1.0 mRad. 92 X-ray data were collected using CrysAlisPro. For data processing the instrument was calibrated using LaB6 as standard. Then, X-ray data were reduced and integrated using CrysAlisPro. Peak hunting and unit cell indexing was performed using TOPAS software. Le Bail profile analysis was performed using JANA2020 software. Some samples suffer from high background scatter from the Fomblin YR-1800 oil used, due to the ratio of powder to oil.