The Eppendorf liquid handling system has space to generate 240 samples (10 locations each holding two trays with 12 samples in each) from one set of four suspension starting materials in each run and could deliver two runs per day. This is a larger number of samples than could be realistically measured on a labbased X-ray diffractometer per day, even if the instrument were dedicated to the workflow. Within our current equipment limitations, this would be 4 trays per day (48 samples per day), which could be increased by, for example, increasing the number of individual samples per tray (i.e., reducing the diameter of the wells). A sensible approach would be to prepare the sample sets at the rate at which the X-ray diffractometer can realistically measure (i.e., 48 per day in our case), so there is a continuous flow of samples through the workflow, with each stage always having a sample set in process, and the ability for results to feedback and influence the experimental design of new samples sets in a timely manner.