Crystal structure solution and refinements from SC-XRD data. After data collection, the unit cell was re-determined using a subset of the entire data collection. Intensity data were corrected for Lorentz, polarization, and background effects using CrysAlis Pro 38 for HTBZ-SAC and APEX4 39 for HTBZ-HMA and HTBZ-HOX. A numerical was used to refine the structure. Both of these programs were utilized within the OLEX2 software . The parameters are presented in Table .