While GPT-4, with careful prompting, can suggest the subsequent experimental conditions , this preliminary study manually selected the reaction conditions for improved suggestions. In the conditions mentioned earlier (Run 1), the reaction was conducted by dissolving 0.2 mmol of monomer in 40 mL of solution. In Runs 2 and 3, the amount of monomer was reduced to 0.1 and 0.05 mmol, respectively (Table ). As the concentration of the reaction solution was lowered, the time it took for the solution to become cloudy increased (Fig. and). For example, the mixture appeared at about 740 seconds opaque at 0.2 mmol (Run 1), partially opaque at 0.1 mmol (Run 2), and almost transparent at 0.05 mmol (Run 3). These differences are due to a decrease in polymerization speed due to lower concentrations and a reduction in the absolute number of particles that cause light scattering.