It is also worth noting that the acylation/C-H chlorination cascades starting either from the acid chlorides or the carboxylic acids can be performed on a 0.5-1 g scale when using carbon cloth as both cathode and anode (Scheme 8). Here, we were able to prepare the compounds 3, 62, 67, 152, 156, 168 and 172 in 50-97% yield, without any significant negative effects on the reaction performance due to the increased scales.