(aq) (1250 µL) was added. The electrolyte was purged with N2 at a flow rate of 10 mL min-1 for 20 minutes. 5 cyclic voltammetry cycles were then conducted at a scan rate of 2 mV s-1 under continued gas flow. The electrolyte was then purged with CO2 at a flow rate of 10 mL min-1 for 30 minutes and a further 5 cyclic voltammetry cycles were performed at a scan rate of 2 mV s-1.