All reagents were obtained from Sigma-Aldrich, TCI Europe, Fisher, Manchester Organics, Alfa Aesar, and Combi-Blocks and used as received. Anhydrous solvents were purchased from Acros Organics and used without further purification. All gases for sorption analysis were supplied by BOC at a purity of ≥99.999%. Reactions were carried out under nitrogen atmosphere using standard Schlenk techniques.