Temperatures are reported in degrees Celsius (°C), and reactions were run at room temperature (25 °C) where no temperature is listed. Reactions were carried out under a nitrogen atmosphere unless otherwise noted. Once reactions were complete and worked up, where necessary, solvent was removed via a rotary evaporator under reduced pressure. Purification via column chromatography was performed using pre-loaded silica gel cartridges on a Biotage automated purification system. The following abbreviations are used in schemes and/or experimental procedures: equiv (equivalent(s)), h (hours), mmol (millimoles), mg (milligrams), min (minutes), μmol (micromoles), and r.t. (room temperature). H NMR and additional microanalytical data was collected for intermediates and all final compounds to confirm their identity and assess their purity.