Experiments were performed in a Mettler-Toledo EasyMax TM 102 using a 100 mL glass reactor equipped with an overhead stirrer, temperature probe, and SP ̶ 50 dosing unit, see SI for details. Execution of experimental events (e.g., dose solvent, stir reaction, change temperature) and recoding of process parameters (e.g., reaction temperature, rate of solvent dose) are handled via iControl running on the adjacent laptop. The webcam was placed inside a 3D-printed enclosure that served to hold the camera in a fixed location, align the camera with the reactor window and block peripheral light to provide consistent illumination during experimental operation. The HeinSight2.0 model was run on the control laptop to provide real-time image analysis and data extraction. Data acquired by our model was imported live into iControl (via iC Data Share) for trend visualization and, where necessary, real-time feedback for workflow control. See SI for additional setup details.