Cyclic voltammetry (CV) was conducted in the same reaction set up to investigate the electrochemical behavior of magnesium in a 0.5M Mg(ClO₄)₂ electrolyte dissolved in DMF with 0.065M ethanol as a proton donor. The CV profile, recorded between -4 V and 4 V vs. Ag/AgCl at a scan rate of 10 mV/s, exhibits distinct cathodic and anodic features corresponding to magnesium deposition and stripping processes, respectively as shown in Figure . On the cathodic sweep, a significant current onset at approximately -2.45 V vs. Ag/AgCl indicates the reduction of Mg²⁺ ions to metallic magnesium on the working electrode. During the reverse anodic sweep, an oxidation peak is observed around 1.45 V vs. Ag/AgCl, signifying the stripping of deposited magnesium 26 back into the electrolyte as Mg²⁺.