The reproducibility of the highest ranking synthesis conditions were also tested, with the robotic platform set up to run 16 reactions over a 24 hour period. The powder was collected by centrifuge, and then washed with solvent and dried overnight. The combined PXRD pattern matched Al-PMOF perfectly, and the surface area and pore volume of the large sample determined from a N 2 isotherm at 77K were also comparable. Continuously synthesising using the platform this way can generate gram amounts of powder that can be used for further applications such as CO 2 capture at a large scale.