Thus, a decagram scale arylation of 14a with arene 91 was performed in recirculating flow. The only modification made to the general procedure was the use of carbon felt instead of RVC and the current was adjusted linearly to 3A (30 mA/mmol). This first arylation delivered 12.65 grams of tertiary acid 31 in a 41% yield (100 mmol scale). The subsequent arylation of the RAE of 31 was then scaled up in batch to 2.4 mmol (1 gram) with arene 24, affording 463 mg of product 66, in 56% isolated yield. The overall route outlined above would clearly enable medicinal chemists to access a myriad of gem-diarylated scaffolds on scale and in a way that is amenable to parallel screening of SAR.