was from 5° to 55° with a step size of 0.01° and a dwell time of 0.15 s per step. SEM and EDX analysis were performed using a TESCAN MIRA3 field emission gun-scanning electron microscope equipped with an Oxford Instruments Aztec Energy X-maxN 80 EDX system. A Thermo Scientific Talos F200X G2 TEM (operating voltage 200 kV) was used for HAADF-STEM images and EDX maps. 300-mesh Ni grids with holey carbon film were used for TEM sample preparation. Powder XRD (PXRD) spectra of the catalyst were recorded by a Panalytical X'Pert Pro (K-α Cu radiation) diffractometer using a 1° min -1 scan rate.