photocatalyst. It is important to note that due to the short residence times, as low as 10 s, the internal volume of the photoreactor had to be reduced to 0.26 mL. This adjustment was necessary as the syringe pumps were unable to handle the high flow rates required with a larger internal volume.