The synthesis of [Pd(2-pymo)2]n was carried out according to the previously reported route. The resulting MOF occurs as a fine yellow powder. The quality of the material was characterized by N2 physisorption and structural confirmation by XRD. From the measured isotherm (Figure ) the BET specific surface area was determined in the relative pressure region p/p0 = 0.009-0.1 to be 600 m²g -1 . Both the isotherm and the BET specific surface area precisely match the ones reported in literature and thus, demonstrate a very robust and reproducible synthesis. The powder X-ray diffractogram (Figure ) indicates an exact match between the calculated and the experimental patterns. Additionally, X-ray fluorescence measurements (SI Table ) prove the expected composition. SEM and STEM images (Figure and Figure ) of the synthesized [Pd(2-pymo)2]n show uniform shapes, sizes and morphology of the particles.