The standard reaction process for synthesizing the (Cu6-dpb) CAM was followed in this experiment, with the sole modification being the substitution of the dpb linker with dpt. Finally, we got truncated tetrahedron-shaped orange crystals (yield: 44.9% on the basis of Cu) were observed forming at the interface between the two immiscible liquid phases. The crystal morphology and chemical composition were confirmed through optical microscopy and SEM imaging combined with EDS analysis (Fig. and Fig. ).