Due to the apparent advantages of electrochemical processes, their implementation in flow is simple and straightforward since further dilution or additives are unnecessary . One early example of this combination in the field of HVI chemistry is the . Therefore, we attempt to transfer our already established one-pot procedure towards CDIS 1 into a multi-step electrochemical flow process, improving reaction times, atom economy, and scalability (Scheme 1, C). Scheme 1: Synthesis of acyclic (DIS) and cyclic (CDIS) diaryliodonium salts.